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Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method

In this study, zinc oxide (ZnO) nanowires are grown by chemical bath deposition (CBD) using aqueous solutions with [Zn (NO3)2]: [HMTA] ratios of 1:2/5, 1:1/2, 1:2/3, 1:1, 1:2, and 1:3. The effects of hexamethylenetetramine (HMTA) on the formation of Zinc oxide (ZnO) nanowires are investigated. The X...

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Main Authors: Mohd Aris, Siti Nurnadiah, Azmi, Zaidatul Hanis, Sagadevan, Suresh, Abubakar, Shamsu, Siburian, Rikson, Paiman, Suriati
Format: Article
Published: Wiley 2023
Online Access:http://psasir.upm.edu.my/id/eprint/107509/
https://onlinelibrary.wiley.com/doi/10.1002/crat.202300075
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spelling my.upm.eprints.1075092024-10-17T07:35:26Z http://psasir.upm.edu.my/id/eprint/107509/ Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method Mohd Aris, Siti Nurnadiah Azmi, Zaidatul Hanis Sagadevan, Suresh Abubakar, Shamsu Siburian, Rikson Paiman, Suriati In this study, zinc oxide (ZnO) nanowires are grown by chemical bath deposition (CBD) using aqueous solutions with [Zn (NO3)2]: [HMTA] ratios of 1:2/5, 1:1/2, 1:2/3, 1:1, 1:2, and 1:3. The effects of hexamethylenetetramine (HMTA) on the formation of Zinc oxide (ZnO) nanowires are investigated. The XRD results reveal that the dominant peak observed at 2θ = 36.25° indicates preferential growth along the (101) crystal plane, and the ZnO nanowires have a larger crystallite size than the others. The length of the ZnO nanowires, grows with a ZnO seed in the thickness of one and three layers, gets increased from 256.16 ± 15.15 to 497.80 ± 7.84 nm, while the diameter decreases from 497.80 ± 7.84 to 50.34 ± 4.23 nm. The ZnO nanowires deposited by one layer show a similar pattern with the three layers, in which the length is increased from 8.44 ± 0.31 to 14.60 ± 0.51 µm, and the diameter has decreased from 1.95 ± 0.09 to 0.49 ± 0.06 µm. These results support the role of HMTA as a capping agent for the production of ammonia (NH3). This study can control the dimensions of ZnO nanowires using the HMTA concentration to obtain extra-long nanowires desired for piezoelectric applications. Wiley 2023-11 Article PeerReviewed Mohd Aris, Siti Nurnadiah and Azmi, Zaidatul Hanis and Sagadevan, Suresh and Abubakar, Shamsu and Siburian, Rikson and Paiman, Suriati (2023) Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method. Crystal Research and Technology, 58 (11). art. no. 2300075. pp. 1-7. ISSN 0232-1300; ESSN: 1521-4079 https://onlinelibrary.wiley.com/doi/10.1002/crat.202300075 10.1002/crat.202300075
institution Universiti Putra Malaysia
building UPM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Putra Malaysia
content_source UPM Institutional Repository
url_provider http://psasir.upm.edu.my/
description In this study, zinc oxide (ZnO) nanowires are grown by chemical bath deposition (CBD) using aqueous solutions with [Zn (NO3)2]: [HMTA] ratios of 1:2/5, 1:1/2, 1:2/3, 1:1, 1:2, and 1:3. The effects of hexamethylenetetramine (HMTA) on the formation of Zinc oxide (ZnO) nanowires are investigated. The XRD results reveal that the dominant peak observed at 2θ = 36.25° indicates preferential growth along the (101) crystal plane, and the ZnO nanowires have a larger crystallite size than the others. The length of the ZnO nanowires, grows with a ZnO seed in the thickness of one and three layers, gets increased from 256.16 ± 15.15 to 497.80 ± 7.84 nm, while the diameter decreases from 497.80 ± 7.84 to 50.34 ± 4.23 nm. The ZnO nanowires deposited by one layer show a similar pattern with the three layers, in which the length is increased from 8.44 ± 0.31 to 14.60 ± 0.51 µm, and the diameter has decreased from 1.95 ± 0.09 to 0.49 ± 0.06 µm. These results support the role of HMTA as a capping agent for the production of ammonia (NH3). This study can control the dimensions of ZnO nanowires using the HMTA concentration to obtain extra-long nanowires desired for piezoelectric applications.
format Article
author Mohd Aris, Siti Nurnadiah
Azmi, Zaidatul Hanis
Sagadevan, Suresh
Abubakar, Shamsu
Siburian, Rikson
Paiman, Suriati
spellingShingle Mohd Aris, Siti Nurnadiah
Azmi, Zaidatul Hanis
Sagadevan, Suresh
Abubakar, Shamsu
Siburian, Rikson
Paiman, Suriati
Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method
author_facet Mohd Aris, Siti Nurnadiah
Azmi, Zaidatul Hanis
Sagadevan, Suresh
Abubakar, Shamsu
Siburian, Rikson
Paiman, Suriati
author_sort Mohd Aris, Siti Nurnadiah
title Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method
title_short Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method
title_full Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method
title_fullStr Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method
title_full_unstemmed Effect of hexamethylenetetramine of Zinc oxide nanowires using chemical bath deposition method
title_sort effect of hexamethylenetetramine of zinc oxide nanowires using chemical bath deposition method
publisher Wiley
publishDate 2023
url http://psasir.upm.edu.my/id/eprint/107509/
https://onlinelibrary.wiley.com/doi/10.1002/crat.202300075
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score 13.244368

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