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Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol

Copper nanoparticles (CuNPs) have been prepared by the reduction of copper chloride in glycerol using hydrazine at ambient conditions. The reduction process takes place under vigorous stirring for 8 h. The formation of CuNPs and size were confirmed by UV/Vis analysis and TEM imaging respectively. Th...

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Main Authors: Khan, Maksudur R., Ong, Huei Ruey, Ridzuan, Ramli, R. M., Yunus
Format: Article
Published: Trans Tech Publications Inc. 2014
Subjects:
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/5378/
http://dx.doi.org/10.4028/www.scientific.net/AMM.481.21
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spelling my.ump.umpir.53782018-01-12T03:00:15Z http://umpir.ump.edu.my/id/eprint/5378/ Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol Khan, Maksudur R. Ong, Huei Ruey Ridzuan, Ramli R. M., Yunus TP Chemical technology Copper nanoparticles (CuNPs) have been prepared by the reduction of copper chloride in glycerol using hydrazine at ambient conditions. The reduction process takes place under vigorous stirring for 8 h. The formation of CuNPs and size were confirmed by UV/Vis analysis and TEM imaging respectively. The experiment result showed that, 7.062 mM of hydrazine solution and 0.0147 mM of Cu2+ solution were needed to synthesize narrow size monodisperseCuNPs.The presence of nanoparticle was found after an induction period of 4 h and further reaction time, complete Cu0 state nanoparticle was obtained as deep red wine colour was observed. Stability study of CuNPs showed that the nanoparticles were stable up to 4 days. The particle size of the nanoparticles have been analysed by transmission electron microscopy (TEM) and the average size of CuNPs was in the range 2 to 10 nm. Trans Tech Publications Inc. 2014 Article PeerReviewed Khan, Maksudur R. and Ong, Huei Ruey and Ridzuan, Ramli and R. M., Yunus (2014) Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol. Applied Mechanics and Materials, 481. pp. 21-26. ISSN 1662-7482 http://dx.doi.org/10.4028/www.scientific.net/AMM.481.21 doi:10.4028/www.scientific.net/AMM.481.21
institution Universiti Malaysia Pahang
building UMP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang
content_source UMP Institutional Repository
url_provider http://umpir.ump.edu.my/
topic TP Chemical technology
spellingShingle TP Chemical technology
Khan, Maksudur R.
Ong, Huei Ruey
Ridzuan, Ramli
R. M., Yunus
Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
description Copper nanoparticles (CuNPs) have been prepared by the reduction of copper chloride in glycerol using hydrazine at ambient conditions. The reduction process takes place under vigorous stirring for 8 h. The formation of CuNPs and size were confirmed by UV/Vis analysis and TEM imaging respectively. The experiment result showed that, 7.062 mM of hydrazine solution and 0.0147 mM of Cu2+ solution were needed to synthesize narrow size monodisperseCuNPs.The presence of nanoparticle was found after an induction period of 4 h and further reaction time, complete Cu0 state nanoparticle was obtained as deep red wine colour was observed. Stability study of CuNPs showed that the nanoparticles were stable up to 4 days. The particle size of the nanoparticles have been analysed by transmission electron microscopy (TEM) and the average size of CuNPs was in the range 2 to 10 nm.
format Article
author Khan, Maksudur R.
Ong, Huei Ruey
Ridzuan, Ramli
R. M., Yunus
author_facet Khan, Maksudur R.
Ong, Huei Ruey
Ridzuan, Ramli
R. M., Yunus
author_sort Khan, Maksudur R.
title Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_short Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_full Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_fullStr Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_full_unstemmed Synthesis of Copper Nanoparticles at Room Temperature Using Hydrazine in Glycerol
title_sort synthesis of copper nanoparticles at room temperature using hydrazine in glycerol
publisher Trans Tech Publications Inc.
publishDate 2014
url http://umpir.ump.edu.my/id/eprint/5378/
http://dx.doi.org/10.4028/www.scientific.net/AMM.481.21
_version_ 1643665188265656320
score 13.211869

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