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Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents

Zeolite T were synthesized from molar chemical composition of 1 SiO2: 0.04 Al2O3: 0.26 Na2O: 0.09 K2O: 14 H2O in form of homogenous milky solution in presence of two different structure directing agents of TMAOH and TEAOH respectively. Modification for composition of silica were using metakaolin fr...

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Main Authors: Sazmal E., Arshad, Lutfor, M. R., Sarkar, Shaheen M., Eddy F., Yusslee, Siti Z., Patuwan
Format: Article
Language:English
English
Published: Institute of Physics Publishing 2017
Subjects:
QD Chemistry
Online Access:http://umpir.ump.edu.my/id/eprint/19782/1/10.1088%402053-1591%40aa9d05.pdf
http://umpir.ump.edu.my/id/eprint/19782/7/fist-2017-shaheen.pdf
http://umpir.ump.edu.my/id/eprint/19782/
https://doi.org/10.1088/2053-1591/aa9d05
https://doi.org/10.1088/2053-1591/aa9d05
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spelling my.ump.umpir.197822018-02-14T07:29:16Z http://umpir.ump.edu.my/id/eprint/19782/ Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents Sazmal E., Arshad Lutfor, M. R. Sarkar, Shaheen M. Eddy F., Yusslee Siti Z., Patuwan QD Chemistry Zeolite T were synthesized from molar chemical composition of 1 SiO2: 0.04 Al2O3: 0.26 Na2O: 0.09 K2O: 14 H2O in form of homogenous milky solution in presence of two different structure directing agents of TMAOH and TEAOH respectively. Modification for composition of silica were using metakaolin from calcined kaolin at 750 ˚C in 4 h while molar composition of each different SDA were variated from 0.05, 0.10, 0.15, 0.20 and 0.25. The homogenous mixture was left at room temperature for 24 h before undergoing hydrothermal synthesis at 100 ˚C for 168 hours. Synthesized samples filtered and aged at 120 ˚C for 2 h and each samples were calcined at high temperatures(545oC for TMAOH and 520oC for TEAOH) for templates removal before characterization using XRD and SEM. Crystallization of zeolite T in major form were only at molar ratio of 0.10 of TMAOH while in TEAOH showed species evolution of zeolite T into zeolite L and W for the other molar ratios. Institute of Physics Publishing 2017-12 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/19782/1/10.1088%402053-1591%40aa9d05.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/19782/7/fist-2017-shaheen.pdf Sazmal E., Arshad and Lutfor, M. R. and Sarkar, Shaheen M. and Eddy F., Yusslee and Siti Z., Patuwan (2017) Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents. Materials Research Express, 5 (015011). pp. 1-11. ISSN 2053-1591 https://doi.org/10.1088/2053-1591/aa9d05 https://doi.org/10.1088/2053-1591/aa9d05
institution Universiti Malaysia Pahang
building UMP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang
content_source UMP Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
English
topic QD Chemistry
spellingShingle QD Chemistry
Sazmal E., Arshad
Lutfor, M. R.
Sarkar, Shaheen M.
Eddy F., Yusslee
Siti Z., Patuwan
Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents
description Zeolite T were synthesized from molar chemical composition of 1 SiO2: 0.04 Al2O3: 0.26 Na2O: 0.09 K2O: 14 H2O in form of homogenous milky solution in presence of two different structure directing agents of TMAOH and TEAOH respectively. Modification for composition of silica were using metakaolin from calcined kaolin at 750 ˚C in 4 h while molar composition of each different SDA were variated from 0.05, 0.10, 0.15, 0.20 and 0.25. The homogenous mixture was left at room temperature for 24 h before undergoing hydrothermal synthesis at 100 ˚C for 168 hours. Synthesized samples filtered and aged at 120 ˚C for 2 h and each samples were calcined at high temperatures(545oC for TMAOH and 520oC for TEAOH) for templates removal before characterization using XRD and SEM. Crystallization of zeolite T in major form were only at molar ratio of 0.10 of TMAOH while in TEAOH showed species evolution of zeolite T into zeolite L and W for the other molar ratios.
format Article
author Sazmal E., Arshad
Lutfor, M. R.
Sarkar, Shaheen M.
Eddy F., Yusslee
Siti Z., Patuwan
author_facet Sazmal E., Arshad
Lutfor, M. R.
Sarkar, Shaheen M.
Eddy F., Yusslee
Siti Z., Patuwan
author_sort Sazmal E., Arshad
title Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents
title_short Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents
title_full Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents
title_fullStr Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents
title_full_unstemmed Hydrothermal Synthesis of Zeolite T from Kaolin using Two Different Structure Directing Agents
title_sort hydrothermal synthesis of zeolite t from kaolin using two different structure directing agents
publisher Institute of Physics Publishing
publishDate 2017
url http://umpir.ump.edu.my/id/eprint/19782/1/10.1088%402053-1591%40aa9d05.pdf
http://umpir.ump.edu.my/id/eprint/19782/7/fist-2017-shaheen.pdf
http://umpir.ump.edu.my/id/eprint/19782/
https://doi.org/10.1088/2053-1591/aa9d05
https://doi.org/10.1088/2053-1591/aa9d05
_version_ 1643668732727263232
score 13.211869

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