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Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils

In this research, palm oil and soy oil were used as a natural polyol to prepare novel poly(silyl ether)s. Palm oil and soy oil were first converted to monoglyceride by one step via alcoholysis process in the presence of 0.1% CaO as a catalyst. The monoglycerides were characterized by Fourier transfo...

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Main Authors: Mohammed, Issam Ahmed, Shahabuddin, Syed, Khanam, Rashmin, Saidur, Rahman
Format: Article
Published: Associacao Brasileira de Polimeros 2018
Subjects:
Q Science (General)
QD Chemistry
Online Access:http://eprints.um.edu.my/21245/
https://doi.org/10.1590/0104-1428.10317
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spelling my.um.eprints.212452019-05-15T08:42:24Z http://eprints.um.edu.my/21245/ Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils Mohammed, Issam Ahmed Shahabuddin, Syed Khanam, Rashmin Saidur, Rahman Q Science (General) QD Chemistry In this research, palm oil and soy oil were used as a natural polyol to prepare novel poly(silyl ether)s. Palm oil and soy oil were first converted to monoglyceride by one step via alcoholysis process in the presence of 0.1% CaO as a catalyst. The monoglycerides were characterized by Fourier transform infrared spectrometer (FT-IR), nuclear magnetic resonance (NMR) and iodine test. The novel poly(silyl ether)s were prepared via polycondensation reaction between dimethyldichlorosilane with monoglycerides based on palm and soy oils, respectively. FT-IR, NMR and silicone-29 ( 29 Si NMR) were used to confirm and determine the presence of silicone in the synthesized polymers. Thermal behavior was studied by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). Antibacterial activity of the polymers was screened against three different strains of bacteria, namely Escherichia coli E266, Staphylococcus aureus S276 and Salmonella choleeraesuis 10708. Associacao Brasileira de Polimeros 2018 Article PeerReviewed Mohammed, Issam Ahmed and Shahabuddin, Syed and Khanam, Rashmin and Saidur, Rahman (2018) Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils. Polimeros, 28 (5). pp. 406-412. ISSN 0104-1428 https://doi.org/10.1590/0104-1428.10317 doi:10.1590/0104-1428.10317
institution Universiti Malaya
building UM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Malaya
content_source UM Research Repository
url_provider http://eprints.um.edu.my/
topic Q Science (General)
QD Chemistry
spellingShingle Q Science (General)
QD Chemistry
Mohammed, Issam Ahmed
Shahabuddin, Syed
Khanam, Rashmin
Saidur, Rahman
Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
description In this research, palm oil and soy oil were used as a natural polyol to prepare novel poly(silyl ether)s. Palm oil and soy oil were first converted to monoglyceride by one step via alcoholysis process in the presence of 0.1% CaO as a catalyst. The monoglycerides were characterized by Fourier transform infrared spectrometer (FT-IR), nuclear magnetic resonance (NMR) and iodine test. The novel poly(silyl ether)s were prepared via polycondensation reaction between dimethyldichlorosilane with monoglycerides based on palm and soy oils, respectively. FT-IR, NMR and silicone-29 ( 29 Si NMR) were used to confirm and determine the presence of silicone in the synthesized polymers. Thermal behavior was studied by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). Antibacterial activity of the polymers was screened against three different strains of bacteria, namely Escherichia coli E266, Staphylococcus aureus S276 and Salmonella choleeraesuis 10708.
format Article
author Mohammed, Issam Ahmed
Shahabuddin, Syed
Khanam, Rashmin
Saidur, Rahman
author_facet Mohammed, Issam Ahmed
Shahabuddin, Syed
Khanam, Rashmin
Saidur, Rahman
author_sort Mohammed, Issam Ahmed
title Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_short Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_full Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_fullStr Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_full_unstemmed Synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
title_sort synthesis, characterization and antibacterial activity of novel poly(silyl ether)s based on palm and soy oils
publisher Associacao Brasileira de Polimeros
publishDate 2018
url http://eprints.um.edu.my/21245/
https://doi.org/10.1590/0104-1428.10317
_version_ 1643691508592803840
score 13.211869

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