Staff View: Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System

Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System

Lead zirconate titanate (PZT) is a piezoelectric material which is most widely used in ceramics. La3+ and Sr2+ co-doped PZT (PLSZT) shows the improvement in piezoelectric and dielectric properties which were piezoelectric coefficient (d33), electromechanical coupling factor (kp) and dielectric permi...

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Main Author:	Rashid, Tuan Nur Izzah Tuan Ab
Format:	Thesis
Language:	English
Published:	2018
Subjects:	T Technology TA401-492 Materials of engineering and construction. Mechanics of materials
Online Access:	http://eprints.usm.my/46677/1/Effect%20Of%20Ca%20Addition%20On%20Piezoelectric%20And%20Dielectric%20Properties%20In%20b0.93la0.02sr0.05%28Zr0.52ti0.48%29O3%20%28Plszt%29%20System.pdf http://eprints.usm.my/46677/
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spelling	my.usm.eprints.46677 http://eprints.usm.my/46677/ Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System Rashid, Tuan Nur Izzah Tuan Ab T Technology TA401-492 Materials of engineering and construction. Mechanics of materials Lead zirconate titanate (PZT) is a piezoelectric material which is most widely used in ceramics. La3+ and Sr2+ co-doped PZT (PLSZT) shows the improvement in piezoelectric and dielectric properties which were piezoelectric coefficient (d33), electromechanical coupling factor (kp) and dielectric permittivity (ɛᵣ). However, the d33 and kp still indicated a lower value for electronic device applications. In order to improve d33 and kp, the doping process and poling behaviour were investigated. In this research, Pb0.93La0.02Sr0.05(Zr0.52Ti0.48)O3 (PLSZT) ceramic was synthesized by high energy planetary ball milling for 40 hours and sintered at 1200 °C for 3 hours. The poling parameters (temperature, electric field and time) were studied based on design of experiment (DOE) in order to investigate the effect of poling parameter towards the piezoelectric and dielectric properties for PLSZT. Besides, a new dopant (CaCO3) for PLSZT was studied followed by sintering parameters (1100 °C to 1300 °C for 2 to 4 hours) for further improving their piezoelectric and dielectric properties. The optimum poling parameter shows a good d33 and ɛᵣ which were 320 pC/N and 1660, respectively. Poling parameters were optimized at T = 140 °C, Ef = 4 kV/mm and t = 20 min. Ca2+ doped PLSZT (PCLSZT) show that enhancement of d33, kp and ɛᵣ occurred at lower Ca addition. Optimum piezoelectric and dielectric properties were obtained at 0.005 mol% CaCO3 (PCLSZT0.005) sintered at 1200 °C for 3 hours with d33 = 430 pC/N, kp = 0.5866, ɛᵣ = 2450 and tan δ = 0.0426. In conclusion the addition of Ca2+ successfully increased the piezoelectric and dielectric properties of PLSZT. 2018-04-01 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/46677/1/Effect%20Of%20Ca%20Addition%20On%20Piezoelectric%20And%20Dielectric%20Properties%20In%20b0.93la0.02sr0.05%28Zr0.52ti0.48%29O3%20%28Plszt%29%20System.pdf Rashid, Tuan Nur Izzah Tuan Ab (2018) Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System. Masters thesis, Universiti Sains Malaysia.
institution	Universiti Sains Malaysia
building	Hamzah Sendut Library
collection	Institutional Repository
continent	Asia
country	Malaysia
content_provider	Universiti Sains Malaysia
content_source	USM Institutional Repository
url_provider	http://eprints.usm.my/
language	English
topic	T Technology TA401-492 Materials of engineering and construction. Mechanics of materials
spellingShingle	T Technology TA401-492 Materials of engineering and construction. Mechanics of materials Rashid, Tuan Nur Izzah Tuan Ab Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System
description	Lead zirconate titanate (PZT) is a piezoelectric material which is most widely used in ceramics. La3+ and Sr2+ co-doped PZT (PLSZT) shows the improvement in piezoelectric and dielectric properties which were piezoelectric coefficient (d33), electromechanical coupling factor (kp) and dielectric permittivity (ɛᵣ). However, the d33 and kp still indicated a lower value for electronic device applications. In order to improve d33 and kp, the doping process and poling behaviour were investigated. In this research, Pb0.93La0.02Sr0.05(Zr0.52Ti0.48)O3 (PLSZT) ceramic was synthesized by high energy planetary ball milling for 40 hours and sintered at 1200 °C for 3 hours. The poling parameters (temperature, electric field and time) were studied based on design of experiment (DOE) in order to investigate the effect of poling parameter towards the piezoelectric and dielectric properties for PLSZT. Besides, a new dopant (CaCO3) for PLSZT was studied followed by sintering parameters (1100 °C to 1300 °C for 2 to 4 hours) for further improving their piezoelectric and dielectric properties. The optimum poling parameter shows a good d33 and ɛᵣ which were 320 pC/N and 1660, respectively. Poling parameters were optimized at T = 140 °C, Ef = 4 kV/mm and t = 20 min. Ca2+ doped PLSZT (PCLSZT) show that enhancement of d33, kp and ɛᵣ occurred at lower Ca addition. Optimum piezoelectric and dielectric properties were obtained at 0.005 mol% CaCO3 (PCLSZT0.005) sintered at 1200 °C for 3 hours with d33 = 430 pC/N, kp = 0.5866, ɛᵣ = 2450 and tan δ = 0.0426. In conclusion the addition of Ca2+ successfully increased the piezoelectric and dielectric properties of PLSZT.
format	Thesis
author	Rashid, Tuan Nur Izzah Tuan Ab
author_facet	Rashid, Tuan Nur Izzah Tuan Ab
author_sort	Rashid, Tuan Nur Izzah Tuan Ab
title	Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System
title_short	Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System
title_full	Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System
title_fullStr	Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System
title_full_unstemmed	Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System
title_sort	effect of ca addition on piezoelectric and dielectric properties in b0.93la0.02sr0.05(zr0.52ti0.48)o3 (plszt) system
publishDate	2018
url	http://eprints.usm.my/46677/1/Effect%20Of%20Ca%20Addition%20On%20Piezoelectric%20And%20Dielectric%20Properties%20In%20b0.93la0.02sr0.05%28Zr0.52ti0.48%29O3%20%28Plszt%29%20System.pdf http://eprints.usm.my/46677/
_version_	1717094467017637888
score	13.211869

Effect Of Ca Addition On Piezoelectric And Dielectric Properties In b0.93la0.02sr0.05(Zr0.52ti0.48)O3 (Plszt) System

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