Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline
4-((4-nonylphenyl)diazenyl)aniline and 4-(4-decylphenyl)diazenyl)aniline are an azo compounds with different terminal chains. The synthesis process was started via diazotization of 4- nitroaniline with phenol formed 4-(4-nitrophenyl)phenol (1). After that, 4-(4-nitrophenyl)phenol was alkylated with...
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my.ums.eprints.321262022-03-31T06:04:29Z https://eprints.ums.edu.my/id/eprint/32126/ Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud QD1-999 Chemistry 4-((4-nonylphenyl)diazenyl)aniline and 4-(4-decylphenyl)diazenyl)aniline are an azo compounds with different terminal chains. The synthesis process was started via diazotization of 4- nitroaniline with phenol formed 4-(4-nitrophenyl)phenol (1). After that, 4-(4-nitrophenyl)phenol was alkylated with 1-bromononane and 1-bromodecane to yield 1-(4-nitrophenyl)-2-(4-nonylphenyl)diazene (2) and 1-(4-decylphenyl)-2-(4-nitrophenyl)diazene (3), respectively. Finally, both molecules will undergo reduction to yield 4-((4-nonylphenyl)diazenyl)aniline (4) and 4-(4-decylphenyl)diazenyl)aniline (5), respectively. These two compounds were submitted to extensive spectroscopic examination, including Fourier Transform-Infrared (FT-IR) and Nuclear Magnetic Resonance (NMR). Faculty of Science and Natural Resources 2021-10 Proceedings PeerReviewed text en https://eprints.ums.edu.my/id/eprint/32126/1/Synthesis%20and%20chemical%20interpretation%20of%204-%28%284-nonylphenyl%29%20diazenyl%29%20aniline%20and%204-%28%284-decylphenyl%29%20diazenyl%29%20aniline.ABSTRCT.pdf text en https://eprints.ums.edu.my/id/eprint/32126/2/SYNTHESIS%20AND%20CHEMICAL%20INTERPRETATION%20OF%204-%28%284-%20NONYLPHENYL%29%20DIAZENYL%29%20ANILINE%20AND%204-%28%284-DECYLPHENYL%29%20DIAZENYL%29%20ANILINE.pdf S. Habil and Zuhair Jamain and Mohamad Zul Hilmey Makmud (2021) Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline. https://drive.google977-2-73-522200-2.com/file/d/1zKEpSiYvg9vZHHzuKra49512D_AMLubu/view |
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QD1-999 Chemistry S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
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4-((4-nonylphenyl)diazenyl)aniline and 4-(4-decylphenyl)diazenyl)aniline are an azo compounds with different terminal chains. The synthesis process was started via diazotization of 4- nitroaniline with phenol formed 4-(4-nitrophenyl)phenol (1). After that, 4-(4-nitrophenyl)phenol was alkylated with 1-bromononane and 1-bromodecane to yield 1-(4-nitrophenyl)-2-(4-nonylphenyl)diazene (2) and 1-(4-decylphenyl)-2-(4-nitrophenyl)diazene (3), respectively. Finally, both molecules will undergo reduction to yield 4-((4-nonylphenyl)diazenyl)aniline (4) and 4-(4-decylphenyl)diazenyl)aniline (5), respectively. These two compounds were submitted to extensive spectroscopic examination, including Fourier Transform-Infrared (FT-IR) and Nuclear Magnetic Resonance (NMR). |
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Proceedings |
author |
S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud |
author_facet |
S. Habil Zuhair Jamain Mohamad Zul Hilmey Makmud |
author_sort |
S. Habil |
title |
Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
title_short |
Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
title_full |
Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
title_fullStr |
Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
title_full_unstemmed |
Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
title_sort |
synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline |
publisher |
Faculty of Science and Natural Resources |
publishDate |
2021 |
url |
https://eprints.ums.edu.my/id/eprint/32126/1/Synthesis%20and%20chemical%20interpretation%20of%204-%28%284-nonylphenyl%29%20diazenyl%29%20aniline%20and%204-%28%284-decylphenyl%29%20diazenyl%29%20aniline.ABSTRCT.pdf https://eprints.ums.edu.my/id/eprint/32126/2/SYNTHESIS%20AND%20CHEMICAL%20INTERPRETATION%20OF%204-%28%284-%20NONYLPHENYL%29%20DIAZENYL%29%20ANILINE%20AND%204-%28%284-DECYLPHENYL%29%20DIAZENYL%29%20ANILINE.pdf https://eprints.ums.edu.my/id/eprint/32126/ https://drive.google977-2-73-522200-2.com/file/d/1zKEpSiYvg9vZHHzuKra49512D_AMLubu/view |
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