Rapid synthesis of thermally stable hydroxyapaptite

We have optimized the wet precipitation synthesis of hydroxyapaptite to obtain thermally stable powder in the short time span of 3 min. Exposure of the reaction mixture to 1000 W microwave for 3 min furnished hydroxyapatite, which was thermally stable at temperatures up to 1200 °C. Powders were anal...

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Main Authors: Nazir, Rabia, Iqbal, Nida, Khan, Abdul S., Akram, Aftab, Asif, Anila, Chaudhry, Aqif A., Rehman, Ihtesham ur., Hussain, Rafaqat
Format: Article
Published: Elsevier Ltd. and Techna Group S.r.l. 2012
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Online Access:http://eprints.utm.my/id/eprint/29403/
http://dx.doi.org/10.1016/j.ceramint.2011.07.027
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spelling my.utm.294032019-03-26T08:07:25Z http://eprints.utm.my/id/eprint/29403/ Rapid synthesis of thermally stable hydroxyapaptite Nazir, Rabia Iqbal, Nida Khan, Abdul S. Akram, Aftab Asif, Anila Chaudhry, Aqif A. Rehman, Ihtesham ur. Hussain, Rafaqat QD Chemistry We have optimized the wet precipitation synthesis of hydroxyapaptite to obtain thermally stable powder in the short time span of 3 min. Exposure of the reaction mixture to 1000 W microwave for 3 min furnished hydroxyapatite, which was thermally stable at temperatures up to 1200 °C. Powders were analyzed for phase purity using X-ray crystallography; chemical composition was studied using Fourier transform infrared spectroscopy while particle morphology was analyzed using scanning electron microscopy. Elsevier Ltd. and Techna Group S.r.l. 2012-01 Article PeerReviewed Nazir, Rabia and Iqbal, Nida and Khan, Abdul S. and Akram, Aftab and Asif, Anila and Chaudhry, Aqif A. and Rehman, Ihtesham ur. and Hussain, Rafaqat (2012) Rapid synthesis of thermally stable hydroxyapaptite. Ceramics International, 38 (1). pp. 457-462. ISSN 0272-8842 http://dx.doi.org/10.1016/j.ceramint.2011.07.027 DOI:10.1016/j.ceramint.2011.07.027
institution Universiti Teknologi Malaysia
building UTM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Malaysia
content_source UTM Institutional Repository
url_provider http://eprints.utm.my/
topic QD Chemistry
spellingShingle QD Chemistry
Nazir, Rabia
Iqbal, Nida
Khan, Abdul S.
Akram, Aftab
Asif, Anila
Chaudhry, Aqif A.
Rehman, Ihtesham ur.
Hussain, Rafaqat
Rapid synthesis of thermally stable hydroxyapaptite
description We have optimized the wet precipitation synthesis of hydroxyapaptite to obtain thermally stable powder in the short time span of 3 min. Exposure of the reaction mixture to 1000 W microwave for 3 min furnished hydroxyapatite, which was thermally stable at temperatures up to 1200 °C. Powders were analyzed for phase purity using X-ray crystallography; chemical composition was studied using Fourier transform infrared spectroscopy while particle morphology was analyzed using scanning electron microscopy.
format Article
author Nazir, Rabia
Iqbal, Nida
Khan, Abdul S.
Akram, Aftab
Asif, Anila
Chaudhry, Aqif A.
Rehman, Ihtesham ur.
Hussain, Rafaqat
author_facet Nazir, Rabia
Iqbal, Nida
Khan, Abdul S.
Akram, Aftab
Asif, Anila
Chaudhry, Aqif A.
Rehman, Ihtesham ur.
Hussain, Rafaqat
author_sort Nazir, Rabia
title Rapid synthesis of thermally stable hydroxyapaptite
title_short Rapid synthesis of thermally stable hydroxyapaptite
title_full Rapid synthesis of thermally stable hydroxyapaptite
title_fullStr Rapid synthesis of thermally stable hydroxyapaptite
title_full_unstemmed Rapid synthesis of thermally stable hydroxyapaptite
title_sort rapid synthesis of thermally stable hydroxyapaptite
publisher Elsevier Ltd. and Techna Group S.r.l.
publishDate 2012
url http://eprints.utm.my/id/eprint/29403/
http://dx.doi.org/10.1016/j.ceramint.2011.07.027
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score 13.211869