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Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics

Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS11Na2CO324ES6P2O56CaF29Al2O3 (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The...

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Main Authors: Ismail, Nur Quratul Aini, Sa’at, Nor Kamilah, Mohd Zaid, Mohd Hafiz, Zainuddin, Norhazlin, Mayzan, Mohd Zul Hilmi
Format: Article
Published: Springer 2024
Online Access:http://psasir.upm.edu.my/id/eprint/115026/
https://link.springer.com/article/10.1007/s41779-024-01049-z?error=cookies_not_supported&code=e8e56dbe-79f2-49d0-8866-45e24f597657
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spelling my.upm.eprints.1150262025-02-17T07:51:10Z http://psasir.upm.edu.my/id/eprint/115026/ Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics Ismail, Nur Quratul Aini Sa’at, Nor Kamilah Mohd Zaid, Mohd Hafiz Zainuddin, Norhazlin Mayzan, Mohd Zul Hilmi Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS11Na2CO324ES6P2O56CaF29Al2O3 (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The physical properties were characterized by density and linear shrinkage. To characterize the structure properties, X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) were utilized. The high composition of Si and Ca in soda lime silica (SLS) glass and eggshells (ES), respectively, encourage the utilization of waste materials in the production of bioglass-ceramics. The results showed that at a sintering temperature of 950 °C, the crystallization of fluorapatite was the main phase. Moreover, the high density and optimum linear shrinkage were obtained as the sintering temperature increased. Additionally, grain growth and densification took place at this temperature. The compressive strength of bioglass-ceramics is influenced by sintering temperature and the optimal compressive strength is 136.58 MPa. © Australian Ceramic Society 2024. Springer 2024 Article PeerReviewed Ismail, Nur Quratul Aini and Sa’at, Nor Kamilah and Mohd Zaid, Mohd Hafiz and Zainuddin, Norhazlin and Mayzan, Mohd Zul Hilmi (2024) Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics. Journal of the Australian Ceramic Society, 60 (5). pp. 1419-1426. ISSN 2510-1560; eISSN: 2510-1579 https://link.springer.com/article/10.1007/s41779-024-01049-z?error=cookies_not_supported&code=e8e56dbe-79f2-49d0-8866-45e24f597657 10.1007/s41779-024-01049-z
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
description Melt-quenching bioglass-ceramics with the following chemical composition have been prepared 44SLS11Na2CO324ES6P2O56CaF29Al2O3 (wt%). The bioglass-ceramics were sintered at 650 °C, 750 °C, 850 °C, and 950 °C. The aim was to identify the optimal sintering temperature before glass crystallization. The physical properties were characterized by density and linear shrinkage. To characterize the structure properties, X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR) were utilized. The high composition of Si and Ca in soda lime silica (SLS) glass and eggshells (ES), respectively, encourage the utilization of waste materials in the production of bioglass-ceramics. The results showed that at a sintering temperature of 950 °C, the crystallization of fluorapatite was the main phase. Moreover, the high density and optimum linear shrinkage were obtained as the sintering temperature increased. Additionally, grain growth and densification took place at this temperature. The compressive strength of bioglass-ceramics is influenced by sintering temperature and the optimal compressive strength is 136.58 MPa. © Australian Ceramic Society 2024.
format Article
author Ismail, Nur Quratul Aini
Sa’at, Nor Kamilah
Mohd Zaid, Mohd Hafiz
Zainuddin, Norhazlin
Mayzan, Mohd Zul Hilmi
spellingShingle Ismail, Nur Quratul Aini
Sa’at, Nor Kamilah
Mohd Zaid, Mohd Hafiz
Zainuddin, Norhazlin
Mayzan, Mohd Zul Hilmi
Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
author_facet Ismail, Nur Quratul Aini
Sa’at, Nor Kamilah
Mohd Zaid, Mohd Hafiz
Zainuddin, Norhazlin
Mayzan, Mohd Zul Hilmi
author_sort Ismail, Nur Quratul Aini
title Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
title_short Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
title_full Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
title_fullStr Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
title_full_unstemmed Effect of temperature variations on the fabrication of SLS-Na2CO3-ES-P2O5-CaF2-Al2O3 based bioglass-ceramics
title_sort effect of temperature variations on the fabrication of sls-na2co3-es-p2o5-caf2-al2o3 based bioglass-ceramics
publisher Springer
publishDate 2024
url http://psasir.upm.edu.my/id/eprint/115026/
https://link.springer.com/article/10.1007/s41779-024-01049-z?error=cookies_not_supported&code=e8e56dbe-79f2-49d0-8866-45e24f597657
_version_ 1825162416993861632
score 13.239859

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