One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties
Silver, Ag nanoparticles were prepared via one-pot reduction method with two different reducing agents of aniline and NaBH4 whereby the effect of different factors such as the order of mixing the reactants, presence of a stabilizer and time on stability, size and concentration of the silver nanopart...
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my.utm.917192021-07-27T06:23:36Z http://eprints.utm.my/id/eprint/91719/ One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties Yazdi, Mahsa Khoshkhooy Bakar, Mohd. Bakri Nik Malek, Nik Ahmad Nizam QD Chemistry Silver, Ag nanoparticles were prepared via one-pot reduction method with two different reducing agents of aniline and NaBH4 whereby the effect of different factors such as the order of mixing the reactants, presence of a stabilizer and time on stability, size and concentration of the silver nanoparticles were studied using UV-Vis. The resulted colloidal Ag was then incorporated into poly(methyl methacrylate), PMMA nanoparticles through miniemulsion. The obtained products were characterized with UV-Vis DR and TEM to investigate the presence of Ag in the samples and study its morphology. The occurrence of the polymerization was analyzed with FTIR and 1HNMR and the antibacterial activity of the samples was tested via Kirby-Bauer method. Results confirmed the successful synthesis of PMMA/Ag nanoparticles and measurements of the clear zone of inhibition from antimicrobial tests showed that by increasing the concentration of the Ag nanoparticles in the samples, the antibacterial activity was increased. Penerbit Utm Press 2020 Article PeerReviewed Yazdi, Mahsa Khoshkhooy and Bakar, Mohd. Bakri and Nik Malek, Nik Ahmad Nizam (2020) One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties. Malaysian Journal of Fundamental and Applied Sciences, 16 (6). pp. 360-365. ISSN 2289-599X https://mjfas.utm.my/index.php/mjfas/article/view/2001 |
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QD Chemistry Yazdi, Mahsa Khoshkhooy Bakar, Mohd. Bakri Nik Malek, Nik Ahmad Nizam One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties |
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Silver, Ag nanoparticles were prepared via one-pot reduction method with two different reducing agents of aniline and NaBH4 whereby the effect of different factors such as the order of mixing the reactants, presence of a stabilizer and time on stability, size and concentration of the silver nanoparticles were studied using UV-Vis. The resulted colloidal Ag was then incorporated into poly(methyl methacrylate), PMMA nanoparticles through miniemulsion. The obtained products were characterized with UV-Vis DR and TEM to investigate the presence of Ag in the samples and study its morphology. The occurrence of the polymerization was analyzed with FTIR and 1HNMR and the antibacterial activity of the samples was tested via Kirby-Bauer method. Results confirmed the successful synthesis of PMMA/Ag nanoparticles and measurements of the clear zone of inhibition from antimicrobial tests showed that by increasing the concentration of the Ag nanoparticles in the samples, the antibacterial activity was increased. |
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Article |
author |
Yazdi, Mahsa Khoshkhooy Bakar, Mohd. Bakri Nik Malek, Nik Ahmad Nizam |
author_facet |
Yazdi, Mahsa Khoshkhooy Bakar, Mohd. Bakri Nik Malek, Nik Ahmad Nizam |
author_sort |
Yazdi, Mahsa Khoshkhooy |
title |
One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties |
title_short |
One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties |
title_full |
One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties |
title_fullStr |
One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties |
title_full_unstemmed |
One pot synthesis of PMMA/silver nanoparticles and its antibacterial properties |
title_sort |
one pot synthesis of pmma/silver nanoparticles and its antibacterial properties |
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Penerbit Utm Press |
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2020 |
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http://eprints.utm.my/id/eprint/91719/ https://mjfas.utm.my/index.php/mjfas/article/view/2001 |
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