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Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik

A two-dimensional zeolitic imidazolate framework with a leaf-like structure (ZIF-L) was synthesized in aqueous solution at room temperature with a molar ratio of Zn+2/Hmim (1: 8). Various triethylamine (TEA) concentrations were also used for the rapid production of ZIF-L. Different characterization...

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主要な著者: Khan, I. U., Othman, M. H. D., Jaafar, J., Hashim, H., Ismail, A. F., Rahman, M. A., Ismail, N.
フォーマット: 論文
言語:English
出版事項: Malaysian Society of Analytical Sciences 2018
主題:
TP Chemical technology
オンライン･アクセス:http://eprints.utm.my/id/eprint/79939/1/ImranUllahKhan2018_RapidSynthesisandCharacterizationofLeafLikeZeolitic.pdf
http://eprints.utm.my/id/eprint/79939/
http://dx.doi.org/10.17576/mjas-2018-2203-24
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spelling my.utm.799392019-01-28T07:02:14Z http://eprints.utm.my/id/eprint/79939/ Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik Khan, I. U. Othman, M. H. D. Jaafar, J. Hashim, H. Ismail, A. F. Rahman, M. A. Ismail, N. TP Chemical technology A two-dimensional zeolitic imidazolate framework with a leaf-like structure (ZIF-L) was synthesized in aqueous solution at room temperature with a molar ratio of Zn+2/Hmim (1: 8). Various triethylamine (TEA) concentrations were also used for the rapid production of ZIF-L. Different characterization techniques like X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM) and thermogravimetric analysis (TGA) were performed to investigate the effect of base type additive triethylamine (TEA) on the crystal morphology, crystallinity, particle size and thermal stability of ZIF-L particles. From the experimental results, it was found that ZIF-L with a particle size of 5.3 μm was formed at TEA/total mole ratio of 0, but particle size was decreased when TEA/total mole ratio was increased up to 0.0003. The smallest ZIF-L particles obtained were 3 μm that showed excellent thermal stability. It can be concluded that this promising synthesis method with base-type additive would provide the new insights in the development of ZIFs materials in economical ways. © 2018, Malaysian Society of Analytical Sciences. Malaysian Society of Analytical Sciences 2018 Article PeerReviewed application/pdf en http://eprints.utm.my/id/eprint/79939/1/ImranUllahKhan2018_RapidSynthesisandCharacterizationofLeafLikeZeolitic.pdf Khan, I. U. and Othman, M. H. D. and Jaafar, J. and Hashim, H. and Ismail, A. F. and Rahman, M. A. and Ismail, N. (2018) Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik. Malaysian Journal of Analytical Sciences, 22 (3). pp. 553-560. ISSN 1394-2506 http://dx.doi.org/10.17576/mjas-2018-2203-24 DOI:10.17576/mjas-2018-2203-24
institution Universiti Teknologi Malaysia
building UTM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Malaysia
content_source UTM Institutional Repository
url_provider http://eprints.utm.my/
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Khan, I. U.
Othman, M. H. D.
Jaafar, J.
Hashim, H.
Ismail, A. F.
Rahman, M. A.
Ismail, N.
Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik
description A two-dimensional zeolitic imidazolate framework with a leaf-like structure (ZIF-L) was synthesized in aqueous solution at room temperature with a molar ratio of Zn+2/Hmim (1: 8). Various triethylamine (TEA) concentrations were also used for the rapid production of ZIF-L. Different characterization techniques like X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM) and thermogravimetric analysis (TGA) were performed to investigate the effect of base type additive triethylamine (TEA) on the crystal morphology, crystallinity, particle size and thermal stability of ZIF-L particles. From the experimental results, it was found that ZIF-L with a particle size of 5.3 μm was formed at TEA/total mole ratio of 0, but particle size was decreased when TEA/total mole ratio was increased up to 0.0003. The smallest ZIF-L particles obtained were 3 μm that showed excellent thermal stability. It can be concluded that this promising synthesis method with base-type additive would provide the new insights in the development of ZIFs materials in economical ways. © 2018, Malaysian Society of Analytical Sciences.
format Article
author Khan, I. U.
Othman, M. H. D.
Jaafar, J.
Hashim, H.
Ismail, A. F.
Rahman, M. A.
Ismail, N.
author_facet Khan, I. U.
Othman, M. H. D.
Jaafar, J.
Hashim, H.
Ismail, A. F.
Rahman, M. A.
Ismail, N.
author_sort Khan, I. U.
title Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik
title_short Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik
title_full Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik
title_fullStr Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik
title_full_unstemmed Rapid synthesis and characterization of leaf-like zeolitic imidazolate framework Sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik
title_sort rapid synthesis and characterization of leaf-like zeolitic imidazolate framework sintesis cepat dan pencirian kerangka seperti daun imidazolat zeolitik
publisher Malaysian Society of Analytical Sciences
publishDate 2018
url http://eprints.utm.my/id/eprint/79939/1/ImranUllahKhan2018_RapidSynthesisandCharacterizationofLeafLikeZeolitic.pdf
http://eprints.utm.my/id/eprint/79939/
http://dx.doi.org/10.17576/mjas-2018-2203-24
_version_ 1643658337016872960
score 13.251813

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