Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique

Carbon nanotubes (CNTs) with its exceptional thermal and mechanical properties hold the promise of delivering high performance nanocomposite materials. To utilize CNTs as effective reinforcement in metal nanocomposites, appropriate dispersion and robust interfacial adhesion between individual CNT an...

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Main Authors: Muhsan, A.S., Ahmad, F., Mohamed, N.M., Megat Yusoff, P.S.M., Raza, M.R.
Format: Article
Published: American Scientific Publishers 2014
Online Access:https://www.scopus.com/inward/record.uri?eid=2-s2.0-84918788971&doi=10.1166%2fnnl.2014.1794&partnerID=40&md5=e580dc28b1655229b024428253df2a62
http://eprints.utp.edu.my/31848/
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spelling my.utp.eprints.318482022-03-29T03:38:28Z Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique Muhsan, A.S. Ahmad, F. Mohamed, N.M. Megat Yusoff, P.S.M. Raza, M.R. Carbon nanotubes (CNTs) with its exceptional thermal and mechanical properties hold the promise of delivering high performance nanocomposite materials. To utilize CNTs as effective reinforcement in metal nanocomposites, appropriate dispersion and robust interfacial adhesion between individual CNT and metal matrix have to be certain. This work presents a novel combined technique of nanoscale dispersion (NSD) of functionalized multiwalled carbon nanotubes (MWCNTs) in copper (Cu) matrix composite followed by powder injection molding (PIM). MWCNTs contents were varied from 0 to 10 volume fraction. Evidences on the existence of functional groups and microstructural analysis of the fabricated nanocomposites were determined using TEM, EDX, FESEM and FTIR. Thermal conductivity and elasticity measurements were also performed. The results showed that the impurities of the pristine MWCNTs such as Fe, Ni catalyst, and the amorphous carbon have been significantly removed after sonication process. FESEM and TEM observations showed high stability of MWCNTs at elevated temperatures and uniform dispersion of MWCNTs in Cu matrix at different volume fractions and sintering temperatures (950, 1000 and 1050 °C). The experimentally measured thermal conductivities of Cu/MWCNTs nanocomposites showed remarkable increase (11.25 higher than pure sintered Cu) with addition of 1 vol. MWCNTs, while the modulus of elasticity (Young's modulus) of Cu/MWCNTs nanocomposites sintered at 1050 °C for 2 h was increased proportionally to the increment in MWCNTs contents. Copyright © 2014 American Scientific Publishers American Scientific Publishers 2014 Article NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-84918788971&doi=10.1166%2fnnl.2014.1794&partnerID=40&md5=e580dc28b1655229b024428253df2a62 Muhsan, A.S. and Ahmad, F. and Mohamed, N.M. and Megat Yusoff, P.S.M. and Raza, M.R. (2014) Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique. Nanoscience and Nanotechnology Letters, 6 (10). pp. 865-874. http://eprints.utp.edu.my/31848/
institution Universiti Teknologi Petronas
building UTP Resource Centre
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Petronas
content_source UTP Institutional Repository
url_provider http://eprints.utp.edu.my/
description Carbon nanotubes (CNTs) with its exceptional thermal and mechanical properties hold the promise of delivering high performance nanocomposite materials. To utilize CNTs as effective reinforcement in metal nanocomposites, appropriate dispersion and robust interfacial adhesion between individual CNT and metal matrix have to be certain. This work presents a novel combined technique of nanoscale dispersion (NSD) of functionalized multiwalled carbon nanotubes (MWCNTs) in copper (Cu) matrix composite followed by powder injection molding (PIM). MWCNTs contents were varied from 0 to 10 volume fraction. Evidences on the existence of functional groups and microstructural analysis of the fabricated nanocomposites were determined using TEM, EDX, FESEM and FTIR. Thermal conductivity and elasticity measurements were also performed. The results showed that the impurities of the pristine MWCNTs such as Fe, Ni catalyst, and the amorphous carbon have been significantly removed after sonication process. FESEM and TEM observations showed high stability of MWCNTs at elevated temperatures and uniform dispersion of MWCNTs in Cu matrix at different volume fractions and sintering temperatures (950, 1000 and 1050 °C). The experimentally measured thermal conductivities of Cu/MWCNTs nanocomposites showed remarkable increase (11.25 higher than pure sintered Cu) with addition of 1 vol. MWCNTs, while the modulus of elasticity (Young's modulus) of Cu/MWCNTs nanocomposites sintered at 1050 °C for 2 h was increased proportionally to the increment in MWCNTs contents. Copyright © 2014 American Scientific Publishers
format Article
author Muhsan, A.S.
Ahmad, F.
Mohamed, N.M.
Megat Yusoff, P.S.M.
Raza, M.R.
spellingShingle Muhsan, A.S.
Ahmad, F.
Mohamed, N.M.
Megat Yusoff, P.S.M.
Raza, M.R.
Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique
author_facet Muhsan, A.S.
Ahmad, F.
Mohamed, N.M.
Megat Yusoff, P.S.M.
Raza, M.R.
author_sort Muhsan, A.S.
title Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique
title_short Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique
title_full Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique
title_fullStr Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique
title_full_unstemmed Homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique
title_sort homogeneous distribution of carbon nanotubes in copper matrix nanocomposites fabricated via combined technique
publisher American Scientific Publishers
publishDate 2014
url https://www.scopus.com/inward/record.uri?eid=2-s2.0-84918788971&doi=10.1166%2fnnl.2014.1794&partnerID=40&md5=e580dc28b1655229b024428253df2a62
http://eprints.utp.edu.my/31848/
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