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Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties

This paper investigates the influence of the electrolytic bath temperature on the morphology and physical properties of nickel (Ni) nanowires electrochemically deposited into the anodic alumina oxide porous membrane (AAO). The synthesis was performed using nickel sulfate hexahydrate (NiSO4.6H2O) and...

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Main Authors: Nurhanis Sofiah, Abd Ghafar, Kananathan, J., Samykano, Mahendran, Ulakanathan, S., S. A., Che Ghani, W. S., Wan Harun, Sudhakar, K., K., Kadirgama, W. K., Ngui, Siregar, J. P.
Format: Conference or Workshop Item
Language:English
Published: IOP Publishing 2017
Subjects:
Q Science (General)
QC Physics
QD Chemistry
TJ Mechanical engineering and machinery
Online Access:http://umpir.ump.edu.my/id/eprint/17894/1/fkm-2017-samykano-Electrochemical%20deposited%20nickel%20nanowires.pdf
http://umpir.ump.edu.my/id/eprint/17894/
https://doi.org/10.1088/1757-899X/257/1/012032
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spelling my.ump.umpir.178942018-08-28T08:21:32Z http://umpir.ump.edu.my/id/eprint/17894/ Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties Nurhanis Sofiah, Abd Ghafar Kananathan, J. Samykano, Mahendran Ulakanathan, S. S. A., Che Ghani W. S., Wan Harun Sudhakar, K. K., Kadirgama W. K., Ngui Siregar, J. P. Q Science (General) QC Physics QD Chemistry TJ Mechanical engineering and machinery This paper investigates the influence of the electrolytic bath temperature on the morphology and physical properties of nickel (Ni) nanowires electrochemically deposited into the anodic alumina oxide porous membrane (AAO). The synthesis was performed using nickel sulfate hexahydrate (NiSO4.6H2O) and boric acid (H3BO3) as an electrolytic bath for the electrochemical deposition of Ni nanowires. During the experiment, the electrolyte bath temperature varied from 40°C, 80°C, and 120°C. After the electrochemical deposition process, AAO templates cleaned with distilled water preceding to dissolution in sodium hydroxide (NaOH) solution to obtain free-standing Ni nanowires. Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive Spectroscopy (EDX) and X-ray Diffraction (XRD) analysis were employed to characterize the morphology and physical properties of the synthesized Ni nanowires. Finding reveals the electrodeposition bath temperature significantly influences the morphology and physical properties of the synthesized Ni nanowires. Rougher surface texture, larger crystal size, and longer Ni nanowires obtained as the deposition bath temperature increased. IOP Publishing 2017 Conference or Workshop Item PeerReviewed application/pdf en cc_by http://umpir.ump.edu.my/id/eprint/17894/1/fkm-2017-samykano-Electrochemical%20deposited%20nickel%20nanowires.pdf Nurhanis Sofiah, Abd Ghafar and Kananathan, J. and Samykano, Mahendran and Ulakanathan, S. and S. A., Che Ghani and W. S., Wan Harun and Sudhakar, K. and K., Kadirgama and W. K., Ngui and Siregar, J. P. (2017) Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties. In: IOP Conference Series: Materials Science and Engineering, 4th International Conference on Mechanical Engineering Research (ICMER2017), 1-2 August 2017 , Kuantan, Pahang, Malaysia. pp. 1-8., 257 (012032). ISSN 1757-899X https://doi.org/10.1088/1757-899X/257/1/012032
institution Universiti Malaysia Pahang
building UMP Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaysia Pahang
content_source UMP Institutional Repository
url_provider http://umpir.ump.edu.my/
language English
topic Q Science (General)
QC Physics
QD Chemistry
TJ Mechanical engineering and machinery
spellingShingle Q Science (General)
QC Physics
QD Chemistry
TJ Mechanical engineering and machinery
Nurhanis Sofiah, Abd Ghafar
Kananathan, J.
Samykano, Mahendran
Ulakanathan, S.
S. A., Che Ghani
W. S., Wan Harun
Sudhakar, K.
K., Kadirgama
W. K., Ngui
Siregar, J. P.
Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties
description This paper investigates the influence of the electrolytic bath temperature on the morphology and physical properties of nickel (Ni) nanowires electrochemically deposited into the anodic alumina oxide porous membrane (AAO). The synthesis was performed using nickel sulfate hexahydrate (NiSO4.6H2O) and boric acid (H3BO3) as an electrolytic bath for the electrochemical deposition of Ni nanowires. During the experiment, the electrolyte bath temperature varied from 40°C, 80°C, and 120°C. After the electrochemical deposition process, AAO templates cleaned with distilled water preceding to dissolution in sodium hydroxide (NaOH) solution to obtain free-standing Ni nanowires. Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive Spectroscopy (EDX) and X-ray Diffraction (XRD) analysis were employed to characterize the morphology and physical properties of the synthesized Ni nanowires. Finding reveals the electrodeposition bath temperature significantly influences the morphology and physical properties of the synthesized Ni nanowires. Rougher surface texture, larger crystal size, and longer Ni nanowires obtained as the deposition bath temperature increased.
format Conference or Workshop Item
author Nurhanis Sofiah, Abd Ghafar
Kananathan, J.
Samykano, Mahendran
Ulakanathan, S.
S. A., Che Ghani
W. S., Wan Harun
Sudhakar, K.
K., Kadirgama
W. K., Ngui
Siregar, J. P.
author_facet Nurhanis Sofiah, Abd Ghafar
Kananathan, J.
Samykano, Mahendran
Ulakanathan, S.
S. A., Che Ghani
W. S., Wan Harun
Sudhakar, K.
K., Kadirgama
W. K., Ngui
Siregar, J. P.
author_sort Nurhanis Sofiah, Abd Ghafar
title Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties
title_short Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties
title_full Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties
title_fullStr Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties
title_full_unstemmed Electrochemical Deposited Nickel Nanowires: Influence of Deposition Bath Temperature on the Morphology and Physical Properties
title_sort electrochemical deposited nickel nanowires: influence of deposition bath temperature on the morphology and physical properties
publisher IOP Publishing
publishDate 2017
url http://umpir.ump.edu.my/id/eprint/17894/1/fkm-2017-samykano-Electrochemical%20deposited%20nickel%20nanowires.pdf
http://umpir.ump.edu.my/id/eprint/17894/
https://doi.org/10.1088/1757-899X/257/1/012032
_version_ 1643668301507723264
score 13.211869

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