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Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors

Biogenic amines generally can be found in fish due to amines in fish undergoing a degradation process. According to the United States Food and Drug Administration (FDA), biogenic amines in fish and fish products can cause harm to consumers if consumed more than 50 µg/mL. Thus, it is important to ana...

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Main Authors: Ahlam, Inayatullah, Hamid Alkhair, Badrul, Muhammad Abdurrahman, Munir
Format: Article
Language:English
Published: Magister Program of Material Sciences, Graduate School of Universitas Sriwijaya 2021
Subjects:
QD Chemistry
Online Access:http://ir.unimas.my/id/eprint/43926/3/Fish%20Analysis.pdf
http://ir.unimas.my/id/eprint/43926/
https://sciencetechindonesia.com/index.php/jsti/article/view/260#:~:text=Five%20biogenic%20amines%20such%20as,biogenic%20amines%20structures%20were%20confirmed
https://doi.org/10.26554/sti.2021.6.1.1-7
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spelling my.unimas.ir.439262023-12-29T00:20:43Z http://ir.unimas.my/id/eprint/43926/ Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors Ahlam, Inayatullah Hamid Alkhair, Badrul Muhammad Abdurrahman, Munir QD Chemistry Biogenic amines generally can be found in fish due to amines in fish undergoing a degradation process. According to the United States Food and Drug Administration (FDA), biogenic amines in fish and fish products can cause harm to consumers if consumed more than 50 µg/mL. Thus, it is important to analyze them. Five biogenic amines such as heptylamine, histamine, tyramine, cadaverine and spermidine were extracted using soaking method with methanol 50% (v/v), a�erward they were detected in fish and fish products using gas chromatography – flame ionisation detector (GC-FID) and the biogenic amines structures were confirmed using mass spectrometry (MS). The detection limits (DLs) were range at 1.20 – 2.90 µg/mL. Histamine was detected in fish and fish products such as sardine (Sardinella gibosa) and mackerel (Scomberomorus guttatus) at concentration of 5.96 and 2.69 µg/mL, respectively, whereas cadaverine was found in sardine (Sardinella gibosa) at concentration of 4.96 µg/mL. Histamine concentrations in this study were detected below 50 µg/mL which is below the permissible threshold associated with scombroid poisoning. Magister Program of Material Sciences, Graduate School of Universitas Sriwijaya 2021-01-13 Article PeerReviewed text en http://ir.unimas.my/id/eprint/43926/3/Fish%20Analysis.pdf Ahlam, Inayatullah and Hamid Alkhair, Badrul and Muhammad Abdurrahman, Munir (2021) Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors. Science & Technology Indonesia, 6 (1). pp. 1-7. ISSN 2580-4391 https://sciencetechindonesia.com/index.php/jsti/article/view/260#:~:text=Five%20biogenic%20amines%20such%20as,biogenic%20amines%20structures%20were%20confirmed https://doi.org/10.26554/sti.2021.6.1.1-7
institution Universiti Malaysia Sarawak
building Centre for Academic Information Services (CAIS)
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Sarawak
content_source UNIMAS Institutional Repository
url_provider http://ir.unimas.my/
language English
topic QD Chemistry
spellingShingle QD Chemistry
Ahlam, Inayatullah
Hamid Alkhair, Badrul
Muhammad Abdurrahman, Munir
Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors
description Biogenic amines generally can be found in fish due to amines in fish undergoing a degradation process. According to the United States Food and Drug Administration (FDA), biogenic amines in fish and fish products can cause harm to consumers if consumed more than 50 µg/mL. Thus, it is important to analyze them. Five biogenic amines such as heptylamine, histamine, tyramine, cadaverine and spermidine were extracted using soaking method with methanol 50% (v/v), a�erward they were detected in fish and fish products using gas chromatography – flame ionisation detector (GC-FID) and the biogenic amines structures were confirmed using mass spectrometry (MS). The detection limits (DLs) were range at 1.20 – 2.90 µg/mL. Histamine was detected in fish and fish products such as sardine (Sardinella gibosa) and mackerel (Scomberomorus guttatus) at concentration of 5.96 and 2.69 µg/mL, respectively, whereas cadaverine was found in sardine (Sardinella gibosa) at concentration of 4.96 µg/mL. Histamine concentrations in this study were detected below 50 µg/mL which is below the permissible threshold associated with scombroid poisoning.
format Article
author Ahlam, Inayatullah
Hamid Alkhair, Badrul
Muhammad Abdurrahman, Munir
author_facet Ahlam, Inayatullah
Hamid Alkhair, Badrul
Muhammad Abdurrahman, Munir
author_sort Ahlam, Inayatullah
title Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors
title_short Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors
title_full Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors
title_fullStr Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors
title_full_unstemmed Fish Analysis Containing Biogenic Amines Using Gas Chromatography Equipped With Flame Ionization And Mass Spectrometer Detectors
title_sort fish analysis containing biogenic amines using gas chromatography equipped with flame ionization and mass spectrometer detectors
publisher Magister Program of Material Sciences, Graduate School of Universitas Sriwijaya
publishDate 2021
url http://ir.unimas.my/id/eprint/43926/3/Fish%20Analysis.pdf
http://ir.unimas.my/id/eprint/43926/
https://sciencetechindonesia.com/index.php/jsti/article/view/260#:~:text=Five%20biogenic%20amines%20such%20as,biogenic%20amines%20structures%20were%20confirmed
https://doi.org/10.26554/sti.2021.6.1.1-7
_version_ 1787140555012046848
score 13.211869

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