Microemulsion-based peanut oil extraction using surfactant solution

Nowadays, vegetable oil is an alternative for the substitution of biodiesel. Vegetable oil extraction is more favourable by using surfactant compared to hexane which is hazardous to human. In this study, extraction efficiency and physical appearance of oil extracted by Brij-30, GE-460 and their mixt...

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Main Author: Nur Syafiqah Amira, Binti Mohd Zulkefli
Format: Final Year Project Report
Language:English
Published: Universiti Malaysia Sarawak, UNIMAS 2012
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Online Access:http://ir.unimas.my/id/eprint/6211/8/MICROEMULSION-BASED%20PEANUT%20OIL%20EXTRACTION%20USING%20SURFACTANT%20SOLUTION%28OCR%29.pdf
http://ir.unimas.my/id/eprint/6211/
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spelling my.unimas.ir.62112023-11-15T07:21:24Z http://ir.unimas.my/id/eprint/6211/ Microemulsion-based peanut oil extraction using surfactant solution Nur Syafiqah Amira, Binti Mohd Zulkefli GE Environmental Sciences QD Chemistry SB Plant culture Nowadays, vegetable oil is an alternative for the substitution of biodiesel. Vegetable oil extraction is more favourable by using surfactant compared to hexane which is hazardous to human. In this study, extraction efficiency and physical appearance of oil extracted by Brij-30, GE-460 and their mixture were evaluated at optimum conditions. Microemulsionbased extraction was conducted by mixing these surfactants with ground peanut samples (0.2-0.5mm) and agitated at 150 rpm. This enables the oil to be collected because it’s liberated from the samples as a separate phase from the aqueous phase. Contact time, concentration of surfactant, weight of samples and types of surfactant on oil yield were tested to identify optimum extraction conditions. After optimum conditions were achieved, solvent based extraction using hexane was done by soxhlet method for comparison. The oil collected from both extractions was compared based on their extraction efficiencies, physical appearance of oil and Fourier Transform Infrared Spectroscopy (FTIR) characterization. The appearance of oil extracted using surfactant showed lighter yellow colour and did not produced any odour compared to hexane extraction. Optimum extraction of 87.15% was achieved at weight of sample of 1g, 30 minutes extraction at 150 shakes/min, and 0.015M surfactant concentration while the extraction efficiency for mixed surfactant of GE-60 and Brij-30 was 92.93% in the ratio of Brij-30 to GE-460 of 3:1. Percentage of extraction using solvent is 91.37% which is higher compared to microemulsion-based extraction. The FTIR characterization on both methods shows not much difference due to the same source of origin. The formation of oil was proven by ester formation that was detected at 1743cm-1. Universiti Malaysia Sarawak, UNIMAS 2012 Final Year Project Report NonPeerReviewed text en http://ir.unimas.my/id/eprint/6211/8/MICROEMULSION-BASED%20PEANUT%20OIL%20EXTRACTION%20USING%20SURFACTANT%20SOLUTION%28OCR%29.pdf Nur Syafiqah Amira, Binti Mohd Zulkefli (2012) Microemulsion-based peanut oil extraction using surfactant solution. [Final Year Project Report] (Unpublished)
institution Universiti Malaysia Sarawak
building Centre for Academic Information Services (CAIS)
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Sarawak
content_source UNIMAS Institutional Repository
url_provider http://ir.unimas.my/
language English
topic GE Environmental Sciences
QD Chemistry
SB Plant culture
spellingShingle GE Environmental Sciences
QD Chemistry
SB Plant culture
Nur Syafiqah Amira, Binti Mohd Zulkefli
Microemulsion-based peanut oil extraction using surfactant solution
description Nowadays, vegetable oil is an alternative for the substitution of biodiesel. Vegetable oil extraction is more favourable by using surfactant compared to hexane which is hazardous to human. In this study, extraction efficiency and physical appearance of oil extracted by Brij-30, GE-460 and their mixture were evaluated at optimum conditions. Microemulsionbased extraction was conducted by mixing these surfactants with ground peanut samples (0.2-0.5mm) and agitated at 150 rpm. This enables the oil to be collected because it’s liberated from the samples as a separate phase from the aqueous phase. Contact time, concentration of surfactant, weight of samples and types of surfactant on oil yield were tested to identify optimum extraction conditions. After optimum conditions were achieved, solvent based extraction using hexane was done by soxhlet method for comparison. The oil collected from both extractions was compared based on their extraction efficiencies, physical appearance of oil and Fourier Transform Infrared Spectroscopy (FTIR) characterization. The appearance of oil extracted using surfactant showed lighter yellow colour and did not produced any odour compared to hexane extraction. Optimum extraction of 87.15% was achieved at weight of sample of 1g, 30 minutes extraction at 150 shakes/min, and 0.015M surfactant concentration while the extraction efficiency for mixed surfactant of GE-60 and Brij-30 was 92.93% in the ratio of Brij-30 to GE-460 of 3:1. Percentage of extraction using solvent is 91.37% which is higher compared to microemulsion-based extraction. The FTIR characterization on both methods shows not much difference due to the same source of origin. The formation of oil was proven by ester formation that was detected at 1743cm-1.
format Final Year Project Report
author Nur Syafiqah Amira, Binti Mohd Zulkefli
author_facet Nur Syafiqah Amira, Binti Mohd Zulkefli
author_sort Nur Syafiqah Amira, Binti Mohd Zulkefli
title Microemulsion-based peanut oil extraction using surfactant solution
title_short Microemulsion-based peanut oil extraction using surfactant solution
title_full Microemulsion-based peanut oil extraction using surfactant solution
title_fullStr Microemulsion-based peanut oil extraction using surfactant solution
title_full_unstemmed Microemulsion-based peanut oil extraction using surfactant solution
title_sort microemulsion-based peanut oil extraction using surfactant solution
publisher Universiti Malaysia Sarawak, UNIMAS
publishDate 2012
url http://ir.unimas.my/id/eprint/6211/8/MICROEMULSION-BASED%20PEANUT%20OIL%20EXTRACTION%20USING%20SURFACTANT%20SOLUTION%28OCR%29.pdf
http://ir.unimas.my/id/eprint/6211/
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score 13.211869