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Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method

The intercalation of chloroacetic acid (CAA) into the interlayer gallery of zinc layered hydroxide has been achieved via a facile direct reaction method. The nanohybrid synthesised, zinc layered hydroxide-chloroacetate was characterised using Powder X-ray diffraction patterns (PXRD), which demonstra...

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Main Authors: Hashim, Norhayati, Muda, Zuhailimuna, Mohd Sharif, Sharifah Norain, Md Isa, Illyas, Mohd Ali, Noorshida, Ghazuli, Mohammad Rafaei, Hussein, Mohd Zobir
Format: Article
Language:English
Published: Taylor & Francis 2016
Online Access:http://psasir.upm.edu.my/id/eprint/62831/1/Preparation%20of%20zinc%20layered%20.pdf
http://psasir.upm.edu.my/id/eprint/62831/
https://www.tandfonline.com/doi/full/10.1080/14328917.2016.1265248
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spelling my.upm.eprints.628312022-11-10T04:04:54Z http://psasir.upm.edu.my/id/eprint/62831/ Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method Hashim, Norhayati Muda, Zuhailimuna Mohd Sharif, Sharifah Norain Md Isa, Illyas Mohd Ali, Noorshida Ghazuli, Mohammad Rafaei Hussein, Mohd Zobir The intercalation of chloroacetic acid (CAA) into the interlayer gallery of zinc layered hydroxide has been achieved via a facile direct reaction method. The nanohybrid synthesised, zinc layered hydroxide-chloroacetate was characterised using Powder X-ray diffraction patterns (PXRD), which demonstrated the progressive evolution of the nanohybrid structure, as the CAA molarity were increased from 0.05 to 0.3 M. Sharp and symmetrical peaks of 0.3 M CAA were observed in the PXRD pattern. The emergence of intercalation peak, with basal spacing of 14.3 Å signifying the success intercalation of chloroacetate anions into the interlayer space of the host. The intercalation was also validated by FTIR spectroscopy and CHNS elemental analyser. The increased thermal stability of zinc layered hydroxide-chloroacetate nanohybrid was confirmed by thermogravimetric analysis. Taylor & Francis 2016-12 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/62831/1/Preparation%20of%20zinc%20layered%20.pdf Hashim, Norhayati and Muda, Zuhailimuna and Mohd Sharif, Sharifah Norain and Md Isa, Illyas and Mohd Ali, Noorshida and Ghazuli, Mohammad Rafaei and Hussein, Mohd Zobir (2016) Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method. Materials Research Innovations, 21 (6). 396 - 400. ISSN 1433-075X https://www.tandfonline.com/doi/full/10.1080/14328917.2016.1265248 10.1080/14328917.2016.1265248
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
language English
description The intercalation of chloroacetic acid (CAA) into the interlayer gallery of zinc layered hydroxide has been achieved via a facile direct reaction method. The nanohybrid synthesised, zinc layered hydroxide-chloroacetate was characterised using Powder X-ray diffraction patterns (PXRD), which demonstrated the progressive evolution of the nanohybrid structure, as the CAA molarity were increased from 0.05 to 0.3 M. Sharp and symmetrical peaks of 0.3 M CAA were observed in the PXRD pattern. The emergence of intercalation peak, with basal spacing of 14.3 Å signifying the success intercalation of chloroacetate anions into the interlayer space of the host. The intercalation was also validated by FTIR spectroscopy and CHNS elemental analyser. The increased thermal stability of zinc layered hydroxide-chloroacetate nanohybrid was confirmed by thermogravimetric analysis.
format Article
author Hashim, Norhayati
Muda, Zuhailimuna
Mohd Sharif, Sharifah Norain
Md Isa, Illyas
Mohd Ali, Noorshida
Ghazuli, Mohammad Rafaei
Hussein, Mohd Zobir
spellingShingle Hashim, Norhayati
Muda, Zuhailimuna
Mohd Sharif, Sharifah Norain
Md Isa, Illyas
Mohd Ali, Noorshida
Ghazuli, Mohammad Rafaei
Hussein, Mohd Zobir
Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method
author_facet Hashim, Norhayati
Muda, Zuhailimuna
Mohd Sharif, Sharifah Norain
Md Isa, Illyas
Mohd Ali, Noorshida
Ghazuli, Mohammad Rafaei
Hussein, Mohd Zobir
author_sort Hashim, Norhayati
title Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method
title_short Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method
title_full Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method
title_fullStr Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method
title_full_unstemmed Preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method
title_sort preparation of zinc layered hydroxide–chloroacetate nanohybrid using direct reaction method
publisher Taylor & Francis
publishDate 2016
url http://psasir.upm.edu.my/id/eprint/62831/1/Preparation%20of%20zinc%20layered%20.pdf
http://psasir.upm.edu.my/id/eprint/62831/
https://www.tandfonline.com/doi/full/10.1080/14328917.2016.1265248
_version_ 1751538185473622016
score 13.211869

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