Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying

Steel waste product had been used as the main source of raw material in the preparation of permanent magnets ferrites. Steel waste product is an impure material that contains the iron oxide and impurities. The steel waste product is a form of flakes is grinding for several hours to form a fine powde...

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Main Authors: Daud, Noruzaman, Azis, Rabaah Syahidah, Hashim, Mansor, Matori, Khamirul Amin, Hassan, Jumiah, Mohd. Saiden, Norlaily, Mohd Shahrani, Nuraine Mariana
Format: Article
Language:English
Published: Trans Tech Publications 2015
Online Access:http://psasir.upm.edu.my/id/eprint/45961/1/Preparation%20and%20characterization%20of%20Sr1%E2%88%92xNdxFe12O19%20derived%20from%20steel-waste%20product%20via%20mechanical%20alloying.pdf
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spelling my.upm.eprints.459612018-05-15T01:38:15Z http://psasir.upm.edu.my/id/eprint/45961/ Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying Daud, Noruzaman Azis, Rabaah Syahidah Hashim, Mansor Matori, Khamirul Amin Hassan, Jumiah Mohd. Saiden, Norlaily Mohd Shahrani, Nuraine Mariana Steel waste product had been used as the main source of raw material in the preparation of permanent magnets ferrites. Steel waste product is an impure material that contains the iron oxide and impurities. The steel waste product is a form of flakes is grinding for several hours to form a fine powder. The iron oxide powder is separated from magnetic and non-magnetic particle using magnetic particle separation. The magnetic particle was again been purified by using the Curie temperature separation technique. The magnetic powder was carried out from the purification and oxidize at 500 °C for 6 hours at 2 °C/ mins to form the hematite, Fe2O3, used as a raw powder to prepare SrFe12O19. Microstructure of Nd-doped strontium ferrites, Sr1-xNdxFe12O19, with x = 0.0, 0.1, 0.2, 0.3, 0.4 and 0.5, were prepared through a mechanical alloying technique. Several characterizations have been done, such as X-ray Diffraction (XRD) and Field emission scanning electron microscopy (FESEM). The magnetic properties of coercivity (Hc) and the energy product BHmax of samples are carried out. The magnetic properties of samples were investigated with an expectation of enhancing the magnetic properties by substitutions of Nd3+ ions on Fe3+ ion basis sites. The saturation magnetization Ms revealed magnetic behavior with respect to Nd3+ doping concentration, showing a decrease. The coercivity Hc increased with increasing Nd3+ doping concentration. Trans Tech Publications 2015 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/45961/1/Preparation%20and%20characterization%20of%20Sr1%E2%88%92xNdxFe12O19%20derived%20from%20steel-waste%20product%20via%20mechanical%20alloying.pdf Daud, Noruzaman and Azis, Rabaah Syahidah and Hashim, Mansor and Matori, Khamirul Amin and Hassan, Jumiah and Mohd. Saiden, Norlaily and Mohd Shahrani, Nuraine Mariana (2015) Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying. Materials Science Forum, 846. pp. 403-409. ISSN 0255-5476; ESSN: 1662-9752 10.4028/www.scientific.net/MSF.846.403
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
language English
description Steel waste product had been used as the main source of raw material in the preparation of permanent magnets ferrites. Steel waste product is an impure material that contains the iron oxide and impurities. The steel waste product is a form of flakes is grinding for several hours to form a fine powder. The iron oxide powder is separated from magnetic and non-magnetic particle using magnetic particle separation. The magnetic particle was again been purified by using the Curie temperature separation technique. The magnetic powder was carried out from the purification and oxidize at 500 °C for 6 hours at 2 °C/ mins to form the hematite, Fe2O3, used as a raw powder to prepare SrFe12O19. Microstructure of Nd-doped strontium ferrites, Sr1-xNdxFe12O19, with x = 0.0, 0.1, 0.2, 0.3, 0.4 and 0.5, were prepared through a mechanical alloying technique. Several characterizations have been done, such as X-ray Diffraction (XRD) and Field emission scanning electron microscopy (FESEM). The magnetic properties of coercivity (Hc) and the energy product BHmax of samples are carried out. The magnetic properties of samples were investigated with an expectation of enhancing the magnetic properties by substitutions of Nd3+ ions on Fe3+ ion basis sites. The saturation magnetization Ms revealed magnetic behavior with respect to Nd3+ doping concentration, showing a decrease. The coercivity Hc increased with increasing Nd3+ doping concentration.
format Article
author Daud, Noruzaman
Azis, Rabaah Syahidah
Hashim, Mansor
Matori, Khamirul Amin
Hassan, Jumiah
Mohd. Saiden, Norlaily
Mohd Shahrani, Nuraine Mariana
spellingShingle Daud, Noruzaman
Azis, Rabaah Syahidah
Hashim, Mansor
Matori, Khamirul Amin
Hassan, Jumiah
Mohd. Saiden, Norlaily
Mohd Shahrani, Nuraine Mariana
Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying
author_facet Daud, Noruzaman
Azis, Rabaah Syahidah
Hashim, Mansor
Matori, Khamirul Amin
Hassan, Jumiah
Mohd. Saiden, Norlaily
Mohd Shahrani, Nuraine Mariana
author_sort Daud, Noruzaman
title Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying
title_short Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying
title_full Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying
title_fullStr Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying
title_full_unstemmed Preparation and characterization of Sr1−xNdxFe12O19 derived from steel-waste product via mechanical alloying
title_sort preparation and characterization of sr1−xndxfe12o19 derived from steel-waste product via mechanical alloying
publisher Trans Tech Publications
publishDate 2015
url http://psasir.upm.edu.my/id/eprint/45961/1/Preparation%20and%20characterization%20of%20Sr1%E2%88%92xNdxFe12O19%20derived%20from%20steel-waste%20product%20via%20mechanical%20alloying.pdf
http://psasir.upm.edu.my/id/eprint/45961/
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