Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis
Radiation induced technique was employed during the synthesis of silver nanoparticles (AgNPs) on pullulan. In this study, the Ag-NPs on pullulan by γ irradiated process is performed to reduce Ag+ ions at the ambient temperature without using excessive reducing agents or producing unwanted by-product...
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my.utm.925692021-09-30T15:14:43Z http://eprints.utm.my/id/eprint/92569/ Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis Salleh, M. S. N. Rasit Ali, R. Shameli, K. Hamzah, M. Y. Chan, J. Z. T Technology (General) Radiation induced technique was employed during the synthesis of silver nanoparticles (AgNPs) on pullulan. In this study, the Ag-NPs on pullulan by γ irradiated process is performed to reduce Ag+ ions at the ambient temperature without using excessive reducing agents or producing unwanted by-products of the reductant. Moreover, reducing agent can be uniformly distributed in the solution and AgNPs are produced in highly pure and stable form. The results from ultraviolet-visible spectroscopy (UV-vis) and XRD demonstrated that the silver nanoparticles can be synthesize using pullulan. This can be confirmed by absorption band of UV-vis spectrum at 420 nm as well as the XRD pattern at (1 1 1), (2 0 0), (2 2 0), and (3 1 1) planes of silver. In addition, the pullulan also acts as a reducing and stabilizing agent. TEM images showed formed AgNPs are spherical in shape with smooth edges. The TEM also revealed that the increasing radiation dose decreases the particle size and increase the rate of reduction. It was found that the mean diameter of silver nanoparticles was about 3.98-14.87 nm. In addition, the size of the AgNPs is believed can be tuned by controlling the radiation doses. The γ-rays doses also provide the powerful reduction process in a harmless condition by producing a very stable silver nanoparticles. 2020 Conference or Workshop Item PeerReviewed application/pdf en http://eprints.utm.my/id/eprint/92569/1/RoshafimaRasitAli2020_SilverNanoparticlesonPullulanderivedviaGamma.pdf Salleh, M. S. N. and Rasit Ali, R. and Shameli, K. and Hamzah, M. Y. and Chan, J. Z. (2020) Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis. In: 8th Conference on Emerging Energy and Process Technology 2019, CONCEPT 2019, 27 - 28 November 2019, Kuala Lumpur, Malaysia. http://dx.doi.org/10.1088/1757-899X/808/1/012030 |
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Radiation induced technique was employed during the synthesis of silver nanoparticles (AgNPs) on pullulan. In this study, the Ag-NPs on pullulan by γ irradiated process is performed to reduce Ag+ ions at the ambient temperature without using excessive reducing agents or producing unwanted by-products of the reductant. Moreover, reducing agent can be uniformly distributed in the solution and AgNPs are produced in highly pure and stable form. The results from ultraviolet-visible spectroscopy (UV-vis) and XRD demonstrated that the silver nanoparticles can be synthesize using pullulan. This can be confirmed by absorption band of UV-vis spectrum at 420 nm as well as the XRD pattern at (1 1 1), (2 0 0), (2 2 0), and (3 1 1) planes of silver. In addition, the pullulan also acts as a reducing and stabilizing agent. TEM images showed formed AgNPs are spherical in shape with smooth edges. The TEM also revealed that the increasing radiation dose decreases the particle size and increase the rate of reduction. It was found that the mean diameter of silver nanoparticles was about 3.98-14.87 nm. In addition, the size of the AgNPs is believed can be tuned by controlling the radiation doses. The γ-rays doses also provide the powerful reduction process in a harmless condition by producing a very stable silver nanoparticles. |
format |
Conference or Workshop Item |
author |
Salleh, M. S. N. Rasit Ali, R. Shameli, K. Hamzah, M. Y. Chan, J. Z. |
author_facet |
Salleh, M. S. N. Rasit Ali, R. Shameli, K. Hamzah, M. Y. Chan, J. Z. |
author_sort |
Salleh, M. S. N. |
title |
Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis |
title_short |
Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis |
title_full |
Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis |
title_fullStr |
Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis |
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Silver nanoparticles on pullulan derived via gamma irradiation method: A preliminary analysis |
title_sort |
silver nanoparticles on pullulan derived via gamma irradiation method: a preliminary analysis |
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2020 |
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http://eprints.utm.my/id/eprint/92569/1/RoshafimaRasitAli2020_SilverNanoparticlesonPullulanderivedviaGamma.pdf http://eprints.utm.my/id/eprint/92569/ http://dx.doi.org/10.1088/1757-899X/808/1/012030 |
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13.211869 |