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Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution

In the present work, the method developed was cellulose modified surface (CMS) to remove heavy metals such as lead II (Pb2+) from aqueous solution. The objective of present work is to investigate the effectiveness of CMS to remove Pb2+ from aqueous solution which includes some certain parameters suc...

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Main Authors: Mohamad Ismail, Mohamad Isa, Siti Maizatul Ameera, Azhar, Nazikussabah, Zaharudin, Ahmad Salihin, Samsudin, Nurlin, Abu Samah
Format: Article
Language:English
Published: John Wiley & Sons, Inc. 2021
Subjects:
QD Chemistry
Online Access:http://umpir.ump.edu.my/id/eprint/31592/1/Pb.pdf
http://umpir.ump.edu.my/id/eprint/31592/
https://onlinelibrary.wiley.com/journal/15213900
https://doi.org/10.1002/masy.202000240
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spelling my.ump.umpir.315922021-07-15T06:43:41Z http://umpir.ump.edu.my/id/eprint/31592/ Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution Mohamad Ismail, Mohamad Isa Siti Maizatul Ameera, Azhar Nazikussabah, Zaharudin Ahmad Salihin, Samsudin Nurlin, Abu Samah QD Chemistry In the present work, the method developed was cellulose modified surface (CMS) to remove heavy metals such as lead II (Pb2+) from aqueous solution. The objective of present work is to investigate the effectiveness of CMS to remove Pb2+ from aqueous solution which includes some certain parameters such as kinetic study, saturation study and pH effect. CMS was prepared by acidification method then the activated cellulose was mixed with allylthiourea and acetonitrile. CMS was characterized using Atomic Absorption Spectrometer (AAS), Fourier Transform Infrared Spectroscopy (FTIR) and Elemental Analyzer. The most efficient time for sorption was 180 minutes with sorption capacity of 46%. For saturation study, the highest sorption is 45.89% at the concentration of 1.389 mg/L. In pH study, it has been found that CMS works the best at pH 7 (64.35%). For qualitative analysis, based on FTIR spectra, there is difference between before and after sorption of CMS. This difference could indicate there is Pb2+ on the surface of CMS. Elemental analysis indicates that there is oxidation process occur on CMS surface that shows attachment of thiol group on the surface. In conclusion, further study is required in order to enhance the CMS capability to remove more Pb2+ from aqueous solution. John Wiley & Sons, Inc. 2021-06-17 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/31592/1/Pb.pdf Mohamad Ismail, Mohamad Isa and Siti Maizatul Ameera, Azhar and Nazikussabah, Zaharudin and Ahmad Salihin, Samsudin and Nurlin, Abu Samah (2021) Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution. Macromolecular Symposia, 397 (1). p. 2000240. ISSN 1521-3900 https://onlinelibrary.wiley.com/journal/15213900 https://doi.org/10.1002/masy.202000240
institution Universiti Malaysia Pahang
building UMP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang
content_source UMP Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic QD Chemistry
spellingShingle QD Chemistry
Mohamad Ismail, Mohamad Isa
Siti Maizatul Ameera, Azhar
Nazikussabah, Zaharudin
Ahmad Salihin, Samsudin
Nurlin, Abu Samah
Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution
description In the present work, the method developed was cellulose modified surface (CMS) to remove heavy metals such as lead II (Pb2+) from aqueous solution. The objective of present work is to investigate the effectiveness of CMS to remove Pb2+ from aqueous solution which includes some certain parameters such as kinetic study, saturation study and pH effect. CMS was prepared by acidification method then the activated cellulose was mixed with allylthiourea and acetonitrile. CMS was characterized using Atomic Absorption Spectrometer (AAS), Fourier Transform Infrared Spectroscopy (FTIR) and Elemental Analyzer. The most efficient time for sorption was 180 minutes with sorption capacity of 46%. For saturation study, the highest sorption is 45.89% at the concentration of 1.389 mg/L. In pH study, it has been found that CMS works the best at pH 7 (64.35%). For qualitative analysis, based on FTIR spectra, there is difference between before and after sorption of CMS. This difference could indicate there is Pb2+ on the surface of CMS. Elemental analysis indicates that there is oxidation process occur on CMS surface that shows attachment of thiol group on the surface. In conclusion, further study is required in order to enhance the CMS capability to remove more Pb2+ from aqueous solution.
format Article
author Mohamad Ismail, Mohamad Isa
Siti Maizatul Ameera, Azhar
Nazikussabah, Zaharudin
Ahmad Salihin, Samsudin
Nurlin, Abu Samah
author_facet Mohamad Ismail, Mohamad Isa
Siti Maizatul Ameera, Azhar
Nazikussabah, Zaharudin
Ahmad Salihin, Samsudin
Nurlin, Abu Samah
author_sort Mohamad Ismail, Mohamad Isa
title Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution
title_short Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution
title_full Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution
title_fullStr Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution
title_full_unstemmed Synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution
title_sort synthesis and characterization of cellulose modified surface to remove lead (Ⅱ) from aqueous solution
publisher John Wiley & Sons, Inc.
publishDate 2021
url http://umpir.ump.edu.my/id/eprint/31592/1/Pb.pdf
http://umpir.ump.edu.my/id/eprint/31592/
https://onlinelibrary.wiley.com/journal/15213900
https://doi.org/10.1002/masy.202000240
_version_ 1706957249436450816
score 13.211869

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