Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs

Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and...

Full description

Saved in:
Bibliographic Details
Main Authors: Ahmad, Pervaiz, Khandaker, Mayeen Uddin, Muhammad, Nawshad, Rehman, Fida, Khan, Ghulamullah, Khan, Amir Sada, Ullah, Zahoor, Rehman, Muhammad Abdur, Ahmed, Sohail, Gulzar, Mubashar, Din, Israf Ud, Ahmed, Syed Muzamil, Ali, Hazrat, Numan, Arshid
Format: Article
Published: Elsevier 2018
Subjects:
Online Access:http://eprints.um.edu.my/22631/
https://doi.org/10.1016/j.materresbull.2017.10.031
Tags: Add Tag
No Tags, Be the first to tag this record!
id my.um.eprints.22631
record_format eprints
spelling my.um.eprints.226312019-10-04T02:49:24Z http://eprints.um.edu.my/22631/ Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs Ahmad, Pervaiz Khandaker, Mayeen Uddin Muhammad, Nawshad Rehman, Fida Khan, Ghulamullah Khan, Amir Sada Ullah, Zahoor Rehman, Muhammad Abdur Ahmed, Sohail Gulzar, Mubashar Din, Israf Ud Ahmed, Syed Muzamil Ali, Hazrat Numan, Arshid Q Science (General) QC Physics QD Chemistry TP Chemical technology Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and misleading but also result in useless impurities in the final product. Here, we report Magnesium diboride (MgB2) as an effective and novel precursor for the synthesis of vertically aligned BNNTs directly on SiO2 substrate at 1000 °C. Magnesium (Mg) from MgB2 in partially melted form diffuses on SiO2 substrate whereas the adsorbed Boron with Mg reacts with Nitrogen from decomposed ammonia and synthesized vertically aligned BNNTs. The morphology, alignment, structure and compositions of the as-synthesized BNNTs are studied via field emission scanning electron microscope, high resolution transmission electron microscope, energy dispersive x-ray spectroscopy, x-ray diffraction, Raman spectroscopy and Fourier transform infrared spectroscopy. Elsevier 2018 Article PeerReviewed Ahmad, Pervaiz and Khandaker, Mayeen Uddin and Muhammad, Nawshad and Rehman, Fida and Khan, Ghulamullah and Khan, Amir Sada and Ullah, Zahoor and Rehman, Muhammad Abdur and Ahmed, Sohail and Gulzar, Mubashar and Din, Israf Ud and Ahmed, Syed Muzamil and Ali, Hazrat and Numan, Arshid (2018) Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs. Materials Research Bulletin, 98. pp. 235-239. ISSN 0025-5408 https://doi.org/10.1016/j.materresbull.2017.10.031 doi:10.1016/j.materresbull.2017.10.031
institution Universiti Malaya
building UM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaya
content_source UM Research Repository
url_provider http://eprints.um.edu.my/
topic Q Science (General)
QC Physics
QD Chemistry
TP Chemical technology
spellingShingle Q Science (General)
QC Physics
QD Chemistry
TP Chemical technology
Ahmad, Pervaiz
Khandaker, Mayeen Uddin
Muhammad, Nawshad
Rehman, Fida
Khan, Ghulamullah
Khan, Amir Sada
Ullah, Zahoor
Rehman, Muhammad Abdur
Ahmed, Sohail
Gulzar, Mubashar
Din, Israf Ud
Ahmed, Syed Muzamil
Ali, Hazrat
Numan, Arshid
Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
description Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and misleading but also result in useless impurities in the final product. Here, we report Magnesium diboride (MgB2) as an effective and novel precursor for the synthesis of vertically aligned BNNTs directly on SiO2 substrate at 1000 °C. Magnesium (Mg) from MgB2 in partially melted form diffuses on SiO2 substrate whereas the adsorbed Boron with Mg reacts with Nitrogen from decomposed ammonia and synthesized vertically aligned BNNTs. The morphology, alignment, structure and compositions of the as-synthesized BNNTs are studied via field emission scanning electron microscope, high resolution transmission electron microscope, energy dispersive x-ray spectroscopy, x-ray diffraction, Raman spectroscopy and Fourier transform infrared spectroscopy.
format Article
author Ahmad, Pervaiz
Khandaker, Mayeen Uddin
Muhammad, Nawshad
Rehman, Fida
Khan, Ghulamullah
Khan, Amir Sada
Ullah, Zahoor
Rehman, Muhammad Abdur
Ahmed, Sohail
Gulzar, Mubashar
Din, Israf Ud
Ahmed, Syed Muzamil
Ali, Hazrat
Numan, Arshid
author_facet Ahmad, Pervaiz
Khandaker, Mayeen Uddin
Muhammad, Nawshad
Rehman, Fida
Khan, Ghulamullah
Khan, Amir Sada
Ullah, Zahoor
Rehman, Muhammad Abdur
Ahmed, Sohail
Gulzar, Mubashar
Din, Israf Ud
Ahmed, Syed Muzamil
Ali, Hazrat
Numan, Arshid
author_sort Ahmad, Pervaiz
title Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_short Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_full Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_fullStr Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_full_unstemmed Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
title_sort magnesium diboride (mgb2): an effective and novel precursor for the synthesis of vertically aligned bnnts
publisher Elsevier
publishDate 2018
url http://eprints.um.edu.my/22631/
https://doi.org/10.1016/j.materresbull.2017.10.031
_version_ 1648736165281398784
score 13.211869