Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage

Microencapsulated paraffin wax/polyaniline was prepared using a simple in situ polymerization technique, and its performance characteristics were investigated. Weight losses of samples were determined by Thermal Gravimetry Analysis (TGA). The microencapsulated samples with 23% and 49% paraffin showe...

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Main Authors: Silakhori, M., Naghavi, M.S., Metselaar, H.S.C., Mahlia, T.M.I., Fauzi, H., Mehrali, M.
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Published: 2017
Online Access:http://dspace.uniten.edu.my/jspui/handle/123456789/6145
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spelling my.uniten.dspace-61452017-12-08T09:11:42Z Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage Silakhori, M. Naghavi, M.S. Metselaar, H.S.C. Mahlia, T.M.I. Fauzi, H. Mehrali, M. Microencapsulated paraffin wax/polyaniline was prepared using a simple in situ polymerization technique, and its performance characteristics were investigated. Weight losses of samples were determined by Thermal Gravimetry Analysis (TGA). The microencapsulated samples with 23% and 49% paraffin showed less decomposition after 330 °C than with higher percentage of paraffin. These samples were then subjected to a thermal cycling test. Thermal properties of microencapsulated paraffin wax were evaluated by Differential Scanning Calorimeter (DSC). Structure stability and compatibility of core and coating materials were also tested by Fourier transform infrared spectrophotometer (FTIR), and the surface morphology of the samples are shown by Field Emission Scanning Electron Microscopy (FESEM). It has been found that the microencapsulated paraffin waxes show little change in the latent heat of fusion and melting temperature after one thousand thermal recycles. Besides, the chemical characteristics and structural profile remained constant after one thousand thermal cycling tests. Therefore, microencapsulated paraffin wax/polyaniline is a stable material that can be used for thermal energy storage systems. © 2013 by the authors; licensee MDPI, Basel, Switzerland. 2017-12-08T09:11:42Z 2017-12-08T09:11:42Z 2013 http://dspace.uniten.edu.my/jspui/handle/123456789/6145
institution Universiti Tenaga Nasional
building UNITEN Library
collection Institutional Repository
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country Malaysia
content_provider Universiti Tenaga Nasional
content_source UNITEN Institutional Repository
url_provider http://dspace.uniten.edu.my/
description Microencapsulated paraffin wax/polyaniline was prepared using a simple in situ polymerization technique, and its performance characteristics were investigated. Weight losses of samples were determined by Thermal Gravimetry Analysis (TGA). The microencapsulated samples with 23% and 49% paraffin showed less decomposition after 330 °C than with higher percentage of paraffin. These samples were then subjected to a thermal cycling test. Thermal properties of microencapsulated paraffin wax were evaluated by Differential Scanning Calorimeter (DSC). Structure stability and compatibility of core and coating materials were also tested by Fourier transform infrared spectrophotometer (FTIR), and the surface morphology of the samples are shown by Field Emission Scanning Electron Microscopy (FESEM). It has been found that the microencapsulated paraffin waxes show little change in the latent heat of fusion and melting temperature after one thousand thermal recycles. Besides, the chemical characteristics and structural profile remained constant after one thousand thermal cycling tests. Therefore, microencapsulated paraffin wax/polyaniline is a stable material that can be used for thermal energy storage systems. © 2013 by the authors; licensee MDPI, Basel, Switzerland.
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author Silakhori, M.
Naghavi, M.S.
Metselaar, H.S.C.
Mahlia, T.M.I.
Fauzi, H.
Mehrali, M.
spellingShingle Silakhori, M.
Naghavi, M.S.
Metselaar, H.S.C.
Mahlia, T.M.I.
Fauzi, H.
Mehrali, M.
Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage
author_facet Silakhori, M.
Naghavi, M.S.
Metselaar, H.S.C.
Mahlia, T.M.I.
Fauzi, H.
Mehrali, M.
author_sort Silakhori, M.
title Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage
title_short Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage
title_full Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage
title_fullStr Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage
title_full_unstemmed Accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage
title_sort accelerated thermal cycling test of microencapsulated paraffin wax/polyaniline made by simple preparation method for solar thermal energy storage
publishDate 2017
url http://dspace.uniten.edu.my/jspui/handle/123456789/6145
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score 13.211869