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Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment

The physicochemical properties of dabai kernel oil as well as the morphology of dabai samples are affected by the optimal extraction method and process configurations. Subcritical water treatment prior to dabai kernel oil extraction was optimized through the utilization of response surface methodolo...

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Main Authors: Muhammad Hazwan, Hamzah, Nurbalqis, Zulkefli, Adila Fazliyana, Aili Hamzah, Rosnah, Shamsudin, Hasfalina, Che Man, Abd Halim, Md Ali, Maimunah, Mohd Ali, Bernard, Maringgal, Mohd Hafiz, Wondi
Format: Article
Language:English
Published: Springer 2024
Subjects:
Q Science (General)
S Agriculture (General)
T Technology (General)
Online Access:http://ir.unimas.my/id/eprint/44601/1/2667ad68-e4db-4215-bcd6-d71bb08c927f.pdf
http://ir.unimas.my/id/eprint/44601/
https://link.springer.com/article/10.1007/s12161-024-02624-7
https://doi.org/10.1007/s12161-024-02624-7
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spelling my.unimas.ir.446012024-04-22T01:16:16Z http://ir.unimas.my/id/eprint/44601/ Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment Muhammad Hazwan, Hamzah Nurbalqis, Zulkefli Adila Fazliyana, Aili Hamzah Rosnah, Shamsudin Hasfalina, Che Man Abd Halim, Md Ali Maimunah, Mohd Ali Bernard, Maringgal Mohd Hafiz, Wondi Q Science (General) S Agriculture (General) T Technology (General) The physicochemical properties of dabai kernel oil as well as the morphology of dabai samples are affected by the optimal extraction method and process configurations. Subcritical water treatment prior to dabai kernel oil extraction was optimized through the utilization of response surface methodology based on central composite design. The subcritical water treatment was carried out within the following temperature ranges of 100 to 150 °C, 10- to 20-min reaction times, and 10:1 to 20:1 solvent to solid ratios. Results showed that temperature of 100 °C, reaction time of 10 min, and solvent to solid ratio of 10:1 were optimal parameters for dabai kernel oil by subcritical water treatment prior to Soxhlet extraction. Dabai kernel oil yields via subcritical water treatment were 96.53% on average, compared to 42.85% for Soxhlet extraction sample. Gas chromatography mass spectrometry analysis found for subcritical water treatment samples revealed value-added compounds, including oxalic acid and 9-octadecenoic acid, which can be utilized for cleaning and pharmaceutical applications. Scanning electron microscope images provided evidence that rapid extraction was driven by the degradation and aggregation of dabai kernel powder structure. The Brunauer–Emmett–Teller analysis indicated that the dabai kernel of subcritical water treatment displayed a greater surface area (14.813 m2/g) than the raw (2.804 m2/g) or Soxhlet extraction (13.452 m2/g) dabai kernel. Subcritical water treatment could be considered a promising method in combination with Soxhlet extraction in order to improve the oil yield from dabai kernels. Springer 2024-04-19 Article PeerReviewed text en http://ir.unimas.my/id/eprint/44601/1/2667ad68-e4db-4215-bcd6-d71bb08c927f.pdf Muhammad Hazwan, Hamzah and Nurbalqis, Zulkefli and Adila Fazliyana, Aili Hamzah and Rosnah, Shamsudin and Hasfalina, Che Man and Abd Halim, Md Ali and Maimunah, Mohd Ali and Bernard, Maringgal and Mohd Hafiz, Wondi (2024) Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment. Food Analytical Methods. pp. 1-20. ISSN 1936-976X https://link.springer.com/article/10.1007/s12161-024-02624-7 https://doi.org/10.1007/s12161-024-02624-7
institution Universiti Malaysia Sarawak
building Centre for Academic Information Services (CAIS)
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Sarawak
content_source UNIMAS Institutional Repository
url_provider http://ir.unimas.my/
language English
topic Q Science (General)
S Agriculture (General)
T Technology (General)
spellingShingle Q Science (General)
S Agriculture (General)
T Technology (General)
Muhammad Hazwan, Hamzah
Nurbalqis, Zulkefli
Adila Fazliyana, Aili Hamzah
Rosnah, Shamsudin
Hasfalina, Che Man
Abd Halim, Md Ali
Maimunah, Mohd Ali
Bernard, Maringgal
Mohd Hafiz, Wondi
Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment
description The physicochemical properties of dabai kernel oil as well as the morphology of dabai samples are affected by the optimal extraction method and process configurations. Subcritical water treatment prior to dabai kernel oil extraction was optimized through the utilization of response surface methodology based on central composite design. The subcritical water treatment was carried out within the following temperature ranges of 100 to 150 °C, 10- to 20-min reaction times, and 10:1 to 20:1 solvent to solid ratios. Results showed that temperature of 100 °C, reaction time of 10 min, and solvent to solid ratio of 10:1 were optimal parameters for dabai kernel oil by subcritical water treatment prior to Soxhlet extraction. Dabai kernel oil yields via subcritical water treatment were 96.53% on average, compared to 42.85% for Soxhlet extraction sample. Gas chromatography mass spectrometry analysis found for subcritical water treatment samples revealed value-added compounds, including oxalic acid and 9-octadecenoic acid, which can be utilized for cleaning and pharmaceutical applications. Scanning electron microscope images provided evidence that rapid extraction was driven by the degradation and aggregation of dabai kernel powder structure. The Brunauer–Emmett–Teller analysis indicated that the dabai kernel of subcritical water treatment displayed a greater surface area (14.813 m2/g) than the raw (2.804 m2/g) or Soxhlet extraction (13.452 m2/g) dabai kernel. Subcritical water treatment could be considered a promising method in combination with Soxhlet extraction in order to improve the oil yield from dabai kernels.
format Article
author Muhammad Hazwan, Hamzah
Nurbalqis, Zulkefli
Adila Fazliyana, Aili Hamzah
Rosnah, Shamsudin
Hasfalina, Che Man
Abd Halim, Md Ali
Maimunah, Mohd Ali
Bernard, Maringgal
Mohd Hafiz, Wondi
author_facet Muhammad Hazwan, Hamzah
Nurbalqis, Zulkefli
Adila Fazliyana, Aili Hamzah
Rosnah, Shamsudin
Hasfalina, Che Man
Abd Halim, Md Ali
Maimunah, Mohd Ali
Bernard, Maringgal
Mohd Hafiz, Wondi
author_sort Muhammad Hazwan, Hamzah
title Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment
title_short Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment
title_full Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment
title_fullStr Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment
title_full_unstemmed Optimization of Process Parameters Using Response Surface Methodology for Essential Oil Extraction from Canarium odontophyllum Kernels by Subcritical Water Treatment
title_sort optimization of process parameters using response surface methodology for essential oil extraction from canarium odontophyllum kernels by subcritical water treatment
publisher Springer
publishDate 2024
url http://ir.unimas.my/id/eprint/44601/1/2667ad68-e4db-4215-bcd6-d71bb08c927f.pdf
http://ir.unimas.my/id/eprint/44601/
https://link.springer.com/article/10.1007/s12161-024-02624-7
https://doi.org/10.1007/s12161-024-02624-7
_version_ 1797543493455839232
score 13.211869

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