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Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element

The isothermal oxidation of heat-treated Ni-based Fe–Ni–Cr superalloy at 500 ℃ was studied to further investigate the role and effect of Nb alloying element during oxide scale formation. The Ni-based Fe–Ni–Cr superalloys underwent a heat treatment process at two different temperatures, that are, 950...

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Main Authors: Parimin, Noraziana, Hamzah, Esah, Amrin, Astuty
Format: Conference or Workshop Item
Published: 2023
Subjects:
Q Science (General)
TJ Mechanical engineering and machinery
Online Access:http://eprints.utm.my/108448/
http://dx.doi.org/10.1007/978-981-19-9267-4_79
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spelling my.utm.1084482024-11-05T06:19:42Z http://eprints.utm.my/108448/ Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element Parimin, Noraziana Hamzah, Esah Amrin, Astuty Q Science (General) TJ Mechanical engineering and machinery The isothermal oxidation of heat-treated Ni-based Fe–Ni–Cr superalloy at 500 ℃ was studied to further investigate the role and effect of Nb alloying element during oxide scale formation. The Ni-based Fe–Ni–Cr superalloys underwent a heat treatment process at two different temperatures, that are, 950 ℃ and 1100 ℃, for 3 h of soaking time, followed by water quenching. Heat-treated sample at 950 ℃ exhibited fine grain size, while heat-treated sample at 1100 ℃ exhibited coarse grain size. The heat-treated Ni-based Fe–Ni–Cr superalloys were subjected to an isothermal oxidation test at 500 ℃ for 500 h exposure. The oxidized heat-treated Ni-based Fe–Ni–Cr superalloys were analyzed in terms of oxidation kinetic, oxide phase formation and oxide surface morphology. The oxide phases were analyzed by using XRD technique. The surface morphology was examined by using SEM, FESEM and EDX techniques. Both oxidized heat-treated Ni-based Fe–Ni–Cr superalloys’ samples followed a parabolic rate law, indicating a diffusion-controlled oxide growth mechanism. Several oxide phases were formed on the alloy surface after exposures at 500 h. The surface morphology of oxidized samples at 300 h exhibited the formation of continuous oxide scale with distributed overgrown Nb-rich oxides. Nb-rich oxides were formed on coarse-grained heat-treated alloys that developed excessively large Nb-rich oxides. This phenomenon will initiate a crack that propagates around the oxide. 2023 Conference or Workshop Item PeerReviewed Parimin, Noraziana and Hamzah, Esah and Amrin, Astuty (2023) Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element. In: Green Materials and Electronic Packaging Interconnect Technology Symposium, EPITS 2022, 14 September 2022 - 15 September 2022, Langkawi, Kedah, Malaysia. http://dx.doi.org/10.1007/978-981-19-9267-4_79
institution Universiti Teknologi Malaysia
building UTM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Malaysia
content_source UTM Institutional Repository
url_provider http://eprints.utm.my/
topic Q Science (General)
TJ Mechanical engineering and machinery
spellingShingle Q Science (General)
TJ Mechanical engineering and machinery
Parimin, Noraziana
Hamzah, Esah
Amrin, Astuty
Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element
description The isothermal oxidation of heat-treated Ni-based Fe–Ni–Cr superalloy at 500 ℃ was studied to further investigate the role and effect of Nb alloying element during oxide scale formation. The Ni-based Fe–Ni–Cr superalloys underwent a heat treatment process at two different temperatures, that are, 950 ℃ and 1100 ℃, for 3 h of soaking time, followed by water quenching. Heat-treated sample at 950 ℃ exhibited fine grain size, while heat-treated sample at 1100 ℃ exhibited coarse grain size. The heat-treated Ni-based Fe–Ni–Cr superalloys were subjected to an isothermal oxidation test at 500 ℃ for 500 h exposure. The oxidized heat-treated Ni-based Fe–Ni–Cr superalloys were analyzed in terms of oxidation kinetic, oxide phase formation and oxide surface morphology. The oxide phases were analyzed by using XRD technique. The surface morphology was examined by using SEM, FESEM and EDX techniques. Both oxidized heat-treated Ni-based Fe–Ni–Cr superalloys’ samples followed a parabolic rate law, indicating a diffusion-controlled oxide growth mechanism. Several oxide phases were formed on the alloy surface after exposures at 500 h. The surface morphology of oxidized samples at 300 h exhibited the formation of continuous oxide scale with distributed overgrown Nb-rich oxides. Nb-rich oxides were formed on coarse-grained heat-treated alloys that developed excessively large Nb-rich oxides. This phenomenon will initiate a crack that propagates around the oxide.
format Conference or Workshop Item
author Parimin, Noraziana
Hamzah, Esah
Amrin, Astuty
author_facet Parimin, Noraziana
Hamzah, Esah
Amrin, Astuty
author_sort Parimin, Noraziana
title Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element
title_short Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element
title_full Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element
title_fullStr Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element
title_full_unstemmed Isothermal oxidation behavior of Ni-based Fe–Ni–Cr superalloys: role and effect of Nb alloying element
title_sort isothermal oxidation behavior of ni-based fe–ni–cr superalloys: role and effect of nb alloying element
publishDate 2023
url http://eprints.utm.my/108448/
http://dx.doi.org/10.1007/978-981-19-9267-4_79
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score 13.211869

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