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Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology

Nowadays,cyclodextrin widely used in industries due to its ability in encapsulation process with natural dye. However, the production cost for cyclodextrin is very expensive.A study on how to reduce the production cost by optimization of pH, concentration of cyclodextrin and temperature effect on en...

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Main Author: Nor Ashikin , Abdul Hamid
Format: Undergraduates Project Papers
Language:English
Published: 2010
Subjects:
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/5353/1/CD5870.pdf
http://umpir.ump.edu.my/id/eprint/5353/
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spelling my.ump.umpir.53532021-07-05T05:04:01Z http://umpir.ump.edu.my/id/eprint/5353/ Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology Nor Ashikin , Abdul Hamid TP Chemical technology Nowadays,cyclodextrin widely used in industries due to its ability in encapsulation process with natural dye. However, the production cost for cyclodextrin is very expensive.A study on how to reduce the production cost by optimization of pH, concentration of cyclodextrin and temperature effect on encapsulation of natural dye by cyclodextrin using Response Surface Methodology(RSM)was successfully done. During the preliminary experiment,one factor at a time was employed to screen the best range for pH,concentration of cyclodextrin and temperature.All the parameter ranges obtained were used in RSM.RSM software in Design Expert version 6.0.8 was used with Central Composite Design(CCD) mode.Seventeen sets of experiments with different parameter values were suggested by the software.The predicted optimum values for pH,concentration of cyclodextrin,temperature and concentration of encapsulation of natural dye-β-cyclodextrin were pH 3.11,0.004 mol/L,60 oC and 1.27763 g/L respectively.One set of experiment was run using the optimized parameter and as a result,1.2534 g/L concentration on encapsulation of natural dye-β-cyclodextrin was recorded. Before optimization, concentration on encapsulation of natural dye-β-cyclodextrin was only 0.775 g/L and the concentration was increased by 38.17% after optimization. The optimization also reduces the cost and energy consumption as the pH reduced from pH 10.5 to pH 3.11, concentration of cyclodextrin reduced from 0.005 mol/L to 0.004 mol/L and temperature was reduced from 70 oC to 60 oC. As a conclusion, this study was successful to increase encapsulation of natural dye by cyclodextrin production, reduce the energy consumption and also be able to reduce the production cost of cyclodextrin. 2010-05 Undergraduates Project Papers NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/5353/1/CD5870.pdf Nor Ashikin , Abdul Hamid (2010) Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology. Faculty of Chemical & Natural Resource Engineering, Universiti Malaysia Pahang.
institution Universiti Malaysia Pahang
building UMP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang
content_source UMP Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Nor Ashikin , Abdul Hamid
Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology
description Nowadays,cyclodextrin widely used in industries due to its ability in encapsulation process with natural dye. However, the production cost for cyclodextrin is very expensive.A study on how to reduce the production cost by optimization of pH, concentration of cyclodextrin and temperature effect on encapsulation of natural dye by cyclodextrin using Response Surface Methodology(RSM)was successfully done. During the preliminary experiment,one factor at a time was employed to screen the best range for pH,concentration of cyclodextrin and temperature.All the parameter ranges obtained were used in RSM.RSM software in Design Expert version 6.0.8 was used with Central Composite Design(CCD) mode.Seventeen sets of experiments with different parameter values were suggested by the software.The predicted optimum values for pH,concentration of cyclodextrin,temperature and concentration of encapsulation of natural dye-β-cyclodextrin were pH 3.11,0.004 mol/L,60 oC and 1.27763 g/L respectively.One set of experiment was run using the optimized parameter and as a result,1.2534 g/L concentration on encapsulation of natural dye-β-cyclodextrin was recorded. Before optimization, concentration on encapsulation of natural dye-β-cyclodextrin was only 0.775 g/L and the concentration was increased by 38.17% after optimization. The optimization also reduces the cost and energy consumption as the pH reduced from pH 10.5 to pH 3.11, concentration of cyclodextrin reduced from 0.005 mol/L to 0.004 mol/L and temperature was reduced from 70 oC to 60 oC. As a conclusion, this study was successful to increase encapsulation of natural dye by cyclodextrin production, reduce the energy consumption and also be able to reduce the production cost of cyclodextrin.
format Undergraduates Project Papers
author Nor Ashikin , Abdul Hamid
author_facet Nor Ashikin , Abdul Hamid
author_sort Nor Ashikin , Abdul Hamid
title Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology
title_short Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology
title_full Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology
title_fullStr Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology
title_full_unstemmed Optimization of encapsulation of natural dye by cyclodextrin using response surface methodology
title_sort optimization of encapsulation of natural dye by cyclodextrin using response surface methodology
publishDate 2010
url http://umpir.ump.edu.my/id/eprint/5353/1/CD5870.pdf
http://umpir.ump.edu.my/id/eprint/5353/
_version_ 1705056952651874304
score 13.211869

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