Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen

Improving bitumen properties to withstand traffic loads and environmental conditions is essential for prolonging pavement life. Given that nanomaterials stand as potential candidates to fulfil these requirements, this study focused on the potential use of nano eggshell powder (NESP) as a sustainable...

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Main Authors: Zghair Chfat, Alattafi Hadi, Haryati, Yaacob, Nurul Hidayah, Mohd Kamaruddin, Al-Saffar, Zaid Hazim, Putra Jaya, Ramadhansyah
Format: Article
Language:English
Published: Elsevier B.V. 2024
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Online Access:http://umpir.ump.edu.my/id/eprint/40915/1/Effects%20of%20nano%20eggshell%20powder%20as%20a%20sustainable%20bio-filler.pdf
http://umpir.ump.edu.my/id/eprint/40915/
https://doi.org/10.1016/j.rineng.2024.102061
https://doi.org/10.1016/j.rineng.2024.102061
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spelling my.ump.umpir.409152024-04-15T00:41:24Z http://umpir.ump.edu.my/id/eprint/40915/ Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen Zghair Chfat, Alattafi Hadi Haryati, Yaacob Nurul Hidayah, Mohd Kamaruddin Al-Saffar, Zaid Hazim Putra Jaya, Ramadhansyah TA Engineering (General). Civil engineering (General) TE Highway engineering. Roads and pavements Improving bitumen properties to withstand traffic loads and environmental conditions is essential for prolonging pavement life. Given that nanomaterials stand as potential candidates to fulfil these requirements, this study focused on the potential use of nano eggshell powder (NESP) as a sustainable additive in bitumen. NESP was produced using a top-down approach with a ball milling machine. Then, 0% (control), 1%, 3%, 5%, 7%, and 9% NESP by weight of bitumen PEN 60/70 was added. Storage stability and X-Ray Diffraction (XRD) tests were performed to assess the compatibility and dispersion of NESP within the bitumen matrix. Penetration, softening point, ductility, viscosity, and dynamic shear rheometer (DSR) tests were performed to assess the physical and rheological properties of the modified bitumen. Fourier Transform Infrared (FTIR), Atomic Force Microscopy (AFM), contact angle, and thermal analysis (TGA) tests were conducted to analyze the microstructure properties. The results from storage stability tests and XRD patterns suggested that NESP was effectively integrated and evenly dispersed within the bitumen matrix. The incorporation of NESP led to improvement in the hardness and cohesion of the bitumen, as evidenced by reductions in penetration and increase in the softening point. However, higher concentrations of NESP resulted in decreased ductility of the bitumen. The addition of NESP into the bitumen resulted in increased viscosity and improved resistance to aging and rutting. Furthermore, the adhesion and thermal properties of bitumen improved with higher NESP content. Notably, the most effective concentration for enhancing bitumen properties was found to be 9% NESP. Elsevier B.V. 2024 Article PeerReviewed pdf en cc_by_nc_nd_4 http://umpir.ump.edu.my/id/eprint/40915/1/Effects%20of%20nano%20eggshell%20powder%20as%20a%20sustainable%20bio-filler.pdf Zghair Chfat, Alattafi Hadi and Haryati, Yaacob and Nurul Hidayah, Mohd Kamaruddin and Al-Saffar, Zaid Hazim and Putra Jaya, Ramadhansyah (2024) Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen. Results in Engineering, 22 (102061). pp. 1-16. ISSN 2590-1230. (Published) https://doi.org/10.1016/j.rineng.2024.102061 https://doi.org/10.1016/j.rineng.2024.102061
institution Universiti Malaysia Pahang Al-Sultan Abdullah
building UMPSA Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang Al-Sultan Abdullah
content_source UMPSA Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic TA Engineering (General). Civil engineering (General)
TE Highway engineering. Roads and pavements
spellingShingle TA Engineering (General). Civil engineering (General)
TE Highway engineering. Roads and pavements
Zghair Chfat, Alattafi Hadi
Haryati, Yaacob
Nurul Hidayah, Mohd Kamaruddin
Al-Saffar, Zaid Hazim
Putra Jaya, Ramadhansyah
Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen
description Improving bitumen properties to withstand traffic loads and environmental conditions is essential for prolonging pavement life. Given that nanomaterials stand as potential candidates to fulfil these requirements, this study focused on the potential use of nano eggshell powder (NESP) as a sustainable additive in bitumen. NESP was produced using a top-down approach with a ball milling machine. Then, 0% (control), 1%, 3%, 5%, 7%, and 9% NESP by weight of bitumen PEN 60/70 was added. Storage stability and X-Ray Diffraction (XRD) tests were performed to assess the compatibility and dispersion of NESP within the bitumen matrix. Penetration, softening point, ductility, viscosity, and dynamic shear rheometer (DSR) tests were performed to assess the physical and rheological properties of the modified bitumen. Fourier Transform Infrared (FTIR), Atomic Force Microscopy (AFM), contact angle, and thermal analysis (TGA) tests were conducted to analyze the microstructure properties. The results from storage stability tests and XRD patterns suggested that NESP was effectively integrated and evenly dispersed within the bitumen matrix. The incorporation of NESP led to improvement in the hardness and cohesion of the bitumen, as evidenced by reductions in penetration and increase in the softening point. However, higher concentrations of NESP resulted in decreased ductility of the bitumen. The addition of NESP into the bitumen resulted in increased viscosity and improved resistance to aging and rutting. Furthermore, the adhesion and thermal properties of bitumen improved with higher NESP content. Notably, the most effective concentration for enhancing bitumen properties was found to be 9% NESP.
format Article
author Zghair Chfat, Alattafi Hadi
Haryati, Yaacob
Nurul Hidayah, Mohd Kamaruddin
Al-Saffar, Zaid Hazim
Putra Jaya, Ramadhansyah
author_facet Zghair Chfat, Alattafi Hadi
Haryati, Yaacob
Nurul Hidayah, Mohd Kamaruddin
Al-Saffar, Zaid Hazim
Putra Jaya, Ramadhansyah
author_sort Zghair Chfat, Alattafi Hadi
title Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen
title_short Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen
title_full Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen
title_fullStr Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen
title_full_unstemmed Effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen
title_sort effects of nano eggshell powder as a sustainable bio-filler on the physical, rheological, and microstructure properties of bitumen
publisher Elsevier B.V.
publishDate 2024
url http://umpir.ump.edu.my/id/eprint/40915/1/Effects%20of%20nano%20eggshell%20powder%20as%20a%20sustainable%20bio-filler.pdf
http://umpir.ump.edu.my/id/eprint/40915/
https://doi.org/10.1016/j.rineng.2024.102061
https://doi.org/10.1016/j.rineng.2024.102061
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