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Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)

Alcohols; Crystalline materials; Mixing; Morphology; Organometallics; Palm oil; Pressure vessels; Surface active agents; Direct mixing method; Faceted structures; Metal organic framework; Microwave assisted synthesis; Microwave-assisted methods; Non-surfactant Template; Structural characteristics; S...

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Main Authors: Othman S.Z., Misran H., Affendy W.A., Mahadi N.F.
Other Authors: 55548997100
Format: Conference Paper
Published: Institute of Physics Publishing 2023
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id my.uniten.dspace-22771
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spelling my.uniten.dspace-227712023-05-29T14:12:09Z Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5) Othman S.Z. Misran H. Affendy W.A. Mahadi N.F. 55548997100 6506899840 57189241496 57189241140 Alcohols; Crystalline materials; Mixing; Morphology; Organometallics; Palm oil; Pressure vessels; Surface active agents; Direct mixing method; Faceted structures; Metal organic framework; Microwave assisted synthesis; Microwave-assisted methods; Non-surfactant Template; Structural characteristics; Synthesis method; Java programming language; alcohol; numerical method; surfactant; temperature gradient; vegetable oil In this work, metal-organic framework (MOF-5) syntheses were successfully synthesized with three different methods namely i) modified direct-mixing method ii) microwave assisted method and iii) autoclave assisted method without using surfactants. Palm oil derived fatty alcohol (PODFA), dodecyl alcohol (C8) was used as renewable non-surfactant template. Four prominent peaks were observed in all three samples attributable to the reflection planes of (200), (220), (400) and (420) of a cubic structure at ca. 2? = 6.9�, 9.6�, 13.7� and 15.2�. The morphology of MOF-5 produced using modified direct-mixing method was faceted structure with average size of ca. 1 ?m. In addition, the morphology of MOF-5 produced using microwave assisted synthesis was cubic structure with average size of ca. 8.34 ?m. However, the morphology of MOF-5 using autoclave assisted method was interpenetrated cubic with average size of ca. 22.65 ?m. Final 2023-05-29T06:12:09Z 2023-05-29T06:12:09Z 2016 Conference Paper 10.1088/1755-1315/32/1/012060 2-s2.0-84966586699 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84966586699&doi=10.1088%2f1755-1315%2f32%2f1%2f012060&partnerID=40&md5=3bac02d70b187914e1802bb1fb647a14 https://irepository.uniten.edu.my/handle/123456789/22771 32 1 12060 All Open Access, Bronze Institute of Physics Publishing Scopus
institution Universiti Tenaga Nasional
building UNITEN Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Tenaga Nasional
content_source UNITEN Institutional Repository
url_provider http://dspace.uniten.edu.my/
description Alcohols; Crystalline materials; Mixing; Morphology; Organometallics; Palm oil; Pressure vessels; Surface active agents; Direct mixing method; Faceted structures; Metal organic framework; Microwave assisted synthesis; Microwave-assisted methods; Non-surfactant Template; Structural characteristics; Synthesis method; Java programming language; alcohol; numerical method; surfactant; temperature gradient; vegetable oil
author2 55548997100
author_facet 55548997100
Othman S.Z.
Misran H.
Affendy W.A.
Mahadi N.F.
format Conference Paper
author Othman S.Z.
Misran H.
Affendy W.A.
Mahadi N.F.
spellingShingle Othman S.Z.
Misran H.
Affendy W.A.
Mahadi N.F.
Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)
author_sort Othman S.Z.
title Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)
title_short Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)
title_full Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)
title_fullStr Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)
title_full_unstemmed Effect of Synthesis Methods Using Renewable PODFA on Structural Characteristics of Metal-Organic Framework (MOF-5)
title_sort effect of synthesis methods using renewable podfa on structural characteristics of metal-organic framework (mof-5)
publisher Institute of Physics Publishing
publishDate 2023
_version_ 1806426686429855744
score 13.222552

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