Fabrication of novel SnO2 nanofibers bundle and their optical properties

Here we report on the synthesis of novel SnO2 nanofibers bundle (NFB) by using ball milled Fe powders via chemical vapor deposition (CVD). The reaction was carried out in a horizontal tube furnace (HTF) at 1100 °C under Ar flow. The as prepared product was characterized by X-ray diffraction (XRD), s...

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Main Authors: Butt, Faheem K., Cao, Chuanbao, Khan, Waheed S., Ali, Zulfiqar, Mahmood, Tariq, Ahmed, Rashid, Hussain, Sajad, Nabi, Ghulam
Format: Article
Published: Elsevier 2012
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Online Access:http://eprints.utm.my/id/eprint/33536/
http://dx.doi.org/10.1016/j.matchemphys.2012.04.024
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spelling my.utm.335362018-11-30T06:37:31Z http://eprints.utm.my/id/eprint/33536/ Fabrication of novel SnO2 nanofibers bundle and their optical properties Butt, Faheem K. Cao, Chuanbao Khan, Waheed S. Ali, Zulfiqar Mahmood, Tariq Ahmed, Rashid Hussain, Sajad Nabi, Ghulam QC Physics Here we report on the synthesis of novel SnO2 nanofibers bundle (NFB) by using ball milled Fe powders via chemical vapor deposition (CVD). The reaction was carried out in a horizontal tube furnace (HTF) at 1100 °C under Ar flow. The as prepared product was characterized by X-ray diffraction (XRD), scanning electron microscopy, energy dispersive X-ray spectroscopy, transmission electron microscopy, high resolution transmission electron microscopy and selected area electron diffraction (SAED). The microscopy analysis reveals the existence of tubular structure that might be formed by the accumulation of nanofibers. The Raman spectrum reveals that the product is rutile SnO2 with additional peaks ascribed to defects or oxygen vacancies. Room temperature Photoluminescence (PL) spectrum exhibits three emission bands at 369, 450 and 466.6 nm. Using optical absorbance data, a direct optical bandgap of 3.68 eV was calculated. Elsevier 2012-09-14 Article PeerReviewed Butt, Faheem K. and Cao, Chuanbao and Khan, Waheed S. and Ali, Zulfiqar and Mahmood, Tariq and Ahmed, Rashid and Hussain, Sajad and Nabi, Ghulam (2012) Fabrication of novel SnO2 nanofibers bundle and their optical properties. Materials Chemistry and Physics, 136 (1). pp. 10-14. ISSN 0254-0584 http://dx.doi.org/10.1016/j.matchemphys.2012.04.024 DOI:10.1016/j.matchemphys.2012.04.024
institution Universiti Teknologi Malaysia
building UTM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Malaysia
content_source UTM Institutional Repository
url_provider http://eprints.utm.my/
topic QC Physics
spellingShingle QC Physics
Butt, Faheem K.
Cao, Chuanbao
Khan, Waheed S.
Ali, Zulfiqar
Mahmood, Tariq
Ahmed, Rashid
Hussain, Sajad
Nabi, Ghulam
Fabrication of novel SnO2 nanofibers bundle and their optical properties
description Here we report on the synthesis of novel SnO2 nanofibers bundle (NFB) by using ball milled Fe powders via chemical vapor deposition (CVD). The reaction was carried out in a horizontal tube furnace (HTF) at 1100 °C under Ar flow. The as prepared product was characterized by X-ray diffraction (XRD), scanning electron microscopy, energy dispersive X-ray spectroscopy, transmission electron microscopy, high resolution transmission electron microscopy and selected area electron diffraction (SAED). The microscopy analysis reveals the existence of tubular structure that might be formed by the accumulation of nanofibers. The Raman spectrum reveals that the product is rutile SnO2 with additional peaks ascribed to defects or oxygen vacancies. Room temperature Photoluminescence (PL) spectrum exhibits three emission bands at 369, 450 and 466.6 nm. Using optical absorbance data, a direct optical bandgap of 3.68 eV was calculated.
format Article
author Butt, Faheem K.
Cao, Chuanbao
Khan, Waheed S.
Ali, Zulfiqar
Mahmood, Tariq
Ahmed, Rashid
Hussain, Sajad
Nabi, Ghulam
author_facet Butt, Faheem K.
Cao, Chuanbao
Khan, Waheed S.
Ali, Zulfiqar
Mahmood, Tariq
Ahmed, Rashid
Hussain, Sajad
Nabi, Ghulam
author_sort Butt, Faheem K.
title Fabrication of novel SnO2 nanofibers bundle and their optical properties
title_short Fabrication of novel SnO2 nanofibers bundle and their optical properties
title_full Fabrication of novel SnO2 nanofibers bundle and their optical properties
title_fullStr Fabrication of novel SnO2 nanofibers bundle and their optical properties
title_full_unstemmed Fabrication of novel SnO2 nanofibers bundle and their optical properties
title_sort fabrication of novel sno2 nanofibers bundle and their optical properties
publisher Elsevier
publishDate 2012
url http://eprints.utm.my/id/eprint/33536/
http://dx.doi.org/10.1016/j.matchemphys.2012.04.024
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score 13.211869