Synthesis of N-methoxy-N-methylaminocarbonyl-l, 4-benzoquinone: the First Quinone Carrying an N-methoxy-N-methylamino Group
We report herein a four-step preparation of the title compound. Gentisic acid (1) was firstly converted into its diacetate (2) by treatment with acetic anhydride in the presence of concentrated sulfuric acid. Treatment of the diacetate with oxalyl chloride in dichloromethane in the presence of dim...
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| Format: | Article |
| Language: | English English |
| Published: |
1988
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| Online Access: | http://psasir.upm.edu.my/id/eprint/2698/1/Synthesis_of_N-methoxy-N-methylaminocarbonyl-.pdf http://psasir.upm.edu.my/id/eprint/2698/ |
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