Hydrothermal conversion of kaolin to kalsilite (kalSiO₄): the effect of K₂CO₃ concentrations

Kaolin was used as a silica and alumina precursor in the hydrothermal synthesis of kalsilite with the addition of potassium carbonate (K₂CO₃) as a potassium source. The effects of different K₂CO₃ concentrations have been studied. After a 24-hour hydrothermal reaction at 200°C, kaolin treated with 1....

وصف كامل

محفوظ في:
التفاصيل البيبلوغرافية
المؤلفون الرئيسيون: Eddy Mohd Farid Mohd Yusslee, Nur Hazwani Dahon, Mohd Azrul Abdul Rajak, Sazmal Effendi Arshad
التنسيق: Proceedings
اللغة:English
English
منشور في: Pusat e-pembelajaran, UMS 2021
الموضوعات:
الوصول للمادة أونلاين:https://eprints.ums.edu.my/id/eprint/41631/1/ABSTRACT.pdf
https://eprints.ums.edu.my/id/eprint/41631/2/FULL%20TEXT.pdf
https://eprints.ums.edu.my/id/eprint/41631/
https://oer.ums.edu.my/handle/oer_source_files/1874
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الوصف
الملخص:Kaolin was used as a silica and alumina precursor in the hydrothermal synthesis of kalsilite with the addition of potassium carbonate (K₂CO₃) as a potassium source. The effects of different K₂CO₃ concentrations have been studied. After a 24-hour hydrothermal reaction at 200°C, kaolin treated with 1.25M K₂CO₃ shows 28.7°, 34.2°, and 42.3° as the most significant peaks under X-ray diffraction (XRD) which corresponds to hexagonal kalsilite. In addition, Field emission scanning electron microscopy (FESEM) images also revealed hexagonal particles proving the formation of the desired kalsilite. At K₂CO₃ concentrations less than 1.0M, boehmite and bayerite were identified to be the primary products while kalsilite forms as a minor crystalline phase. Hexagonal kalsilite was observed as the major product at higher (>1.0M) K₂CO₃ concentration while the reaction kept constant at 200°C.