Effect of pre-annealing temperature on the growth of aligned α-Fe2o3 nanowires via a two-step thermal oxidation

Pre-annealing as part of a two-step thermal oxidation process has a significant effect on the growth of hematite (α-Fe2O3) nanowires on Fe foil. High-density aligned nanowires were obtained on iron foils pre-annealed at 300°C under a dry air flow for 30min. The X-ray diffraction (XRD) patterns indi...

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Bibliographic Details
Main Authors: Mohamed Rashid, Norhana, Kishi, Naoki, Soga, Tetsuo
Format: Article
Published: World Scientific Publishing Co. Pte Ltd 2016
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Online Access:http://eprints.utm.my/id/eprint/69295/
http://dx.doi.org/10.1142/S0218625X1650027X
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Summary:Pre-annealing as part of a two-step thermal oxidation process has a significant effect on the growth of hematite (α-Fe2O3) nanowires on Fe foil. High-density aligned nanowires were obtained on iron foils pre-annealed at 300°C under a dry air flow for 30min. The X-ray diffraction (XRD) patterns indicate that the nanowires are transformed from the small α-Fe2O3 grains and uniquely grow in the (110) direction. The formation of a high-density of small grains by pre-annealing improved the alignment and density of the α-Fe2O3 nanowires.