Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites

Luffa reinforced polylactic acid (PLA) bio-composites were prepared and examined. The luffa surface was treated using three chemicals, i.e., sodium hydroxide, 3-aminopropyltriethoxysilane, and acetic anhydride, which enhanced luffa compatibility with PLA. Mechanical testing was done on the chemical...

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Main Authors: M. Jahanzail, Kamran, Elammaran, Jayamani, Kok Heng, Soon, Choy Wong, Yat, Md. Rezaur, Rahman, Abdullah S, Al-Bogami, Durul, Huda, Muhammad Khusairy, Bakri, Mohammed M., Rahman
Format: Article
Language:English
Published: NC State University 2022
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Online Access:http://ir.unimas.my/id/eprint/40453/3/Kamran.pdf
http://ir.unimas.my/id/eprint/40453/
https://bioresources.cnr.ncsu.edu/resources/characterization-and-comparative-study-on-chemically-treated-luffa-fiber-as-reinforcement-for-polylactic-acid-bio-composites/
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spelling my.unimas.ir.404532023-05-30T00:56:37Z http://ir.unimas.my/id/eprint/40453/ Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites M. Jahanzail, Kamran Elammaran, Jayamani Kok Heng, Soon Choy Wong, Yat Md. Rezaur, Rahman Abdullah S, Al-Bogami Durul, Huda Muhammad Khusairy, Bakri Mohammed M., Rahman TP Chemical technology Luffa reinforced polylactic acid (PLA) bio-composites were prepared and examined. The luffa surface was treated using three chemicals, i.e., sodium hydroxide, 3-aminopropyltriethoxysilane, and acetic anhydride, which enhanced luffa compatibility with PLA. Mechanical testing was done on the chemically modified luffa reinforced PLA bio-composites, i.e., tensile, flexural, hardness, and thermal. Infrared spectral functional group and morphological analyses were performed on each sample. The results showed increases in tensile and flexural strength of 7.1% and 6.9% for sodium hydroxide, 5.7% and 1.4% for silane, and 4.3% and 0.4% for acetylation, respectively, especially to the surface-treated samples at 15 wt.% fiber volume, and a decrease in water uptake (%). Fourier transform infrared spectroscopy confirmed that the chemical surface treatments were successful with the removal of lignin and hemicellulose structures, which cause the surface structure of the modified fiber to be rough. Smooth surfaces were observed through SEM images. Thermal stability was enhanced due to improved interfacial bonding between luffa and PLA, eliminating other constituents and impurities. Moreover, the morphological analysis showed improved bonding compatibility between the luffa and PLA matrix. NC State University 2022 Article PeerReviewed text en http://ir.unimas.my/id/eprint/40453/3/Kamran.pdf M. Jahanzail, Kamran and Elammaran, Jayamani and Kok Heng, Soon and Choy Wong, Yat and Md. Rezaur, Rahman and Abdullah S, Al-Bogami and Durul, Huda and Muhammad Khusairy, Bakri and Mohammed M., Rahman (2022) Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites. BioResources, 17 (2). pp. 2576-2597. ISSN 1930-2126 https://bioresources.cnr.ncsu.edu/resources/characterization-and-comparative-study-on-chemically-treated-luffa-fiber-as-reinforcement-for-polylactic-acid-bio-composites/ DOI: 10.15376/biores.17.2.2576-2597
institution Universiti Malaysia Sarawak
building Centre for Academic Information Services (CAIS)
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Sarawak
content_source UNIMAS Institutional Repository
url_provider http://ir.unimas.my/
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
M. Jahanzail, Kamran
Elammaran, Jayamani
Kok Heng, Soon
Choy Wong, Yat
Md. Rezaur, Rahman
Abdullah S, Al-Bogami
Durul, Huda
Muhammad Khusairy, Bakri
Mohammed M., Rahman
Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites
description Luffa reinforced polylactic acid (PLA) bio-composites were prepared and examined. The luffa surface was treated using three chemicals, i.e., sodium hydroxide, 3-aminopropyltriethoxysilane, and acetic anhydride, which enhanced luffa compatibility with PLA. Mechanical testing was done on the chemically modified luffa reinforced PLA bio-composites, i.e., tensile, flexural, hardness, and thermal. Infrared spectral functional group and morphological analyses were performed on each sample. The results showed increases in tensile and flexural strength of 7.1% and 6.9% for sodium hydroxide, 5.7% and 1.4% for silane, and 4.3% and 0.4% for acetylation, respectively, especially to the surface-treated samples at 15 wt.% fiber volume, and a decrease in water uptake (%). Fourier transform infrared spectroscopy confirmed that the chemical surface treatments were successful with the removal of lignin and hemicellulose structures, which cause the surface structure of the modified fiber to be rough. Smooth surfaces were observed through SEM images. Thermal stability was enhanced due to improved interfacial bonding between luffa and PLA, eliminating other constituents and impurities. Moreover, the morphological analysis showed improved bonding compatibility between the luffa and PLA matrix.
format Article
author M. Jahanzail, Kamran
Elammaran, Jayamani
Kok Heng, Soon
Choy Wong, Yat
Md. Rezaur, Rahman
Abdullah S, Al-Bogami
Durul, Huda
Muhammad Khusairy, Bakri
Mohammed M., Rahman
author_facet M. Jahanzail, Kamran
Elammaran, Jayamani
Kok Heng, Soon
Choy Wong, Yat
Md. Rezaur, Rahman
Abdullah S, Al-Bogami
Durul, Huda
Muhammad Khusairy, Bakri
Mohammed M., Rahman
author_sort M. Jahanzail, Kamran
title Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites
title_short Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites
title_full Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites
title_fullStr Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites
title_full_unstemmed Characterization and Comparative Study on Chemically Treated Luffa Fiber as Reinforcement for Polylactic Acid Bio-composites
title_sort characterization and comparative study on chemically treated luffa fiber as reinforcement for polylactic acid bio-composites
publisher NC State University
publishDate 2022
url http://ir.unimas.my/id/eprint/40453/3/Kamran.pdf
http://ir.unimas.my/id/eprint/40453/
https://bioresources.cnr.ncsu.edu/resources/characterization-and-comparative-study-on-chemically-treated-luffa-fiber-as-reinforcement-for-polylactic-acid-bio-composites/
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score 13.211869