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Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method

Commiphora gileadensis is a medicinal plant with a wide range of biological characteristics. Many medical diseases can be treated using the leaves of C. gileadensis, including bacterial infections, inflammatory illnesses, and wounds. As a result, the Soxhlet extraction method was used to extract the...

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Main Authors: Aiman A., Mokaizh, Nour, Abdurahman Hamid, Alazaiza, M. Y. D., Mustafa, Sara Elkheir, Omer, Manal Suliman, Nassani, Dia Eddin
Format: Article
Language:English
Published: MDPI 2024
Subjects:
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/42371/1/Extraction%20and%20characterization%20of%20biological%20phytoconstituents%20of%20commiphora%20gileadensis%20leaves%20using%20soxhlet%20method.pdf
http://umpir.ump.edu.my/id/eprint/42371/
https://doi.org/10.3390/pr12081567
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spelling my.ump.umpir.423712024-08-15T05:03:42Z http://umpir.ump.edu.my/id/eprint/42371/ Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method Aiman A., Mokaizh Nour, Abdurahman Hamid Alazaiza, M. Y. D. Mustafa, Sara Elkheir Omer, Manal Suliman Nassani, Dia Eddin TP Chemical technology Commiphora gileadensis is a medicinal plant with a wide range of biological characteristics. Many medical diseases can be treated using the leaves of C. gileadensis, including bacterial infections, inflammatory illnesses, and wounds. As a result, the Soxhlet extraction method was used to extract the phenolic components and measure the recovery yields from C. gileadensis leaf. The impacts of the Soxhlet extraction parameters (extraction time 30–150 min, sample/solvent ratio 1:20–1:40 g/mL, and concentration of ethanol solvent 20–100% v/v) on the total flavonoid content (TFC), total phenolic content (TPC), and extraction yield were investigated using the one-factor-at-a-time (OFAT) technique. Fourier transform infrared spectroscopy (FTIR) and gas chromatography–mass spectroscopy (GC–MS) analyses have been employed to evaluate the extracts for the presence of various phytochemicals. According to the results, the C. gileadensis leafs ethanolic extract extracted via the Soxhlet process achieved the maximum yields at 90 min of extraction time, a feed/solvent ratio of 1:30 g/mL, and a 40% v/v ethanol concentration. These yields were: extraction yield = 23.20 ± 0.10% w/w, TPC = 59.93 ± 1.33 mg GAE/g d.w., and TFC = 19.65 ± 1.77 mg QE/g d.w.. Further, a total of 20 phenolic components with excellent antioxidant characteristics were found in the leaf extract of C. gileadensis extracted via the Soxhlet method. MDPI 2024 Article PeerReviewed pdf en cc_by_4 http://umpir.ump.edu.my/id/eprint/42371/1/Extraction%20and%20characterization%20of%20biological%20phytoconstituents%20of%20commiphora%20gileadensis%20leaves%20using%20soxhlet%20method.pdf Aiman A., Mokaizh and Nour, Abdurahman Hamid and Alazaiza, M. Y. D. and Mustafa, Sara Elkheir and Omer, Manal Suliman and Nassani, Dia Eddin (2024) Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method. Processes, 12 (1567). pp. 1-11. ISSN 2227-9717. (Published) https://doi.org/10.3390/pr12081567 10.3390/pr12081567
institution Universiti Malaysia Pahang Al-Sultan Abdullah
building UMPSA Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang Al-Sultan Abdullah
content_source UMPSA Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Aiman A., Mokaizh
Nour, Abdurahman Hamid
Alazaiza, M. Y. D.
Mustafa, Sara Elkheir
Omer, Manal Suliman
Nassani, Dia Eddin
Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method
description Commiphora gileadensis is a medicinal plant with a wide range of biological characteristics. Many medical diseases can be treated using the leaves of C. gileadensis, including bacterial infections, inflammatory illnesses, and wounds. As a result, the Soxhlet extraction method was used to extract the phenolic components and measure the recovery yields from C. gileadensis leaf. The impacts of the Soxhlet extraction parameters (extraction time 30–150 min, sample/solvent ratio 1:20–1:40 g/mL, and concentration of ethanol solvent 20–100% v/v) on the total flavonoid content (TFC), total phenolic content (TPC), and extraction yield were investigated using the one-factor-at-a-time (OFAT) technique. Fourier transform infrared spectroscopy (FTIR) and gas chromatography–mass spectroscopy (GC–MS) analyses have been employed to evaluate the extracts for the presence of various phytochemicals. According to the results, the C. gileadensis leafs ethanolic extract extracted via the Soxhlet process achieved the maximum yields at 90 min of extraction time, a feed/solvent ratio of 1:30 g/mL, and a 40% v/v ethanol concentration. These yields were: extraction yield = 23.20 ± 0.10% w/w, TPC = 59.93 ± 1.33 mg GAE/g d.w., and TFC = 19.65 ± 1.77 mg QE/g d.w.. Further, a total of 20 phenolic components with excellent antioxidant characteristics were found in the leaf extract of C. gileadensis extracted via the Soxhlet method.
format Article
author Aiman A., Mokaizh
Nour, Abdurahman Hamid
Alazaiza, M. Y. D.
Mustafa, Sara Elkheir
Omer, Manal Suliman
Nassani, Dia Eddin
author_facet Aiman A., Mokaizh
Nour, Abdurahman Hamid
Alazaiza, M. Y. D.
Mustafa, Sara Elkheir
Omer, Manal Suliman
Nassani, Dia Eddin
author_sort Aiman A., Mokaizh
title Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method
title_short Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method
title_full Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method
title_fullStr Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method
title_full_unstemmed Extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method
title_sort extraction and characterization of biological phytoconstituents of commiphora gileadensis leaves using soxhlet method
publisher MDPI
publishDate 2024
url http://umpir.ump.edu.my/id/eprint/42371/1/Extraction%20and%20characterization%20of%20biological%20phytoconstituents%20of%20commiphora%20gileadensis%20leaves%20using%20soxhlet%20method.pdf
http://umpir.ump.edu.my/id/eprint/42371/
https://doi.org/10.3390/pr12081567
_version_ 1822924614967230464
score 13.235784

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