Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa

The synthesis of 4-allyoxy-11, 13-dimethoxystilbene has been made using a series of reactions. Protected iodophenol reaction was the first step using allyl bromide as a protecting agent. After that, through Wittig reaction the protected styrene was successfully synthesized. Both compound finally wer...

Full description

Saved in:
Bibliographic Details
Main Author: Che Pa, Mohd Farizh
Format: Thesis
Language:English
Published: 2005
Subjects:
Online Access:https://ir.uitm.edu.my/id/eprint/98485/1/98485.PDF
https://ir.uitm.edu.my/id/eprint/98485/
Tags: Add Tag
No Tags, Be the first to tag this record!
id my.uitm.ir.98485
record_format eprints
spelling my.uitm.ir.984852024-08-27T18:11:44Z https://ir.uitm.edu.my/id/eprint/98485/ Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa Che Pa, Mohd Farizh QD Chemistry RM Therapeutics. Pharmacology The synthesis of 4-allyoxy-11, 13-dimethoxystilbene has been made using a series of reactions. Protected iodophenol reaction was the first step using allyl bromide as a protecting agent. After that, through Wittig reaction the protected styrene was successfully synthesized. Both compound finally were coupled in the presence of palladium chloride as a catalyst and triphenylphospine as a ligand via Heck reaction to give about 28.84% yield. TLC, UV spectrophotometer and NMR spectrometer were used in the determination of every product for every step. However, the desired compound, which is expected to be formed, was not successfully synthesized due to unknown reason. 2005 Thesis NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/98485/1/98485.PDF Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa. (2005) Degree thesis, thesis, Universiti Teknologi MARA (Kampus Puncak Alam).
institution Universiti Teknologi Mara
building Tun Abdul Razak Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
url_provider http://ir.uitm.edu.my/
language English
topic QD Chemistry
RM Therapeutics. Pharmacology
spellingShingle QD Chemistry
RM Therapeutics. Pharmacology
Che Pa, Mohd Farizh
Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa
description The synthesis of 4-allyoxy-11, 13-dimethoxystilbene has been made using a series of reactions. Protected iodophenol reaction was the first step using allyl bromide as a protecting agent. After that, through Wittig reaction the protected styrene was successfully synthesized. Both compound finally were coupled in the presence of palladium chloride as a catalyst and triphenylphospine as a ligand via Heck reaction to give about 28.84% yield. TLC, UV spectrophotometer and NMR spectrometer were used in the determination of every product for every step. However, the desired compound, which is expected to be formed, was not successfully synthesized due to unknown reason.
format Thesis
author Che Pa, Mohd Farizh
author_facet Che Pa, Mohd Farizh
author_sort Che Pa, Mohd Farizh
title Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa
title_short Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa
title_full Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa
title_fullStr Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa
title_full_unstemmed Synthesis of 4-allyloxy-11, 13-dimethoxystilbene / Mohd Farizh Che Pa
title_sort synthesis of 4-allyloxy-11, 13-dimethoxystilbene / mohd farizh che pa
publishDate 2005
url https://ir.uitm.edu.my/id/eprint/98485/1/98485.PDF
https://ir.uitm.edu.my/id/eprint/98485/
_version_ 1808976036257333248
score 13.223943