Synthesis And Characterization Of Hematite Nanoparticles As Active Photocatalyst For Water Splitting Application

This paper highlights on the hydrogen production through photocatalytic activity by using hematite nanoparticles synthesized from self-combustion method based on different stirring period.The morphologies and microstructures of the nanostructures were determined using Field-Emission Scanning Electro...

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Bibliographic Details
Main Authors: Chin, Sze Mei, Sufian, Suriati, Abd Razak, Jeefferie
Format: Article
Language:English
Published: Trans Tech Publications, Switzerland 2014
Online Access:http://eprints.utem.edu.my/id/eprint/21050/2/Synthesis_and_Characterization_of_Hematite_Nanoparticles_as_Active_Photocatalyst_for_Water_Splitting_Application.pdf
http://eprints.utem.edu.my/id/eprint/21050/
https://www.scientific.net/KEM.594-595.73
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Summary:This paper highlights on the hydrogen production through photocatalytic activity by using hematite nanoparticles synthesized from self-combustion method based on different stirring period.The morphologies and microstructures of the nanostructures were determined using Field-Emission Scanning Electron Microscope (FESEM),X-Ray Diffractometer (XRD) and Particle Size Analyser (PSA).Besides that,surface area analyser was used to determine the BET surface area of the hematite samples.The hematite nanocatalyst as-synthesized are proven to be rhombohedral crystalline hematite (α-Fe2O3) with particle diameters ranging from 60-140 nm.The BET specific surface area of hematite samples increased from 5.437 to 7.6425 m2/g with increasing stirring period from 1 to 4 weeks.This caused the amount of hydrogen gas produced from photocatalytic water splitting to increase as well.