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Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method

Black tilapia (Oreochromis mossambicus) fish scales were used as a source of natural hydroxyapatite (HAp) since it is cheaper than synthetic hydroxyapatite and safer than animal origin such as bones. This study investigates the preparation of natural hydroxyapatite from tilapia fish scales (FsHAp) b...

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Main Authors: Mohd Ismail, Izyan Khairani, Jaafar, Che Nor Aiza, Zainol, Ismail, Mohamed Yusoff, Mohd Zuhri
Format: Article
Language:English
Published: Universiti Putra Malaysia 2019
Online Access:http://psasir.upm.edu.my/id/eprint/81812/1/Preparation%20and%20characterization%20of%20hydroxyapatite%20from%20black%20tilapia%20fish%20scales%20using%20spray-drying%20method.pdf
http://psasir.upm.edu.my/id/eprint/81812/
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spelling my.upm.eprints.818122020-09-02T08:11:50Z http://psasir.upm.edu.my/id/eprint/81812/ Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method Mohd Ismail, Izyan Khairani Jaafar, Che Nor Aiza Zainol, Ismail Mohamed Yusoff, Mohd Zuhri Black tilapia (Oreochromis mossambicus) fish scales were used as a source of natural hydroxyapatite (HAp) since it is cheaper than synthetic hydroxyapatite and safer than animal origin such as bones. This study investigates the preparation of natural hydroxyapatite from tilapia fish scales (FsHAp) by thermal technique followed by ball milling and spray dried to produce FsHAp powder. The effect of milling time on the particles size of FsHAp was investigated. In this study, Mastersizer 2000 was applied to measure the particles size of FsHAp. Field emission scanning electron microscope (FESEM) was used to investigate the morphology of the FsHAp powders whereas x-ray diffraction (XRD) and Fourier transform infrared (FTIR) were used to verify the presence of FsHAp. From the experimental results, it was found that the optimum milling time is 48 hours which produced smallest particles of FsHAp at about 1.86 µm. The spray-drying method produced different sizes of FsHAp ranging from 2.18 micron to 6.36 µm. The FESEM analysis revealed that the FsHAp particles agglomerated in the spray dryer. FTIR and XRD analyses have showed the prominent peaks corresponding to high quality of FsHAp from fish scales. Universiti Putra Malaysia 2019 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/81812/1/Preparation%20and%20characterization%20of%20hydroxyapatite%20from%20black%20tilapia%20fish%20scales%20using%20spray-drying%20method.pdf Mohd Ismail, Izyan Khairani and Jaafar, Che Nor Aiza and Zainol, Ismail and Mohamed Yusoff, Mohd Zuhri (2019) Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method. Malaysian Journal of Microscopy, 15. pp. 155-163. ISSN 1823-7010; ESSN: 2600-7444
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
language English
description Black tilapia (Oreochromis mossambicus) fish scales were used as a source of natural hydroxyapatite (HAp) since it is cheaper than synthetic hydroxyapatite and safer than animal origin such as bones. This study investigates the preparation of natural hydroxyapatite from tilapia fish scales (FsHAp) by thermal technique followed by ball milling and spray dried to produce FsHAp powder. The effect of milling time on the particles size of FsHAp was investigated. In this study, Mastersizer 2000 was applied to measure the particles size of FsHAp. Field emission scanning electron microscope (FESEM) was used to investigate the morphology of the FsHAp powders whereas x-ray diffraction (XRD) and Fourier transform infrared (FTIR) were used to verify the presence of FsHAp. From the experimental results, it was found that the optimum milling time is 48 hours which produced smallest particles of FsHAp at about 1.86 µm. The spray-drying method produced different sizes of FsHAp ranging from 2.18 micron to 6.36 µm. The FESEM analysis revealed that the FsHAp particles agglomerated in the spray dryer. FTIR and XRD analyses have showed the prominent peaks corresponding to high quality of FsHAp from fish scales.
format Article
author Mohd Ismail, Izyan Khairani
Jaafar, Che Nor Aiza
Zainol, Ismail
Mohamed Yusoff, Mohd Zuhri
spellingShingle Mohd Ismail, Izyan Khairani
Jaafar, Che Nor Aiza
Zainol, Ismail
Mohamed Yusoff, Mohd Zuhri
Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method
author_facet Mohd Ismail, Izyan Khairani
Jaafar, Che Nor Aiza
Zainol, Ismail
Mohamed Yusoff, Mohd Zuhri
author_sort Mohd Ismail, Izyan Khairani
title Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method
title_short Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method
title_full Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method
title_fullStr Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method
title_full_unstemmed Preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method
title_sort preparation and characterization of hydroxyapatite from black tilapia fish scales using spray-drying method
publisher Universiti Putra Malaysia
publishDate 2019
url http://psasir.upm.edu.my/id/eprint/81812/1/Preparation%20and%20characterization%20of%20hydroxyapatite%20from%20black%20tilapia%20fish%20scales%20using%20spray-drying%20method.pdf
http://psasir.upm.edu.my/id/eprint/81812/
_version_ 1677783013090394112
score 13.211869

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