A generalized energy-based kinetic model for microwave-assisted extraction of bioactive compounds from plants

By considering the absorbed power and energy based on heating power profile during extraction, a generalized model with washing coefficient (b), diffusion coefficient (k) and predictive parameter namely absorbed power density (APD) was developed for microwave-assisted extraction (MAE) at any operati...

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Bibliographic Details
Main Authors: Chan, C.H., Lim, J.J., Yusoff, R., Ngoh, G.C.
Format: Article
Language:English
Published: Separation and Purification Technology 2015
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Online Access:http://eprints.um.edu.my/13752/1/A_generalized_energy-based_kinetic_model_for_microwave.pdf
http://eprints.um.edu.my/13752/
http://www.sciencedirect.com/science/article/pii/S1383586615000702
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Summary:By considering the absorbed power and energy based on heating power profile during extraction, a generalized model with washing coefficient (b), diffusion coefficient (k) and predictive parameter namely absorbed power density (APD) was developed for microwave-assisted extraction (MAE) at any operational heating modes. To study the model, MAE of flavonoids from cocoa (Theobroma cacao L.) leaves was conducted using the heating modes (constant-power, two-steps-power, intermittent-power and constant-temperature) at various microwave power (100-300W) and extraction temperature (50 degrees C and 70 degrees C). The results shows that the model (b = 0.5595 and k' = 0.01279 mL/J) is able to predict the normalized extraction yields of MAE at any heating modes, heating power, microwave system, extraction scale and batch of plant sample with less than 4 discrepancy. The accuracy of the prediction relies on particle size of sample (0.25-0.60 mm), type of extraction solvent (85 aqueous ethanol) and solvent to feed ratio (50 mL/g). (C) 2015 Elsevier B.V. All rights reserved.