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Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires

Authors have investigated the influence of the stabilizer (Boric Acid) concentration during the template-assisted electrochemical deposition of Nickel (Ni) nanowires in Anodic Alumina Oxide (AAO) templates. The synthesis was performed using Ni Sulfate Hexahydrate (NiSO4.6H2O) as metal salts and Bori...

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Main Authors:	J., Kananathan, Sofiah, A. G. N., Mahendran, Samykano, S., Ulakanathan, Nurul Akmal, Che Lah, W. S., Wan Harun, K., Sudhakar, K., Kadirgama, W. K., Ngui, Siregar, J. P.
Format:	Conference or Workshop Item
Language:	English
Published:	IOP Publishing Ltd 2017
Subjects:	Q Science (General)
Online Access:	http://umpir.ump.edu.my/id/eprint/19652/1/Influence%20of%20boric%20acid%20%28H3BO3%29%20concentration%20on%20the%20physical.pdf http://umpir.ump.edu.my/id/eprint/19652/ https://doi.org/10.1088/1757-899X/257/1/012033
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spelling	my.ump.umpir.196522018-08-28T08:17:37Z http://umpir.ump.edu.my/id/eprint/19652/ Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires J., Kananathan Sofiah, A. G. N. Mahendran, Samykano S., Ulakanathan Nurul Akmal, Che Lah W. S., Wan Harun K., Sudhakar K., Kadirgama W. K., Ngui Siregar, J. P. Q Science (General) Authors have investigated the influence of the stabilizer (Boric Acid) concentration during the template-assisted electrochemical deposition of Nickel (Ni) nanowires in Anodic Alumina Oxide (AAO) templates. The synthesis was performed using Ni Sulfate Hexahydrate (NiSO4.6H2O) as metal salts and Boric Acid (H3BO3) as a stabilizer. The mixture of both solutions creates electrolyte and utilized for the electrochemical deposition of Ni nanowires. During the experiment, the boric acid concentration varied between 5 g/L, 37.5 g/L and 60 g/L with a deposition temperature of 80 °C (constant). After the electrochemical deposition process, AAO templates were cleaned with distilled water before dissolution in Sodium Hydroxide (NaOH) solution to obtain the freestanding Ni nanowires. Physical properties of the synthesized Ni nanowires were analyzed using Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive Spectroscopy (EDX) and X-ray Diffraction (XRD). The physical properties of obtained Ni nanowires has eloborated by taking into account the effect of boric acid concentration on the surface morphology, growth length, elemental composition and crystal orientation crystal of the synthesized nickel nanowires. The finding exposes that the boric acid concentration does not influence all aspects in the physicals properties of the synthesized Ni nanowires. The boric acid concentration did not affect the surface texture and crystal orientation. However, shorter Ni nanowires obtained as the concentration of boric acid increased. IOP Publishing Ltd 2017 Conference or Workshop Item PeerReviewed application/pdf en cc_by http://umpir.ump.edu.my/id/eprint/19652/1/Influence%20of%20boric%20acid%20%28H3BO3%29%20concentration%20on%20the%20physical.pdf J., Kananathan and Sofiah, A. G. N. and Mahendran, Samykano and S., Ulakanathan and Nurul Akmal, Che Lah and W. S., Wan Harun and K., Sudhakar and K., Kadirgama and W. K., Ngui and Siregar, J. P. (2017) Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires. In: IOP Conference Series: Materials Science and Engineering, 4th International Conference on Mechanical Engineering Research (ICMER2017), 1-2 August 2017 , Kuantan, Pahang, Malaysia. pp. 1-7., 257 (012033). ISSN 1757-899X https://doi.org/10.1088/1757-899X/257/1/012033
institution	Universiti Malaysia Pahang
building	UMP Library
collection	Institutional Repository
continent	Asia
country	Malaysia
content_provider	Universiti Malaysia Pahang
content_source	UMP Institutional Repository
url_provider	http://umpir.ump.edu.my/
language	English
topic	Q Science (General)
spellingShingle	Q Science (General) J., Kananathan Sofiah, A. G. N. Mahendran, Samykano S., Ulakanathan Nurul Akmal, Che Lah W. S., Wan Harun K., Sudhakar K., Kadirgama W. K., Ngui Siregar, J. P. Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires
description	Authors have investigated the influence of the stabilizer (Boric Acid) concentration during the template-assisted electrochemical deposition of Nickel (Ni) nanowires in Anodic Alumina Oxide (AAO) templates. The synthesis was performed using Ni Sulfate Hexahydrate (NiSO4.6H2O) as metal salts and Boric Acid (H3BO3) as a stabilizer. The mixture of both solutions creates electrolyte and utilized for the electrochemical deposition of Ni nanowires. During the experiment, the boric acid concentration varied between 5 g/L, 37.5 g/L and 60 g/L with a deposition temperature of 80 °C (constant). After the electrochemical deposition process, AAO templates were cleaned with distilled water before dissolution in Sodium Hydroxide (NaOH) solution to obtain the freestanding Ni nanowires. Physical properties of the synthesized Ni nanowires were analyzed using Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive Spectroscopy (EDX) and X-ray Diffraction (XRD). The physical properties of obtained Ni nanowires has eloborated by taking into account the effect of boric acid concentration on the surface morphology, growth length, elemental composition and crystal orientation crystal of the synthesized nickel nanowires. The finding exposes that the boric acid concentration does not influence all aspects in the physicals properties of the synthesized Ni nanowires. The boric acid concentration did not affect the surface texture and crystal orientation. However, shorter Ni nanowires obtained as the concentration of boric acid increased.
format	Conference or Workshop Item
author	J., Kananathan Sofiah, A. G. N. Mahendran, Samykano S., Ulakanathan Nurul Akmal, Che Lah W. S., Wan Harun K., Sudhakar K., Kadirgama W. K., Ngui Siregar, J. P.
author_facet	J., Kananathan Sofiah, A. G. N. Mahendran, Samykano S., Ulakanathan Nurul Akmal, Che Lah W. S., Wan Harun K., Sudhakar K., Kadirgama W. K., Ngui Siregar, J. P.
author_sort	J., Kananathan
title	Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires
title_short	Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires
title_full	Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires
title_fullStr	Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires
title_full_unstemmed	Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires
title_sort	influence of boric acid (h3bo3) concentration on the physical properties of electrochemical deposited nickel (ni) nanowires
publisher	IOP Publishing Ltd
publishDate	2017
url	http://umpir.ump.edu.my/id/eprint/19652/1/Influence%20of%20boric%20acid%20%28H3BO3%29%20concentration%20on%20the%20physical.pdf http://umpir.ump.edu.my/id/eprint/19652/ https://doi.org/10.1088/1757-899X/257/1/012033
_version_	1643668701586653184
score	13.211869

Influence of Boric Acid (H3BO3) Concentration on the Physical Properties of Electrochemical Deposited Nickel (Ni) Nanowires

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