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Synthesis of palm oil-based fatty methylhydrazide

Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy and 1H...

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Main Authors: Al-Mulla, Emad A. Jaffar, Ibrahim, Nor Azowa, Al-Karkhi, Isam Hussain T., Shameli, Kamyar, Zidan, Mohammed, Ahmad, Mansor, Wan Yunus, Wan Md. Zin
Format: Article
Language:English
Published: Springer Netherlands 2013
Online Access:http://psasir.upm.edu.my/id/eprint/30010/1/Synthesis%20of%20palm%20oil.pdf
http://psasir.upm.edu.my/id/eprint/30010/
http://dx.doi.org/10.1007/s11164-012-0745-0
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spelling my.upm.eprints.300102016-02-12T07:21:49Z http://psasir.upm.edu.my/id/eprint/30010/ Synthesis of palm oil-based fatty methylhydrazide Al-Mulla, Emad A. Jaffar Ibrahim, Nor Azowa Al-Karkhi, Isam Hussain T. Shameli, Kamyar Zidan, Mohammed Ahmad, Mansor Wan Yunus, Wan Md. Zin Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy and 1H nuclear magnetic resonance technique. The results showed that a 6:1 molar ratio of palm oil to methylhydrazine, a round 78 % maximum conversion of palm oil into FMHs and a 10 h reaction time are the optimum reaction conditions. Springer Netherlands 2013-05-05 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/30010/1/Synthesis%20of%20palm%20oil.pdf Al-Mulla, Emad A. Jaffar and Ibrahim, Nor Azowa and Al-Karkhi, Isam Hussain T. and Shameli, Kamyar and Zidan, Mohammed and Ahmad, Mansor and Wan Yunus, Wan Md. Zin (2013) Synthesis of palm oil-based fatty methylhydrazide. Research on Chemical Intermediates, 39 (5). pp. 2133-2139. ISSN 0922-6168; ESSN: 1568-5675 http://dx.doi.org/10.1007/s11164-012-0745-0 10.1007/s11164-012-0745-0
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
language English
description Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy and 1H nuclear magnetic resonance technique. The results showed that a 6:1 molar ratio of palm oil to methylhydrazine, a round 78 % maximum conversion of palm oil into FMHs and a 10 h reaction time are the optimum reaction conditions.
format Article
author Al-Mulla, Emad A. Jaffar
Ibrahim, Nor Azowa
Al-Karkhi, Isam Hussain T.
Shameli, Kamyar
Zidan, Mohammed
Ahmad, Mansor
Wan Yunus, Wan Md. Zin
spellingShingle Al-Mulla, Emad A. Jaffar
Ibrahim, Nor Azowa
Al-Karkhi, Isam Hussain T.
Shameli, Kamyar
Zidan, Mohammed
Ahmad, Mansor
Wan Yunus, Wan Md. Zin
Synthesis of palm oil-based fatty methylhydrazide
author_facet Al-Mulla, Emad A. Jaffar
Ibrahim, Nor Azowa
Al-Karkhi, Isam Hussain T.
Shameli, Kamyar
Zidan, Mohammed
Ahmad, Mansor
Wan Yunus, Wan Md. Zin
author_sort Al-Mulla, Emad A. Jaffar
title Synthesis of palm oil-based fatty methylhydrazide
title_short Synthesis of palm oil-based fatty methylhydrazide
title_full Synthesis of palm oil-based fatty methylhydrazide
title_fullStr Synthesis of palm oil-based fatty methylhydrazide
title_full_unstemmed Synthesis of palm oil-based fatty methylhydrazide
title_sort synthesis of palm oil-based fatty methylhydrazide
publisher Springer Netherlands
publishDate 2013
url http://psasir.upm.edu.my/id/eprint/30010/1/Synthesis%20of%20palm%20oil.pdf
http://psasir.upm.edu.my/id/eprint/30010/
http://dx.doi.org/10.1007/s11164-012-0745-0
_version_ 1643829929993830400
score 13.211869

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