Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection

Rapid detection of vitamin D levels in human serum presents significant benefits for diagnosing deficiency and managing treatments. This work reports the preparation and application of silver-graphene oxide (Ag-GO) composites for the development of vitamin D biosensors through chemical reduction met...

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Main Authors: Kiki C., Mohd Said N.A., Mohammad Haniff M.A.S., Zaid M.H.M., Mohd Nashruddin S.N.A., Wee M.F.M.R., Menon P.S.
Other Authors: 58121554300
Format: Conference paper
Published: Institute of Electrical and Electronics Engineers Inc. 2025
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spelling my.uniten.dspace-369692025-03-03T15:46:12Z Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection Kiki C. Mohd Said N.A. Mohammad Haniff M.A.S. Zaid M.H.M. Mohd Nashruddin S.N.A. Wee M.F.M.R. Menon P.S. 58121554300 57201749501 57212061586 57287246700 57250413900 56028366000 57201289731 Atomic emission spectroscopy Electrochemical sensors Graphene oxide Metal nanoparticles Silver nanoparticles Chemical reduction methods Electrochemicals Graphene oxide-silver nanoparticle Graphene oxides Human serum Oxide composites Rapid detection Screen-printed carbon electrodes Vitamin D detection Vitamin-D Fourier transform infrared spectroscopy Rapid detection of vitamin D levels in human serum presents significant benefits for diagnosing deficiency and managing treatments. This work reports the preparation and application of silver-graphene oxide (Ag-GO) composites for the development of vitamin D biosensors through chemical reduction method of silver nanoparticles (AgNPs) in aqueous suspension of graphene oxide (GO). Different concentrations of graphene oxide (GO) and silver (Ag) were tested to identify optimal electrochemical enhancements of screen-printed carbon electrodes (SPCE). By synthesizing Ag-GO composites and modifying SPCE, the electrochemical behaviour was investigated using differential pulse voltammetry (DPV). The Ag-GO composite prepared were characterised using Fourier-Transform infrared spectroscopy (FTIR) and field-emission scanning electron microscopy (FESEM). AgGO synthesised from 2?10-3 mol dm-3 AgNO3 and 1.0 g/L GO provided the most favourable conducting environment for electron transfer from the electrolyte to the electrode. The modified SPCE exhibited more than a threefold enhancement in peak current, reaching 37.98 ?A, compared to an unmodified electrode. ? 2024 IEEE. Final 2025-03-03T07:46:12Z 2025-03-03T07:46:12Z 2024 Conference paper 10.1109/ICSE62991.2024.10681353 2-s2.0-85206492578 https://www.scopus.com/inward/record.uri?eid=2-s2.0-85206492578&doi=10.1109%2fICSE62991.2024.10681353&partnerID=40&md5=82a6fac9d6c5404d088f15cb4d6fd82f https://irepository.uniten.edu.my/handle/123456789/36969 104 107 Institute of Electrical and Electronics Engineers Inc. Scopus
institution Universiti Tenaga Nasional
building UNITEN Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Tenaga Nasional
content_source UNITEN Institutional Repository
url_provider http://dspace.uniten.edu.my/
topic Atomic emission spectroscopy
Electrochemical sensors
Graphene oxide
Metal nanoparticles
Silver nanoparticles
Chemical reduction methods
Electrochemicals
Graphene oxide-silver nanoparticle
Graphene oxides
Human serum
Oxide composites
Rapid detection
Screen-printed carbon electrodes
Vitamin D detection
Vitamin-D
Fourier transform infrared spectroscopy
spellingShingle Atomic emission spectroscopy
Electrochemical sensors
Graphene oxide
Metal nanoparticles
Silver nanoparticles
Chemical reduction methods
Electrochemicals
Graphene oxide-silver nanoparticle
Graphene oxides
Human serum
Oxide composites
Rapid detection
Screen-printed carbon electrodes
Vitamin D detection
Vitamin-D
Fourier transform infrared spectroscopy
Kiki C.
Mohd Said N.A.
Mohammad Haniff M.A.S.
Zaid M.H.M.
Mohd Nashruddin S.N.A.
Wee M.F.M.R.
Menon P.S.
Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection
description Rapid detection of vitamin D levels in human serum presents significant benefits for diagnosing deficiency and managing treatments. This work reports the preparation and application of silver-graphene oxide (Ag-GO) composites for the development of vitamin D biosensors through chemical reduction method of silver nanoparticles (AgNPs) in aqueous suspension of graphene oxide (GO). Different concentrations of graphene oxide (GO) and silver (Ag) were tested to identify optimal electrochemical enhancements of screen-printed carbon electrodes (SPCE). By synthesizing Ag-GO composites and modifying SPCE, the electrochemical behaviour was investigated using differential pulse voltammetry (DPV). The Ag-GO composite prepared were characterised using Fourier-Transform infrared spectroscopy (FTIR) and field-emission scanning electron microscopy (FESEM). AgGO synthesised from 2?10-3 mol dm-3 AgNO3 and 1.0 g/L GO provided the most favourable conducting environment for electron transfer from the electrolyte to the electrode. The modified SPCE exhibited more than a threefold enhancement in peak current, reaching 37.98 ?A, compared to an unmodified electrode. ? 2024 IEEE.
author2 58121554300
author_facet 58121554300
Kiki C.
Mohd Said N.A.
Mohammad Haniff M.A.S.
Zaid M.H.M.
Mohd Nashruddin S.N.A.
Wee M.F.M.R.
Menon P.S.
format Conference paper
author Kiki C.
Mohd Said N.A.
Mohammad Haniff M.A.S.
Zaid M.H.M.
Mohd Nashruddin S.N.A.
Wee M.F.M.R.
Menon P.S.
author_sort Kiki C.
title Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection
title_short Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection
title_full Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection
title_fullStr Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection
title_full_unstemmed Impact of Varied Ag-GO Ratios on the Electrochemical Enhancement of Vitamin D Detection
title_sort impact of varied ag-go ratios on the electrochemical enhancement of vitamin d detection
publisher Institute of Electrical and Electronics Engineers Inc.
publishDate 2025
_version_ 1825816038262964224
score 13.244413