Micro-extraction of xenobiotics and biomolecules from different matrices on nanostructures

Sample preparation is the backbone of any analytical procedure; it involves extraction and pre-concentration of the desired analytes; often at trace levels. The present article describes the applications of nanomaterials (carbon-based inorganic and polymeric materials) in miniaturized extraction suc...

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Bibliographic Details
Main Authors: Sanagi, Mohd Marsin, Hussain, Iqbal, Wan Ibrahim, Wan Aini, Yahaya, Noorfatimah, Kamaruzaman, Sazlinda, Zainal Abidin, Nurul Nabilah, Ali, Imran
Format: Article
Language:English
Published: Taylor & Francis 2016
Online Access:http://psasir.upm.edu.my/id/eprint/53278/1/Micro-extraction%20of%20xenobiotics%20and%20biomolecules%20from%20different%20matrices%20on%20nanostructures.pdf
http://psasir.upm.edu.my/id/eprint/53278/
https://www.tandfonline.com/doi/abs/10.1080/15422119.2014.973507
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Summary:Sample preparation is the backbone of any analytical procedure; it involves extraction and pre-concentration of the desired analytes; often at trace levels. The present article describes the applications of nanomaterials (carbon-based inorganic and polymeric materials) in miniaturized extraction such as solid phase micro-extraction, stir-bar sorptive extraction, liquid phase micro-extraction, and dispersive liquid phase micro-extraction in the analyses of aqueous samples. The nanoparticles used for micro-extractions are discussed on the basis of their chemical natures. The synthetic route and the preparation of nanomaterials are described along with the optimization strategies for micro-extraction. A comparison between the conventional materials and nanomaterials for micro-extraction is proposed. The key roles of the nanomaterials for the micro-extraction of different analytes such as drugs, pesticides, polycyclic aromatic hydrocarbons, proteins and peptides from aqueous samples are reported. The use of nanomaterials, combined with miniaturized micro-extraction techniques, proved to be highly promising for sample preparation of various matrices with analytes at trace levels.