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Enzymatic synthesis of fatty amides from palm olein

Fatty amides have been successfully synthesized from palm olein and urea by a one-step lipase catalyzed reaction. The use of immobilized lipase as the catalyst for the preparation reaction provides an easy isolation of the enzyme from the products and other components in the reaction mixture. The fa...

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Main Authors: Al-Mulla, Emad A. Jaffar, Wan Yunus, Wan Md. Zin, Ibrahim, Nor Azowa, Ab. Rahman, Mohamad Zaki
Format: Article
Language:English
Published: Japan Oil Chemists' Society 2010
Online Access:http://psasir.upm.edu.my/id/eprint/14541/1/Enzymatic%20synthesis%20of%20fatty%20amides%20from%20palm%20olein.pdf
http://psasir.upm.edu.my/id/eprint/14541/
https://www.jstage.jst.go.jp/article/jos/59/2/59_2_59/_article
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spelling my.upm.eprints.145412015-10-29T06:08:12Z http://psasir.upm.edu.my/id/eprint/14541/ Enzymatic synthesis of fatty amides from palm olein Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki Fatty amides have been successfully synthesized from palm olein and urea by a one-step lipase catalyzed reaction. The use of immobilized lipase as the catalyst for the preparation reaction provides an easy isolation of the enzyme from the products and other components in the reaction mixture. The fatty amides were characterized using Fourier transform infrared (FTIR) spectroscopy, proton nuclear magnetic resonance (1 H NMR) technique and elemental analysis. The highest conversion percentage (96%) was obtained when the process was carried out for 36 hours using urea to palm oil ratio of 5.2: 1.0 at 40°C. The method employed offers several advantages such as renewable and abundant of the raw material,simple reaction procedure, environmentally friendly process and high yield of the product. Japan Oil Chemists' Society 2010 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/14541/1/Enzymatic%20synthesis%20of%20fatty%20amides%20from%20palm%20olein.pdf Al-Mulla, Emad A. Jaffar and Wan Yunus, Wan Md. Zin and Ibrahim, Nor Azowa and Ab. Rahman, Mohamad Zaki (2010) Enzymatic synthesis of fatty amides from palm olein. Journal of Oleo Science, 59 (2). pp. 59-64. ISSN 1345-8957; ESSN: 1347-3352 https://www.jstage.jst.go.jp/article/jos/59/2/59_2_59/_article 10.5650/jos.59.59
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
language English
description Fatty amides have been successfully synthesized from palm olein and urea by a one-step lipase catalyzed reaction. The use of immobilized lipase as the catalyst for the preparation reaction provides an easy isolation of the enzyme from the products and other components in the reaction mixture. The fatty amides were characterized using Fourier transform infrared (FTIR) spectroscopy, proton nuclear magnetic resonance (1 H NMR) technique and elemental analysis. The highest conversion percentage (96%) was obtained when the process was carried out for 36 hours using urea to palm oil ratio of 5.2: 1.0 at 40°C. The method employed offers several advantages such as renewable and abundant of the raw material,simple reaction procedure, environmentally friendly process and high yield of the product.
format Article
author Al-Mulla, Emad A. Jaffar
Wan Yunus, Wan Md. Zin
Ibrahim, Nor Azowa
Ab. Rahman, Mohamad Zaki
spellingShingle Al-Mulla, Emad A. Jaffar
Wan Yunus, Wan Md. Zin
Ibrahim, Nor Azowa
Ab. Rahman, Mohamad Zaki
Enzymatic synthesis of fatty amides from palm olein
author_facet Al-Mulla, Emad A. Jaffar
Wan Yunus, Wan Md. Zin
Ibrahim, Nor Azowa
Ab. Rahman, Mohamad Zaki
author_sort Al-Mulla, Emad A. Jaffar
title Enzymatic synthesis of fatty amides from palm olein
title_short Enzymatic synthesis of fatty amides from palm olein
title_full Enzymatic synthesis of fatty amides from palm olein
title_fullStr Enzymatic synthesis of fatty amides from palm olein
title_full_unstemmed Enzymatic synthesis of fatty amides from palm olein
title_sort enzymatic synthesis of fatty amides from palm olein
publisher Japan Oil Chemists' Society
publishDate 2010
url http://psasir.upm.edu.my/id/eprint/14541/1/Enzymatic%20synthesis%20of%20fatty%20amides%20from%20palm%20olein.pdf
http://psasir.upm.edu.my/id/eprint/14541/
https://www.jstage.jst.go.jp/article/jos/59/2/59_2_59/_article
_version_ 1643825663291949056
score 13.211869

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