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Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design

In this work, stannic oxide (SnO2) nanoparticles were biologically synthesized utilizing the polysaccharide extract of gum acacia by performing the calcination of stannous chloride precursors at 450° centigrade. The confirmation of SnO2 nanoparticles was done through various characterizations. Makin...

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Main Authors:	Dash, Archita Rani, Lakhani, Aadit J., Priya, Duraipandi Devi, Surendra, T. V., Khan, Md. Maksudur Rahman, Samuel, E. James Jebaseelan, Roopan, Selvaraj Mohana
Format:	Article
Language:	English
Published:	Springer 2021
Subjects:	TP Chemical technology
Online Access:	http://umpir.ump.edu.my/id/eprint/34396/1/Green%20synthesis%20of%20stannic%20oxide%20nanoparticles.pdf http://umpir.ump.edu.my/id/eprint/34396/ https://doi.org/10.1007/s10876-021-02198-y https://doi.org/10.1007/s10876-021-02198-y
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spelling	my.ump.umpir.343962022-11-15T07:52:28Z http://umpir.ump.edu.my/id/eprint/34396/ Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design Dash, Archita Rani Lakhani, Aadit J. Priya, Duraipandi Devi Surendra, T. V. Khan, Md. Maksudur Rahman Samuel, E. James Jebaseelan Roopan, Selvaraj Mohana TP Chemical technology In this work, stannic oxide (SnO2) nanoparticles were biologically synthesized utilizing the polysaccharide extract of gum acacia by performing the calcination of stannous chloride precursors at 450° centigrade. The confirmation of SnO2 nanoparticles was done through various characterizations. Making use of the Scherer formula within the XRD analysis, the dimensions confirmed for the synthesized nanoparticles of SnO2 was obtained to be 4.66 nm. SnO2 NPs are 4.22 nm in size, according to TEM images. ciprofloxacin is a frequently utilized antibiotic as well as exclusive therapy for bacterial infections, and not viral pathogens. In this report, ciprofloxacin photocatalytic degradation in presence of stannic oxide was investigated, which was confirmed by the UV–Vis characterization. The results also optimized using RSM optimization and indicated that the efficiency of ciprofloxacin removal is 99.7% under the optimum conditions of experimental factors (catalyst concentration (R1) in 50 mg/L, ciprofloxacin dose (R2) in 0.5 g/L, and Reaction time (R3) in 120 min). These results suggest that these nanoparticles possess great potential for removing ciprofloxacin from aqueous solutions. Springer 2021 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/34396/1/Green%20synthesis%20of%20stannic%20oxide%20nanoparticles.pdf Dash, Archita Rani and Lakhani, Aadit J. and Priya, Duraipandi Devi and Surendra, T. V. and Khan, Md. Maksudur Rahman and Samuel, E. James Jebaseelan and Roopan, Selvaraj Mohana (2021) Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design. Journal of Cluster Science. pp. 1-13. ISSN 1572-8862 https://doi.org/10.1007/s10876-021-02198-y https://doi.org/10.1007/s10876-021-02198-y
institution	Universiti Malaysia Pahang
building	UMP Library
collection	Institutional Repository
continent	Asia
country	Malaysia
content_provider	Universiti Malaysia Pahang
content_source	UMP Institutional Repository
url_provider	http://umpir.ump.edu.my/
language	English
topic	TP Chemical technology
spellingShingle	TP Chemical technology Dash, Archita Rani Lakhani, Aadit J. Priya, Duraipandi Devi Surendra, T. V. Khan, Md. Maksudur Rahman Samuel, E. James Jebaseelan Roopan, Selvaraj Mohana Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
description	In this work, stannic oxide (SnO2) nanoparticles were biologically synthesized utilizing the polysaccharide extract of gum acacia by performing the calcination of stannous chloride precursors at 450° centigrade. The confirmation of SnO2 nanoparticles was done through various characterizations. Making use of the Scherer formula within the XRD analysis, the dimensions confirmed for the synthesized nanoparticles of SnO2 was obtained to be 4.66 nm. SnO2 NPs are 4.22 nm in size, according to TEM images. ciprofloxacin is a frequently utilized antibiotic as well as exclusive therapy for bacterial infections, and not viral pathogens. In this report, ciprofloxacin photocatalytic degradation in presence of stannic oxide was investigated, which was confirmed by the UV–Vis characterization. The results also optimized using RSM optimization and indicated that the efficiency of ciprofloxacin removal is 99.7% under the optimum conditions of experimental factors (catalyst concentration (R1) in 50 mg/L, ciprofloxacin dose (R2) in 0.5 g/L, and Reaction time (R3) in 120 min). These results suggest that these nanoparticles possess great potential for removing ciprofloxacin from aqueous solutions.
format	Article
author	Dash, Archita Rani Lakhani, Aadit J. Priya, Duraipandi Devi Surendra, T. V. Khan, Md. Maksudur Rahman Samuel, E. James Jebaseelan Roopan, Selvaraj Mohana
author_facet	Dash, Archita Rani Lakhani, Aadit J. Priya, Duraipandi Devi Surendra, T. V. Khan, Md. Maksudur Rahman Samuel, E. James Jebaseelan Roopan, Selvaraj Mohana
author_sort	Dash, Archita Rani
title	Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_short	Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_full	Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_fullStr	Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_full_unstemmed	Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design
title_sort	green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a response surface methodology (rsm) based on the box–behnken design
publisher	Springer
publishDate	2021
url	http://umpir.ump.edu.my/id/eprint/34396/1/Green%20synthesis%20of%20stannic%20oxide%20nanoparticles.pdf http://umpir.ump.edu.my/id/eprint/34396/ https://doi.org/10.1007/s10876-021-02198-y https://doi.org/10.1007/s10876-021-02198-y
_version_	1751536372832796672
score	13.211869

Green synthesis of stannic oxide nanoparticles for ciprofloxacin degradation: optimization and modelling using a Response Surface Methodology (RSM) based on the box–behnken design

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