Optimizing graphene-silver embedded phase change composite synthesis using design of experiments

The paradigm shift from fossil fuels to renewable ones is at stake with the underdeveloped energy storage technology. However, Phase Change Materials (PCMs) are congruent with batteries but possess degraded thermophysical properties, which can be tuned by dispersing nanofillers. Numerous trials are...

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Main Authors: Paul, John, Pandey, A. K., Kadirgama, K., Samykano, M., Jacob, Jeeja, Selvaraj, Jeyraj, Saidur, R.
Format: Article
Published: Elsevier 2024
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Online Access:http://eprints.um.edu.my/45765/
https://doi.org/10.1016/j.est.2024.110523
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spelling my.um.eprints.457652024-11-12T01:37:45Z http://eprints.um.edu.my/45765/ Optimizing graphene-silver embedded phase change composite synthesis using design of experiments Paul, John Pandey, A. K. Kadirgama, K. Samykano, M. Jacob, Jeeja Selvaraj, Jeyraj Saidur, R. TA Engineering (General). Civil engineering (General) The paradigm shift from fossil fuels to renewable ones is at stake with the underdeveloped energy storage technology. However, Phase Change Materials (PCMs) are congruent with batteries but possess degraded thermophysical properties, which can be tuned by dispersing nanofillers. Numerous trials are needed to find the optimum responses for maximal thermophysical properties. This research aims to apply statistical methods for hybrid nanocomposite synthesis to deliver maximal favourable thermophysical properties. Response Surface Methodology with a central composite design was sourced to generate optimal input response conditions for maximal thermal conductivity. The present work also focuses on the synthesis and thermophysical characterization of nanocomposite with nanofillers (graphene: silver) at optimum input response. The maximal thermal conductivity value for the optimum input response of nanofiller and surfactant concentration was 0.412 W/mK, 0.310 %, and 0.313 %, respectively. Statistical parameters (f-values, predicted R-2, observed R-2, adjusted R-2) were used to validate the experimentally developed Response Surface Methodology (RSM) model. The reliability of the predicted model was proved as there was little distinction between simulation data and validation experiments. The induction of statistical methods will significantly reduce the experimental trials and deliver insight into major input parameters and their effects on responses. Moreover, the macro-packed nano phase change composite reduced the surface temperature by 7 degrees C. The thermophysical characterization and experimental results validate the usage of NPCCs as a thermal interface material for building thermal management applications. Elsevier 2024-03 Article PeerReviewed Paul, John and Pandey, A. K. and Kadirgama, K. and Samykano, M. and Jacob, Jeeja and Selvaraj, Jeyraj and Saidur, R. (2024) Optimizing graphene-silver embedded phase change composite synthesis using design of experiments. Journal of Energy Storage, 82. p. 110523. ISSN 2352-152X, DOI https://doi.org/10.1016/j.est.2024.110523 <https://doi.org/10.1016/j.est.2024.110523>. https://doi.org/10.1016/j.est.2024.110523 10.1016/j.est.2024.110523
institution Universiti Malaya
building UM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaya
content_source UM Research Repository
url_provider http://eprints.um.edu.my/
topic TA Engineering (General). Civil engineering (General)
spellingShingle TA Engineering (General). Civil engineering (General)
Paul, John
Pandey, A. K.
Kadirgama, K.
Samykano, M.
Jacob, Jeeja
Selvaraj, Jeyraj
Saidur, R.
Optimizing graphene-silver embedded phase change composite synthesis using design of experiments
description The paradigm shift from fossil fuels to renewable ones is at stake with the underdeveloped energy storage technology. However, Phase Change Materials (PCMs) are congruent with batteries but possess degraded thermophysical properties, which can be tuned by dispersing nanofillers. Numerous trials are needed to find the optimum responses for maximal thermophysical properties. This research aims to apply statistical methods for hybrid nanocomposite synthesis to deliver maximal favourable thermophysical properties. Response Surface Methodology with a central composite design was sourced to generate optimal input response conditions for maximal thermal conductivity. The present work also focuses on the synthesis and thermophysical characterization of nanocomposite with nanofillers (graphene: silver) at optimum input response. The maximal thermal conductivity value for the optimum input response of nanofiller and surfactant concentration was 0.412 W/mK, 0.310 %, and 0.313 %, respectively. Statistical parameters (f-values, predicted R-2, observed R-2, adjusted R-2) were used to validate the experimentally developed Response Surface Methodology (RSM) model. The reliability of the predicted model was proved as there was little distinction between simulation data and validation experiments. The induction of statistical methods will significantly reduce the experimental trials and deliver insight into major input parameters and their effects on responses. Moreover, the macro-packed nano phase change composite reduced the surface temperature by 7 degrees C. The thermophysical characterization and experimental results validate the usage of NPCCs as a thermal interface material for building thermal management applications.
format Article
author Paul, John
Pandey, A. K.
Kadirgama, K.
Samykano, M.
Jacob, Jeeja
Selvaraj, Jeyraj
Saidur, R.
author_facet Paul, John
Pandey, A. K.
Kadirgama, K.
Samykano, M.
Jacob, Jeeja
Selvaraj, Jeyraj
Saidur, R.
author_sort Paul, John
title Optimizing graphene-silver embedded phase change composite synthesis using design of experiments
title_short Optimizing graphene-silver embedded phase change composite synthesis using design of experiments
title_full Optimizing graphene-silver embedded phase change composite synthesis using design of experiments
title_fullStr Optimizing graphene-silver embedded phase change composite synthesis using design of experiments
title_full_unstemmed Optimizing graphene-silver embedded phase change composite synthesis using design of experiments
title_sort optimizing graphene-silver embedded phase change composite synthesis using design of experiments
publisher Elsevier
publishDate 2024
url http://eprints.um.edu.my/45765/
https://doi.org/10.1016/j.est.2024.110523
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score 13.232414