Catalytic transfer hydrogenation of castor oil using glycerolbased reaction
A catalytic transfer hydrogenation of castor oil using glycerol-based is a process of adding hydrogen to the castor oil to produce hydrogenated castor oil with the addition of 10 Pd/C as the catalyst and glycerol as a hydrogen donor. The reaction occurred at the reaction temperature of 178°C for an...
Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Conference or Workshop Item |
| Published: |
Institute of Physics Publishing
2020
|
| Online Access: | https://www.scopus.com/inward/record.uri?eid=2-s2.0-85081288717&doi=10.1088%2f1757-899X%2f736%2f4%2f042040&partnerID=40&md5=12234ea9a51389092258dffad9f88082 http://eprints.utp.edu.my/24637/ |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| id |
my.utp.eprints.24637 |
|---|---|
| record_format |
eprints |
| spelling |
my.utp.eprints.246372021-08-27T06:24:45Z Catalytic transfer hydrogenation of castor oil using glycerolbased reaction Amin, U.S.M. Osman, N.B. Uemura, Y. Majid, N.M. A catalytic transfer hydrogenation of castor oil using glycerol-based is a process of adding hydrogen to the castor oil to produce hydrogenated castor oil with the addition of 10 Pd/C as the catalyst and glycerol as a hydrogen donor. The reaction occurred at the reaction temperature of 178°C for an hour. To prove whether glycerol can be one of the hydrogen donors like limonene that is commonly used, the research started by using pure glycerol as the hydrogen donor and as a control to determine the protocol. A direct heating aparatus connected with a reflux system was used for this experiment. The result from FTIR along with the melting point shows the formation of hydrogenated castor oil from this reaction. The increment in melting point value and the absence of C=C peak (1655.79 cm-1) from FTIR spectrum shows that the catalytic transfer hydrogenation successfully occurred. The melting point of the hydrogenated castor oil is 65°C and the melting point of castor oil is -7°C. Therefore, it was proven that, the glycerol can be used as the hydrogen donor for the castor oil for a catalytic transfer hydrogenation reaction. © Published under licence by IOP Publishing Ltd. Institute of Physics Publishing 2020 Conference or Workshop Item NonPeerReviewed https://www.scopus.com/inward/record.uri?eid=2-s2.0-85081288717&doi=10.1088%2f1757-899X%2f736%2f4%2f042040&partnerID=40&md5=12234ea9a51389092258dffad9f88082 Amin, U.S.M. and Osman, N.B. and Uemura, Y. and Majid, N.M. (2020) Catalytic transfer hydrogenation of castor oil using glycerolbased reaction. In: UNSPECIFIED. http://eprints.utp.edu.my/24637/ |
| institution |
Universiti Teknologi Petronas |
| building |
UTP Resource Centre |
| collection |
Institutional Repository |
| continent |
Asia |
| country |
Malaysia |
| content_provider |
Universiti Teknologi Petronas |
| content_source |
UTP Institutional Repository |
| url_provider |
http://eprints.utp.edu.my/ |
| description |
A catalytic transfer hydrogenation of castor oil using glycerol-based is a process of adding hydrogen to the castor oil to produce hydrogenated castor oil with the addition of 10 Pd/C as the catalyst and glycerol as a hydrogen donor. The reaction occurred at the reaction temperature of 178°C for an hour. To prove whether glycerol can be one of the hydrogen donors like limonene that is commonly used, the research started by using pure glycerol as the hydrogen donor and as a control to determine the protocol. A direct heating aparatus connected with a reflux system was used for this experiment. The result from FTIR along with the melting point shows the formation of hydrogenated castor oil from this reaction. The increment in melting point value and the absence of C=C peak (1655.79 cm-1) from FTIR spectrum shows that the catalytic transfer hydrogenation successfully occurred. The melting point of the hydrogenated castor oil is 65°C and the melting point of castor oil is -7°C. Therefore, it was proven that, the glycerol can be used as the hydrogen donor for the castor oil for a catalytic transfer hydrogenation reaction. © Published under licence by IOP Publishing Ltd. |
| format |
Conference or Workshop Item |
| author |
Amin, U.S.M. Osman, N.B. Uemura, Y. Majid, N.M. |
| spellingShingle |
Amin, U.S.M. Osman, N.B. Uemura, Y. Majid, N.M. Catalytic transfer hydrogenation of castor oil using glycerolbased reaction |
| author_facet |
Amin, U.S.M. Osman, N.B. Uemura, Y. Majid, N.M. |
| author_sort |
Amin, U.S.M. |
| title |
Catalytic transfer hydrogenation of castor oil using glycerolbased reaction |
| title_short |
Catalytic transfer hydrogenation of castor oil using glycerolbased reaction |
| title_full |
Catalytic transfer hydrogenation of castor oil using glycerolbased reaction |
| title_fullStr |
Catalytic transfer hydrogenation of castor oil using glycerolbased reaction |
| title_full_unstemmed |
Catalytic transfer hydrogenation of castor oil using glycerolbased reaction |
| title_sort |
catalytic transfer hydrogenation of castor oil using glycerolbased reaction |
| publisher |
Institute of Physics Publishing |
| publishDate |
2020 |
| url |
https://www.scopus.com/inward/record.uri?eid=2-s2.0-85081288717&doi=10.1088%2f1757-899X%2f736%2f4%2f042040&partnerID=40&md5=12234ea9a51389092258dffad9f88082 http://eprints.utp.edu.my/24637/ |
| _version_ |
1738656618114973696 |
| score |
13.211869 |