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Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)

Endocrine-disrupting compounds are routinely detected in environmental water. In this study, a simple and rapid sample preparation method based on ultrasound-assisted salt-induced liquid-liquid microextraction (UA-SI-LLME) followed by high performance liquid chromatography�diode array detection (H...

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Main Authors: Rozaini, M.N.H., Saad, B., Yahaya, N., Lim, J.W., Mohd Aris, M.N., Ramachandran, M.R.
Format: Article
Published: Taylor and Francis Ltd. 2022
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-85106048229&doi=10.1080%2f00032719.2021.1919691&partnerID=40&md5=99bca6089af6dce8d4b978af059f1588
http://eprints.utp.edu.my/32382/
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spelling my.utp.eprints.323822022-03-29T01:25:53Z Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD) Rozaini, M.N.H. Saad, B. Yahaya, N. Lim, J.W. Mohd Aris, M.N. Ramachandran, M.R. Endocrine-disrupting compounds are routinely detected in environmental water. In this study, a simple and rapid sample preparation method based on ultrasound-assisted salt-induced liquid-liquid microextraction (UA-SI-LLME) followed by high performance liquid chromatography�diode array detection (HPLC-DAD) was developed for the determination of triclosan, triclocarban and methyl-triclosan in water. Parameters that affect the extraction efficiency�such as type and mass of salt, type and volume of extraction solvent, extraction time, sample pH and sample volume�were studied. Under the optimized conditions, the method demonstrated linearity from 0.18 to 1000 µg L�1 with coefficients of determination R2 � 0.9899, limits of detection from 0.05 to 0.2 µg L�1, and good recoveries (> 70) with relative standard deviations < 10. The method was applied for the determination of triclosan, triclocarban, and methyl-triclosan in swimming pool, lake, and wastewater. The greenness of the method was quantified using the Analytical Eco-Scale Index. © 2022 Taylor & Francis Group, LLC. Taylor and Francis Ltd. 2022 Article NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-85106048229&doi=10.1080%2f00032719.2021.1919691&partnerID=40&md5=99bca6089af6dce8d4b978af059f1588 Rozaini, M.N.H. and Saad, B. and Yahaya, N. and Lim, J.W. and Mohd Aris, M.N. and Ramachandran, M.R. (2022) Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD). Analytical Letters, 55 (1). pp. 132-145. http://eprints.utp.edu.my/32382/
institution Universiti Teknologi Petronas
building UTP Resource Centre
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Petronas
content_source UTP Institutional Repository
url_provider http://eprints.utp.edu.my/
description Endocrine-disrupting compounds are routinely detected in environmental water. In this study, a simple and rapid sample preparation method based on ultrasound-assisted salt-induced liquid-liquid microextraction (UA-SI-LLME) followed by high performance liquid chromatography�diode array detection (HPLC-DAD) was developed for the determination of triclosan, triclocarban and methyl-triclosan in water. Parameters that affect the extraction efficiency�such as type and mass of salt, type and volume of extraction solvent, extraction time, sample pH and sample volume�were studied. Under the optimized conditions, the method demonstrated linearity from 0.18 to 1000 µg L�1 with coefficients of determination R2 � 0.9899, limits of detection from 0.05 to 0.2 µg L�1, and good recoveries (> 70) with relative standard deviations < 10. The method was applied for the determination of triclosan, triclocarban, and methyl-triclosan in swimming pool, lake, and wastewater. The greenness of the method was quantified using the Analytical Eco-Scale Index. © 2022 Taylor & Francis Group, LLC.
format Article
author Rozaini, M.N.H.
Saad, B.
Yahaya, N.
Lim, J.W.
Mohd Aris, M.N.
Ramachandran, M.R.
spellingShingle Rozaini, M.N.H.
Saad, B.
Yahaya, N.
Lim, J.W.
Mohd Aris, M.N.
Ramachandran, M.R.
Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
author_facet Rozaini, M.N.H.
Saad, B.
Yahaya, N.
Lim, J.W.
Mohd Aris, M.N.
Ramachandran, M.R.
author_sort Rozaini, M.N.H.
title Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
title_short Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
title_full Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
title_fullStr Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
title_full_unstemmed Determination of Three Endocrine Disruptors in Water Samples by Ultrasound-Assisted Salt-Induced Liquid-Liquid Microextraction (UA-SI-LLME) and High-Performance Liquid Chromatography�Diode Array Detection (HPLC-DAD)
title_sort determination of three endocrine disruptors in water samples by ultrasound-assisted salt-induced liquid-liquid microextraction (ua-si-llme) and high-performance liquid chromatography�diode array detection (hplc-dad)
publisher Taylor and Francis Ltd.
publishDate 2022
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-85106048229&doi=10.1080%2f00032719.2021.1919691&partnerID=40&md5=99bca6089af6dce8d4b978af059f1588
http://eprints.utp.edu.my/32382/
_version_ 1738657379405266944
score 13.211869

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