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Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods

Recently, there has been an increase in the number of studies conducted on the process of developing hydroxyapatite (HA) to use in biocomposites. HA can be derived from natural sources such as bovine bone. The HA usage obtained from green mussel shells in biocomposites in this study will be explored...

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Main Authors: Ismail, Rifky, Cionita, Tezara, Lai, Yinling, Fitriyana, Deni Fajar, Siregar, Januar Parlaungan, Bayuseno, Athanasius Priharyoto, Nugraha, Fariz Wisda, Muhamadin, Rilo Chandra, Irawan, Agustinus Purna, Hadi, Agung Efriyo
Format: Article
Language:English
Published: MDPI 2022
Subjects:
T Technology (General)
TA Engineering (General). Civil engineering (General)
TJ Mechanical engineering and machinery
TL Motor vehicles. Aeronautics. Astronautics
Online Access:http://umpir.ump.edu.my/id/eprint/40613/1/Characterization%20of%20PLA_PCL_green%20mussel%20shells%20hydroxyapatite.pdf
http://umpir.ump.edu.my/id/eprint/40613/
https://doi.org/10.3390/ma15238641
https://doi.org/10.3390/ma15238641
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spelling my.ump.umpir.406132024-04-30T06:33:09Z http://umpir.ump.edu.my/id/eprint/40613/ Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods Ismail, Rifky Cionita, Tezara Lai, Yinling Fitriyana, Deni Fajar Siregar, Januar Parlaungan Bayuseno, Athanasius Priharyoto Nugraha, Fariz Wisda Muhamadin, Rilo Chandra Irawan, Agustinus Purna Hadi, Agung Efriyo T Technology (General) TA Engineering (General). Civil engineering (General) TJ Mechanical engineering and machinery TL Motor vehicles. Aeronautics. Astronautics Recently, there has been an increase in the number of studies conducted on the process of developing hydroxyapatite (HA) to use in biocomposites. HA can be derived from natural sources such as bovine bone. The HA usage obtained from green mussel shells in biocomposites in this study will be explored. The research goal is to investigate the composition effect of biomaterials derived from polycaprolactone (PCL), polylactic acid (PLA), as well as HA obtained from green mussel shells with a chemical blending method on mechanical properties and degradation rate. First, 80 mL of chloroform solution was utilized to immerse 16 g of the PLA/PCL mixture with the ratios of 85:15 and 60:40 for 30 min. A magnetic stirrer was used to mix the solution for an additional 30 min at a temperature and speed of 50 °C and 300 rpm. Next, the hydroxyapatite (HA) was added in percentages of 5%, 10%, and 15%, as well as 20% of the PLA/PCL mixture’s total weight. It was then stirred for 1 h at 100 rpm at 65 °C to produce a homogeneous mixture of HA and polymer. The biocomposite mixture was then added into a glass mold as per ASTM D790. Following this, biocomposite specimens were tested for their density, biodegradability, and three points of bending in determining the effect of HA and polymer composition on the degradation rate and mechanical properties. According to the findings of this study, increasing the HA and PLA composition yields a rise in the mechanical properties of the biocomposites. However, the biocomposite degradation rate is increasing. MDPI 2022-12 Article PeerReviewed pdf en cc_by_4 http://umpir.ump.edu.my/id/eprint/40613/1/Characterization%20of%20PLA_PCL_green%20mussel%20shells%20hydroxyapatite.pdf Ismail, Rifky and Cionita, Tezara and Lai, Yinling and Fitriyana, Deni Fajar and Siregar, Januar Parlaungan and Bayuseno, Athanasius Priharyoto and Nugraha, Fariz Wisda and Muhamadin, Rilo Chandra and Irawan, Agustinus Purna and Hadi, Agung Efriyo (2022) Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods. Materials, 15 (8641). pp. 1-17. ISSN 1996-1944. (Published) https://doi.org/10.3390/ma15238641 https://doi.org/10.3390/ma15238641
institution Universiti Malaysia Pahang Al-Sultan Abdullah
building UMPSA Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang Al-Sultan Abdullah
content_source UMPSA Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic T Technology (General)
TA Engineering (General). Civil engineering (General)
TJ Mechanical engineering and machinery
TL Motor vehicles. Aeronautics. Astronautics
spellingShingle T Technology (General)
TA Engineering (General). Civil engineering (General)
TJ Mechanical engineering and machinery
TL Motor vehicles. Aeronautics. Astronautics
Ismail, Rifky
Cionita, Tezara
Lai, Yinling
Fitriyana, Deni Fajar
Siregar, Januar Parlaungan
Bayuseno, Athanasius Priharyoto
Nugraha, Fariz Wisda
Muhamadin, Rilo Chandra
Irawan, Agustinus Purna
Hadi, Agung Efriyo
Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods
description Recently, there has been an increase in the number of studies conducted on the process of developing hydroxyapatite (HA) to use in biocomposites. HA can be derived from natural sources such as bovine bone. The HA usage obtained from green mussel shells in biocomposites in this study will be explored. The research goal is to investigate the composition effect of biomaterials derived from polycaprolactone (PCL), polylactic acid (PLA), as well as HA obtained from green mussel shells with a chemical blending method on mechanical properties and degradation rate. First, 80 mL of chloroform solution was utilized to immerse 16 g of the PLA/PCL mixture with the ratios of 85:15 and 60:40 for 30 min. A magnetic stirrer was used to mix the solution for an additional 30 min at a temperature and speed of 50 °C and 300 rpm. Next, the hydroxyapatite (HA) was added in percentages of 5%, 10%, and 15%, as well as 20% of the PLA/PCL mixture’s total weight. It was then stirred for 1 h at 100 rpm at 65 °C to produce a homogeneous mixture of HA and polymer. The biocomposite mixture was then added into a glass mold as per ASTM D790. Following this, biocomposite specimens were tested for their density, biodegradability, and three points of bending in determining the effect of HA and polymer composition on the degradation rate and mechanical properties. According to the findings of this study, increasing the HA and PLA composition yields a rise in the mechanical properties of the biocomposites. However, the biocomposite degradation rate is increasing.
format Article
author Ismail, Rifky
Cionita, Tezara
Lai, Yinling
Fitriyana, Deni Fajar
Siregar, Januar Parlaungan
Bayuseno, Athanasius Priharyoto
Nugraha, Fariz Wisda
Muhamadin, Rilo Chandra
Irawan, Agustinus Purna
Hadi, Agung Efriyo
author_facet Ismail, Rifky
Cionita, Tezara
Lai, Yinling
Fitriyana, Deni Fajar
Siregar, Januar Parlaungan
Bayuseno, Athanasius Priharyoto
Nugraha, Fariz Wisda
Muhamadin, Rilo Chandra
Irawan, Agustinus Purna
Hadi, Agung Efriyo
author_sort Ismail, Rifky
title Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods
title_short Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods
title_full Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods
title_fullStr Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods
title_full_unstemmed Characterization of PLA/PCL/green mussel shells Hydroxyapatite (HA) biocomposites prepared by chemical blending methods
title_sort characterization of pla/pcl/green mussel shells hydroxyapatite (ha) biocomposites prepared by chemical blending methods
publisher MDPI
publishDate 2022
url http://umpir.ump.edu.my/id/eprint/40613/1/Characterization%20of%20PLA_PCL_green%20mussel%20shells%20hydroxyapatite.pdf
http://umpir.ump.edu.my/id/eprint/40613/
https://doi.org/10.3390/ma15238641
https://doi.org/10.3390/ma15238641
_version_ 1822924244794736640
score 13.235362

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