Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs
Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and...
Saved in:
Main Authors: | , , , , , , , , , , , , , |
---|---|
Format: | Article |
Published: |
Elsevier
2018
|
Subjects: | |
Online Access: | http://eprints.um.edu.my/22631/ https://doi.org/10.1016/j.materresbull.2017.10.031 |
Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
id |
my.um.eprints.22631 |
---|---|
record_format |
eprints |
spelling |
my.um.eprints.226312019-10-04T02:49:24Z http://eprints.um.edu.my/22631/ Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs Ahmad, Pervaiz Khandaker, Mayeen Uddin Muhammad, Nawshad Rehman, Fida Khan, Ghulamullah Khan, Amir Sada Ullah, Zahoor Rehman, Muhammad Abdur Ahmed, Sohail Gulzar, Mubashar Din, Israf Ud Ahmed, Syed Muzamil Ali, Hazrat Numan, Arshid Q Science (General) QC Physics QD Chemistry TP Chemical technology Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and misleading but also result in useless impurities in the final product. Here, we report Magnesium diboride (MgB2) as an effective and novel precursor for the synthesis of vertically aligned BNNTs directly on SiO2 substrate at 1000 °C. Magnesium (Mg) from MgB2 in partially melted form diffuses on SiO2 substrate whereas the adsorbed Boron with Mg reacts with Nitrogen from decomposed ammonia and synthesized vertically aligned BNNTs. The morphology, alignment, structure and compositions of the as-synthesized BNNTs are studied via field emission scanning electron microscope, high resolution transmission electron microscope, energy dispersive x-ray spectroscopy, x-ray diffraction, Raman spectroscopy and Fourier transform infrared spectroscopy. Elsevier 2018 Article PeerReviewed Ahmad, Pervaiz and Khandaker, Mayeen Uddin and Muhammad, Nawshad and Rehman, Fida and Khan, Ghulamullah and Khan, Amir Sada and Ullah, Zahoor and Rehman, Muhammad Abdur and Ahmed, Sohail and Gulzar, Mubashar and Din, Israf Ud and Ahmed, Syed Muzamil and Ali, Hazrat and Numan, Arshid (2018) Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs. Materials Research Bulletin, 98. pp. 235-239. ISSN 0025-5408 https://doi.org/10.1016/j.materresbull.2017.10.031 doi:10.1016/j.materresbull.2017.10.031 |
institution |
Universiti Malaya |
building |
UM Library |
collection |
Institutional Repository |
continent |
Asia |
country |
Malaysia |
content_provider |
Universiti Malaya |
content_source |
UM Research Repository |
url_provider |
http://eprints.um.edu.my/ |
topic |
Q Science (General) QC Physics QD Chemistry TP Chemical technology |
spellingShingle |
Q Science (General) QC Physics QD Chemistry TP Chemical technology Ahmad, Pervaiz Khandaker, Mayeen Uddin Muhammad, Nawshad Rehman, Fida Khan, Ghulamullah Khan, Amir Sada Ullah, Zahoor Rehman, Muhammad Abdur Ahmed, Sohail Gulzar, Mubashar Din, Israf Ud Ahmed, Syed Muzamil Ali, Hazrat Numan, Arshid Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs |
description |
Vertically aligned Boron nitride nanotubes (BNNTs) have exceptional electrical, mechanical and thermal properties suitable for its potential applications without any further purification. However, the synthesis of aligned BNNTs via previously reported techniques is not only complicated, lengthy and misleading but also result in useless impurities in the final product. Here, we report Magnesium diboride (MgB2) as an effective and novel precursor for the synthesis of vertically aligned BNNTs directly on SiO2 substrate at 1000 °C. Magnesium (Mg) from MgB2 in partially melted form diffuses on SiO2 substrate whereas the adsorbed Boron with Mg reacts with Nitrogen from decomposed ammonia and synthesized vertically aligned BNNTs. The morphology, alignment, structure and compositions of the as-synthesized BNNTs are studied via field emission scanning electron microscope, high resolution transmission electron microscope, energy dispersive x-ray spectroscopy, x-ray diffraction, Raman spectroscopy and Fourier transform infrared spectroscopy. |
format |
Article |
author |
Ahmad, Pervaiz Khandaker, Mayeen Uddin Muhammad, Nawshad Rehman, Fida Khan, Ghulamullah Khan, Amir Sada Ullah, Zahoor Rehman, Muhammad Abdur Ahmed, Sohail Gulzar, Mubashar Din, Israf Ud Ahmed, Syed Muzamil Ali, Hazrat Numan, Arshid |
author_facet |
Ahmad, Pervaiz Khandaker, Mayeen Uddin Muhammad, Nawshad Rehman, Fida Khan, Ghulamullah Khan, Amir Sada Ullah, Zahoor Rehman, Muhammad Abdur Ahmed, Sohail Gulzar, Mubashar Din, Israf Ud Ahmed, Syed Muzamil Ali, Hazrat Numan, Arshid |
author_sort |
Ahmad, Pervaiz |
title |
Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs |
title_short |
Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs |
title_full |
Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs |
title_fullStr |
Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs |
title_full_unstemmed |
Magnesium diboride (MgB2): An effective and novel precursor for the synthesis of vertically aligned BNNTs |
title_sort |
magnesium diboride (mgb2): an effective and novel precursor for the synthesis of vertically aligned bnnts |
publisher |
Elsevier |
publishDate |
2018 |
url |
http://eprints.um.edu.my/22631/ https://doi.org/10.1016/j.materresbull.2017.10.031 |
_version_ |
1648736165281398784 |
score |
13.211869 |