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Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method

Iron oxide nanoparticles (NPs) have potential in biological, biomedical, and environmental applications because of their characteristics such as magnetic susceptibility, stability and biocompatibility. However, it also has limitation, such as aggregation of magnetic NP. As a result, coating material...

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Main Authors: Siti Hajar, Omar, Rosli, Mohd Yunus, Khan, Maksudur R., Mohd Mawardi, Saari
Format: Article
Language:English
Published: Universiti Malaysia Pahang 2023
Subjects:
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/40424/1/Ferromagnetic%20Enhancement%20of%20Microcrystalline%20Cellulose.pdf
http://umpir.ump.edu.my/id/eprint/40424/
https://doi.org/10.15282/jceib.v9i2.9253
https://doi.org/10.15282/jceib.v9i2.9253
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spelling my.ump.umpir.404242024-02-19T06:59:10Z http://umpir.ump.edu.my/id/eprint/40424/ Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method Siti Hajar, Omar Rosli, Mohd Yunus Khan, Maksudur R. Mohd Mawardi, Saari TP Chemical technology Iron oxide nanoparticles (NPs) have potential in biological, biomedical, and environmental applications because of their characteristics such as magnetic susceptibility, stability and biocompatibility. However, it also has limitation, such as aggregation of magnetic NP. As a result, coating materials should be used to modify the particles’ outer surface. In this paper, we focused on the synthesis of iron oxide by chemical reduction method and coating it with Fe(III) nitrate, polyvinylpyrrolidone (PVP) and hydrazine. In order to determine effective and economical usage conditions, the coating solution at two different concentrations were prepared. The effect of coating iron oxide with microcrystalline cellulose (MCC) was prepared at different concentrations of iron (III) nitrate on the nanomaterials with respect to morphological, thermal, magnetic susceptibility. A good morphology images of FeNp-MCC were proved by Scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Energy dispersive X-ray (EDX) spectra reveals the presence of carbon, oxygen and iron in the synthesized microparticles. TGA analysis showed iron material was successfully formed into the surface of MCC. Lastly, the magnetism results proved that cellulose is strongly interacting with magnetite nanoparticles. Universiti Malaysia Pahang 2023-12 Article PeerReviewed pdf en cc_by_nc_4 http://umpir.ump.edu.my/id/eprint/40424/1/Ferromagnetic%20Enhancement%20of%20Microcrystalline%20Cellulose.pdf Siti Hajar, Omar and Rosli, Mohd Yunus and Khan, Maksudur R. and Mohd Mawardi, Saari (2023) Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method. Journal of Chemical Engineering and Industrial Biotechnology (JCEIB), 9 (2). pp. 33-40. ISSN 0126-8139. (Published) https://doi.org/10.15282/jceib.v9i2.9253 https://doi.org/10.15282/jceib.v9i2.9253
institution Universiti Malaysia Pahang Al-Sultan Abdullah
building UMPSA Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang Al-Sultan Abdullah
content_source UMPSA Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic TP Chemical technology
spellingShingle TP Chemical technology
Siti Hajar, Omar
Rosli, Mohd Yunus
Khan, Maksudur R.
Mohd Mawardi, Saari
Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method
description Iron oxide nanoparticles (NPs) have potential in biological, biomedical, and environmental applications because of their characteristics such as magnetic susceptibility, stability and biocompatibility. However, it also has limitation, such as aggregation of magnetic NP. As a result, coating materials should be used to modify the particles’ outer surface. In this paper, we focused on the synthesis of iron oxide by chemical reduction method and coating it with Fe(III) nitrate, polyvinylpyrrolidone (PVP) and hydrazine. In order to determine effective and economical usage conditions, the coating solution at two different concentrations were prepared. The effect of coating iron oxide with microcrystalline cellulose (MCC) was prepared at different concentrations of iron (III) nitrate on the nanomaterials with respect to morphological, thermal, magnetic susceptibility. A good morphology images of FeNp-MCC were proved by Scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Energy dispersive X-ray (EDX) spectra reveals the presence of carbon, oxygen and iron in the synthesized microparticles. TGA analysis showed iron material was successfully formed into the surface of MCC. Lastly, the magnetism results proved that cellulose is strongly interacting with magnetite nanoparticles.
format Article
author Siti Hajar, Omar
Rosli, Mohd Yunus
Khan, Maksudur R.
Mohd Mawardi, Saari
author_facet Siti Hajar, Omar
Rosli, Mohd Yunus
Khan, Maksudur R.
Mohd Mawardi, Saari
author_sort Siti Hajar, Omar
title Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method
title_short Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method
title_full Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method
title_fullStr Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method
title_full_unstemmed Ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method
title_sort ferromagnetic enhancement of microcrystalline cellulose via chemical reduction method
publisher Universiti Malaysia Pahang
publishDate 2023
url http://umpir.ump.edu.my/id/eprint/40424/1/Ferromagnetic%20Enhancement%20of%20Microcrystalline%20Cellulose.pdf
http://umpir.ump.edu.my/id/eprint/40424/
https://doi.org/10.15282/jceib.v9i2.9253
https://doi.org/10.15282/jceib.v9i2.9253
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score 13.244413

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