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Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate

The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6...

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Main Authors: M. Osman, Uwaisulqarni, Mohamed Tahir, Mohamed Ibrahim, Crouse, Karen Anne, Ravoof, Thahira Begum S. A.
Format: Article
Language:English
Published: Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry 2017
Online Access:http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf
http://psasir.upm.edu.my/id/eprint/61263/
https://www.jstage.jst.go.jp/article/xraystruct/33/0/33_57/_article
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spelling my.upm.eprints.612632022-03-04T07:52:21Z http://psasir.upm.edu.my/id/eprint/61263/ Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate M. Osman, Uwaisulqarni Mohamed Tahir, Mohamed Ibrahim Crouse, Karen Anne Ravoof, Thahira Begum S. A. The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6)Å3. The compound was nearly planar with intermolecular N–H···S hydrogen bonding observed in the crystal lattice. Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry 2017 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf M. Osman, Uwaisulqarni and Mohamed Tahir, Mohamed Ibrahim and Crouse, Karen Anne and Ravoof, Thahira Begum S. A. (2017) Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate. X-ray Structure Analysis Online, 33 (9). 57 - 58. ISSN 1883-3578 (Unpublished) https://www.jstage.jst.go.jp/article/xraystruct/33/0/33_57/_article 10.2116/xraystruct.33.57
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
language English
description The title compound, C9H12N2S3, was obtained from a condensation reaction between S-methyldithiocarbazate and 1-(2-thienyl)-1-propane. The compound crystallized in the monoclinic space group P21/n with cell parameters a = 10.178(3), b = 13.357(4), c = 8.845(3)Å, β =98.613(5)°, Z = 4 and V = 1188.9(6)Å3. The compound was nearly planar with intermolecular N–H···S hydrogen bonding observed in the crystal lattice.
format Article
author M. Osman, Uwaisulqarni
Mohamed Tahir, Mohamed Ibrahim
Crouse, Karen Anne
Ravoof, Thahira Begum S. A.
spellingShingle M. Osman, Uwaisulqarni
Mohamed Tahir, Mohamed Ibrahim
Crouse, Karen Anne
Ravoof, Thahira Begum S. A.
Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
author_facet M. Osman, Uwaisulqarni
Mohamed Tahir, Mohamed Ibrahim
Crouse, Karen Anne
Ravoof, Thahira Begum S. A.
author_sort M. Osman, Uwaisulqarni
title Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
title_short Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
title_full Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
title_fullStr Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
title_full_unstemmed Crystal structure of methyl-N′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
title_sort crystal structure of methyl-n′-[1-(thiophen-2-yl) propylidene] hydrazinecarbodithioate
publisher Nihon Bunseki Kagakkai, Japan Society for Analytical Chemistry
publishDate 2017
url http://psasir.upm.edu.my/id/eprint/61263/1/Crystal%20structure%20of%20methyl-N%E2%80%B2-%5B1-%28thiophen-2-yl%29%20propylidene%5D%20hydrazinecarbodithioate.pdf
http://psasir.upm.edu.my/id/eprint/61263/
https://www.jstage.jst.go.jp/article/xraystruct/33/0/33_57/_article
_version_ 1726793250612707328
score 13.211869

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