Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design
Both the conventional one-factor-at-a-time (OFT) optimization, in which one of the factors is varied maintaining the other parameters fixed at constant levels, and the central composite design (CCD) optimization, in which all factors are varied simultaneously, were carried out for silk dyeing with c...
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my.utm.760982018-05-30T04:20:11Z http://eprints.utm.my/id/eprint/76098/ Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design Shahid, M. Zhou, Y. Tang, R. C. Chen, G. Wani, W. A. TP Chemical technology Both the conventional one-factor-at-a-time (OFT) optimization, in which one of the factors is varied maintaining the other parameters fixed at constant levels, and the central composite design (CCD) optimization, in which all factors are varied simultaneously, were carried out for silk dyeing with chlorogenic acid. The CCD experiments were designed with the help of Design-Expert 10.0.3 software (trial version) and used for evaluating the interactive effects of the four most important operating variables namely pH, temperature, time and dye concentration. The colour characteristics, fastness properties, FT-IR spectra and antioxidant activity of dyed fabrics were also evaluated. The silk fabrics dyed with chlorogenic acid displayed light yellowish brown colour, and exhibited good fastness properties and excellent antioxidant activity. Elsevier Ltd 2017 Article PeerReviewed Shahid, M. and Zhou, Y. and Tang, R. C. and Chen, G. and Wani, W. A. (2017) Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design. Dyes and Pigments, 138 . pp. 30-38. ISSN 0143-7208 https://www.scopus.com/inward/record.uri?eid=2-s2.0-85005976138&doi=10.1016%2fj.dyepig.2016.11.012&partnerID=40&md5=7f654e3d48ab2962c5eb9a46c2aa930b |
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TP Chemical technology Shahid, M. Zhou, Y. Tang, R. C. Chen, G. Wani, W. A. Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design |
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Both the conventional one-factor-at-a-time (OFT) optimization, in which one of the factors is varied maintaining the other parameters fixed at constant levels, and the central composite design (CCD) optimization, in which all factors are varied simultaneously, were carried out for silk dyeing with chlorogenic acid. The CCD experiments were designed with the help of Design-Expert 10.0.3 software (trial version) and used for evaluating the interactive effects of the four most important operating variables namely pH, temperature, time and dye concentration. The colour characteristics, fastness properties, FT-IR spectra and antioxidant activity of dyed fabrics were also evaluated. The silk fabrics dyed with chlorogenic acid displayed light yellowish brown colour, and exhibited good fastness properties and excellent antioxidant activity. |
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Article |
author |
Shahid, M. Zhou, Y. Tang, R. C. Chen, G. Wani, W. A. |
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Shahid, M. Zhou, Y. Tang, R. C. Chen, G. Wani, W. A. |
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Shahid, M. |
title |
Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design |
title_short |
Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design |
title_full |
Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design |
title_fullStr |
Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design |
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Colourful and antioxidant silk with chlorogenic acid: Process development and optimization by central composite design |
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colourful and antioxidant silk with chlorogenic acid: process development and optimization by central composite design |
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Elsevier Ltd |
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2017 |
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http://eprints.utm.my/id/eprint/76098/ https://www.scopus.com/inward/record.uri?eid=2-s2.0-85005976138&doi=10.1016%2fj.dyepig.2016.11.012&partnerID=40&md5=7f654e3d48ab2962c5eb9a46c2aa930b |
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