Staff View: Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin

Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin

Turmeric flavour is important in Asian cuisine; however, the production of turmeric-based ingredient with the current method of extraction of turmeric oleoresin is very laborious, time consuming and consumes large amount of solvent, coupled with limited solubility in aqueous solution, which limits i...

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Main Authors:	Hadi, Binta Jume, Sanagi, Mohd. Marsin, Wan Ibrahim, W. A., Jamil, Shajarahtunnur, AbdullahiMu’azu, Mohammed, Aboul Enein, Hassan Y.
Format:	Article
Published:	Springer New York 2015
Subjects:	TP Chemical technology
Online Access:	http://eprints.utm.my/id/eprint/55952/ http://dx.doi.org/10.1007/s12161-014-0016-3
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id	my.utm.55952
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spelling	my.utm.559522017-08-25T10:51:43Z http://eprints.utm.my/id/eprint/55952/ Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin Hadi, Binta Jume Sanagi, Mohd. Marsin Wan Ibrahim, W. A. Jamil, Shajarahtunnur AbdullahiMu’azu, Mohammed Aboul Enein, Hassan Y. TP Chemical technology Turmeric flavour is important in Asian cuisine; however, the production of turmeric-based ingredient with the current method of extraction of turmeric oleoresin is very laborious, time consuming and consumes large amount of solvent, coupled with limited solubility in aqueous solution, which limits its application to food system. The extract was optimised by determining the content of three marker curcuminoid compounds, namely, curcumin (C), demethoxycurcumin (DMC) and bisdemethoxycurcumin (BDMC). The optimised extraction parameters for ultrasonic-assisted extraction (UAE) with aqueous extraction solvent for curcuminoids were amplitude of 100, particle size of 0.30–0.60 mm, extraction time of 20 min, extraction solvent volume of 10 mL and extraction temperature of 60 °C. The applications showed remarkable improvements in terms of reduced extraction time, solvent consumption, extraction yield and the quality of extracts. The turmeric oleoresin was successfully solubilised in aqueous solution by forming inclusion complex with methyl-ß-cyclodextrin (Mß-CD). Phase solubility studies used curcumin as a marker compounds to represent turmeric oleoresin. In the presence of Mß-CD, the curcumin was enhanced. Result from characterisation of inclusion complexes with Fourier transform infrared (FTIR) spectrometry indicates that all the mixing methods were found to be suitable for encapsulation. However, scanning electron microscopy (SEM) shows a drastic change in particle sizes, indicating a formation of a new solid phase in kneading method, implying it as the best mixing method. Springer New York 2015-10-18 Article PeerReviewed Hadi, Binta Jume and Sanagi, Mohd. Marsin and Wan Ibrahim, W. A. and Jamil, Shajarahtunnur and AbdullahiMu’azu, Mohammed and Aboul Enein, Hassan Y. (2015) Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin. Food Analytical Methods, 8 (6). pp. 1373-1381. ISSN 1936-9751 http://dx.doi.org/10.1007/s12161-014-0016-3 DOI:10.1007/s12161-014-0016-3
institution	Universiti Teknologi Malaysia
building	UTM Library
collection	Institutional Repository
continent	Asia
country	Malaysia
content_provider	Universiti Teknologi Malaysia
content_source	UTM Institutional Repository
url_provider	http://eprints.utm.my/
topic	TP Chemical technology
spellingShingle	TP Chemical technology Hadi, Binta Jume Sanagi, Mohd. Marsin Wan Ibrahim, W. A. Jamil, Shajarahtunnur AbdullahiMu’azu, Mohammed Aboul Enein, Hassan Y. Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin
description	Turmeric flavour is important in Asian cuisine; however, the production of turmeric-based ingredient with the current method of extraction of turmeric oleoresin is very laborious, time consuming and consumes large amount of solvent, coupled with limited solubility in aqueous solution, which limits its application to food system. The extract was optimised by determining the content of three marker curcuminoid compounds, namely, curcumin (C), demethoxycurcumin (DMC) and bisdemethoxycurcumin (BDMC). The optimised extraction parameters for ultrasonic-assisted extraction (UAE) with aqueous extraction solvent for curcuminoids were amplitude of 100, particle size of 0.30–0.60 mm, extraction time of 20 min, extraction solvent volume of 10 mL and extraction temperature of 60 °C. The applications showed remarkable improvements in terms of reduced extraction time, solvent consumption, extraction yield and the quality of extracts. The turmeric oleoresin was successfully solubilised in aqueous solution by forming inclusion complex with methyl-ß-cyclodextrin (Mß-CD). Phase solubility studies used curcumin as a marker compounds to represent turmeric oleoresin. In the presence of Mß-CD, the curcumin was enhanced. Result from characterisation of inclusion complexes with Fourier transform infrared (FTIR) spectrometry indicates that all the mixing methods were found to be suitable for encapsulation. However, scanning electron microscopy (SEM) shows a drastic change in particle sizes, indicating a formation of a new solid phase in kneading method, implying it as the best mixing method.
format	Article
author	Hadi, Binta Jume Sanagi, Mohd. Marsin Wan Ibrahim, W. A. Jamil, Shajarahtunnur AbdullahiMu’azu, Mohammed Aboul Enein, Hassan Y.
author_facet	Hadi, Binta Jume Sanagi, Mohd. Marsin Wan Ibrahim, W. A. Jamil, Shajarahtunnur AbdullahiMu’azu, Mohammed Aboul Enein, Hassan Y.
author_sort	Hadi, Binta Jume
title	Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin
title_short	Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin
title_full	Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin
title_fullStr	Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin
title_full_unstemmed	Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin
title_sort	ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin
publisher	Springer New York
publishDate	2015
url	http://eprints.utm.my/id/eprint/55952/ http://dx.doi.org/10.1007/s12161-014-0016-3
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score	13.211869

Ultrasonic-assisted extraction of curcumin complexed with methyl-beta-cyclodextrin

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