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Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization

Phenolic acids from Q.Infectoria (QI) galls were extracted using focused–type ultrasound extraction method and further optimized using sequential optimization by response surface methodology (RSM). Different independent variables of sonication time, A (6–10 h), solvent concentration, B (0.05–0.15 M)...

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Main Authors: N. F., Sukor, R., Jusoh, N. S., Kamarudin
Format: Article
Language:English
English
Published: Elsevier Ltd 2020
Subjects:
TP Chemical technology
Online Access:http://umpir.ump.edu.my/id/eprint/28775/1/Focused%E2%80%93type%20ultrasound%20extraction%20of%20phenolic%20acids%20from%20Q.Infectoria_FULL.pdf
http://umpir.ump.edu.my/id/eprint/28775/2/Focused%E2%80%93type%20ultrasound%20extraction%20of%20phenolic%20acids%20from%20Q.Infectoria%20.pdf
http://umpir.ump.edu.my/id/eprint/28775/
https://doi.org/10.1016/j.cep.2020.108004
https://doi.org/10.1016/j.cep.2020.108004
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spelling my.ump.umpir.287752022-06-20T03:24:53Z http://umpir.ump.edu.my/id/eprint/28775/ Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization N. F., Sukor R., Jusoh N. S., Kamarudin TP Chemical technology Phenolic acids from Q.Infectoria (QI) galls were extracted using focused–type ultrasound extraction method and further optimized using sequential optimization by response surface methodology (RSM). Different independent variables of sonication time, A (6–10 h), solvent concentration, B (0.05–0.15 M), ratio, C (1:05–1:15), duty cycle, D (30–50 %) and temperature, E (60–80 °C) were first screened via full factorial design (FFD) and the obtained results indicated that sonication time, ratio and temperature were the most significant variables in attaining higher yields. The significant curvature from focused–type ultrasound performance provides insights to a subsequent optimization of the factorial model via face–centred central composite design (FCCCD). The later results revealed that temperature highly impacted the yield with highest contribution percentage of 56.76 %. Notably, maximum extraction yield of 4119.77 mg/g was achieved at optimum condition of 9 h sonication time, ratio of 1:6 and temperature of 75 °C. Besides, Fick’s model successfully promotes diffusivity and appropriately foreseen that temperature factor governed the extraction process from QI galls. Relevant activation energy of 83.39 J/mol, along with the thermodynamic factors which include activation enthalpy (ΔH*) and activation Gibbs free energy (ΔG*), affirmed the extraction process was endothermic and non-spontaneous in identity. Elsevier Ltd 2020-06-21 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/28775/1/Focused%E2%80%93type%20ultrasound%20extraction%20of%20phenolic%20acids%20from%20Q.Infectoria_FULL.pdf pdf en http://umpir.ump.edu.my/id/eprint/28775/2/Focused%E2%80%93type%20ultrasound%20extraction%20of%20phenolic%20acids%20from%20Q.Infectoria%20.pdf N. F., Sukor and R., Jusoh and N. S., Kamarudin (2020) Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization. Chemical Engineering and Processing - Process Intensification, 154 (108004). pp. 1-14. ISSN 0255-2701 https://doi.org/10.1016/j.cep.2020.108004 https://doi.org/10.1016/j.cep.2020.108004
institution Universiti Malaysia Pahang
building UMP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang
content_source UMP Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
English
topic TP Chemical technology
spellingShingle TP Chemical technology
N. F., Sukor
R., Jusoh
N. S., Kamarudin
Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization
description Phenolic acids from Q.Infectoria (QI) galls were extracted using focused–type ultrasound extraction method and further optimized using sequential optimization by response surface methodology (RSM). Different independent variables of sonication time, A (6–10 h), solvent concentration, B (0.05–0.15 M), ratio, C (1:05–1:15), duty cycle, D (30–50 %) and temperature, E (60–80 °C) were first screened via full factorial design (FFD) and the obtained results indicated that sonication time, ratio and temperature were the most significant variables in attaining higher yields. The significant curvature from focused–type ultrasound performance provides insights to a subsequent optimization of the factorial model via face–centred central composite design (FCCCD). The later results revealed that temperature highly impacted the yield with highest contribution percentage of 56.76 %. Notably, maximum extraction yield of 4119.77 mg/g was achieved at optimum condition of 9 h sonication time, ratio of 1:6 and temperature of 75 °C. Besides, Fick’s model successfully promotes diffusivity and appropriately foreseen that temperature factor governed the extraction process from QI galls. Relevant activation energy of 83.39 J/mol, along with the thermodynamic factors which include activation enthalpy (ΔH*) and activation Gibbs free energy (ΔG*), affirmed the extraction process was endothermic and non-spontaneous in identity.
format Article
author N. F., Sukor
R., Jusoh
N. S., Kamarudin
author_facet N. F., Sukor
R., Jusoh
N. S., Kamarudin
author_sort N. F., Sukor
title Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization
title_short Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization
title_full Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization
title_fullStr Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization
title_full_unstemmed Focused–type ultrasound extraction of phenolic acids from Q.Infectoria galls: process modelling and sequential optimization
title_sort focused–type ultrasound extraction of phenolic acids from q.infectoria galls: process modelling and sequential optimization
publisher Elsevier Ltd
publishDate 2020
url http://umpir.ump.edu.my/id/eprint/28775/1/Focused%E2%80%93type%20ultrasound%20extraction%20of%20phenolic%20acids%20from%20Q.Infectoria_FULL.pdf
http://umpir.ump.edu.my/id/eprint/28775/2/Focused%E2%80%93type%20ultrasound%20extraction%20of%20phenolic%20acids%20from%20Q.Infectoria%20.pdf
http://umpir.ump.edu.my/id/eprint/28775/
https://doi.org/10.1016/j.cep.2020.108004
https://doi.org/10.1016/j.cep.2020.108004
_version_ 1736833884126969856
score 13.211869

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